山田 裕久
(エネルギー・環境材料研究拠点/液体水素材料研究センター/水素材料制御グループ, 物質・材料研究機構)
;
横山信吾
(電力中央研究所)
;
八田珠郎
(千葉科学大学)
;
中村 真佐樹
(技術開発・共用部門/材料創製・評価プラットフォーム/表面・バルク分析ユニット, 物質・材料研究機構)
;
鈴木正哉
(産業技術総合研究所)
;
武田 良彦
(エネルギー・環境材料研究センター/水素材料分野/水素関連材料グループ, 物質・材料研究機構)
Alternative title: Hydrothermal synthesis of high-purity layered clay minerals
Description:
(abstract)The hydrothermal method can be used to synthesize high purity layered clay minerals. Experiential techniques for the hydrothermal synthesis of layered clay minerals are described. The method of cleaning, annealing and welding Au capsule in the hydrothermal experiment is also presented. Two types of starting materials: quenched glass and dried gel, were prepared through chemical selection, pretreatment, mixing, and thermal treatment. The starting materials have different chemical compositions of smectite with different layer charge and interlayer cations, and those in smectite-mica pseudobinary system. The synthesized minerals were tabulated with starting material composition, synthesis temperature, and reaction time. The procedure and product list would be useful for clay mineralogy and materials science, especially for materials informatics.
Rights:
Keyword: hydrothermal synthesis, layered clay minerals, experimental procedure
Date published:
Publisher: 一般社団法人 日本粘土学会
Journal:
Funding:
Manuscript type: Publisher's version (Version of record)
MDR DOI:
First published URL: https://doi.org/10.11362/jcssjnendokagaku.63.3_55
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Other identifier(s):
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Updated at: 2024-12-27 16:30:43 +0900
Published on MDR: 2024-12-27 16:30:43 +0900
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