Investigation of the Process Optimization for L-PBF Hastelloy X Alloy on Microstructure and Mechanical Properties

Phuangphaga Daram; Masahiro Kusano; Makoto Watanabe

doi:10.3390/ma18081890

Article Investigation of the Process Optimization for L-PBF Hastelloy X Alloy on Microstructure and Mechanical Properties

Phuangphaga Daram (National Institute for Materials Science) ; Masahiro Kusano (National Institute for Materials Science) ; Makoto Watanabe (National Institute for Materials Science)

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Phuangphaga Daram, Masahiro Kusano, Makoto Watanabe. Investigation of the Process Optimization for L-PBF Hastelloy X Alloy on Microstructure and Mechanical Properties. Materials. 2025, 18 (8), 1890. https://doi.org/10.3390/ma18081890

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The purpose of this study is to investigate the effects of process parameters on the mi-crostructure and mechanical properties of the Hastelloy X (HX) alloy using a laser powder bed fusion (L-PBF) process. A combined experimental and numerical approach was used to evaluate the influence of the energy density distribution and temperature evolution on the microstructure, defects, and mechanical properties. After the specimens were built on SUS304 substrate by the L-PBF, the microstructure and defects in the specimens were analyzed by SEM and EBSD analysis methods, and then the hardness and the tensile tests were performed. The cooling rate under different laser conditions was obtained by the finite element method (FEM). The results show that a low volume energy density (VED) was applied to the unmelted powder particles, and a high energy density resulted in spherical defects. In addition, the microstructures were found to coarsen with increasing the energy density along with a tendency to strengthen the (001) texture orientation in both xy and xz planes. Compared to the parts with the thermal history from numerical results, the low cooling rate with high energy density had larger crystal grains elongated along the building direction, coarser sub-grains, resulting in a reduction of microhardness and yield strength together with an increase in elongation for the L-PBF HX alloy. The presented results provide new insight into the effect of parameters and the cooling rates. It can play an important role in optimizing the L-PBF processing parameters, identifying the cause of defects, and controlling the cooling rates for the crystallographic texture in such a way as to guide the development of better metrics for designing processing pa-rameters with the desired mechanical properties.

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