mandatory mandatory 1 column Title タイトル XAFS spectrum of Niobium(V) chloride Anhydrous File Name ファイル名 spring8.c5d3ca66-cbcb-45b0-ac49-a9fe1fd70e0d.zip Description 説明 This dataset consists of X-ray absorption fine structure (XAFS) spectra at Nb K-edge of Niobium(V) chloride, anhydrous measured at SPring-8 BL14B2, and is a part of XAFS database (MDR XAFS DB, https://doi.org/10.48505/nims.1447) as a collection of MDR Data Origin データの起源 experiments Contact Person データ責任者 Industrial Application and Partnership Division Data Creator データ作成者 ISHII, Masashi instrument instrument 1 column instrument_name instrument_name BL14B2_XAFS maker maker Japan Synchrotron Radiation Research Institute instrumentation instrumentation Japan Synchrotron Radiation Research Institute method_category method_category 分光法(X線吸収分光法) description description SPring-8 Engineering Science Research Beamline XAFS setup specimen specimen_meta 1 column Specimen_ID 試料ID 68183796 Description 説明 Standard Sample General name 一般名称 Niobium(V) chloride Anhydrous Chemical composition 化学組成 NbCl5 Material Type 物質タイプ Chloride Material Sub Category 物質サブカテゴリー Niobium(V) chloride, anhydrous Structural Features 構造的特長 局所構造 Structural Sub Category 構造サブカテゴリー 動径分布関数 supplier 製造者・購入先 KOJUNDO CHEMICAL LABORATORY Lot No. /Product No. etc ロット番号/製造番号など NBH01XB measurement measurement_meta 1 column Method category 計測法カテゴリー 分光法 Method sub-category 計測法サブカテゴリー X線吸収分光法 Analysis field 分析分野 結晶学 Measurement environment 測定環境 空気中 Energy Level_Transition_Structure etc. of interst 対象準位_遷移_構造 Nb K-edge Measurement date 分析年月日 2017-04-19 Standardized procedure 標準手順 Transmission( 2) Instrumentation site 装置設置場所 SPring-8/BL14B2 Reference 参考文献 T. Honda, SPring-8/SACLA Information Vol.12 (2007) 276-278. measurement 1 column @data_info@identifier@pid @data_info@identifier@pid spring8.c5d3ca66-cbcb-45b0-ac49-a9fe1fd70e0d @data_info@identifier@proposal_number @data_info@identifier@proposal_number 2014S0000 @data_info@identifier@register_name @data_info@identifier@register_name /SPring-8/BL14B2/XAFS_Standard/Nb/K/311/NbCl5 @data_info@date@create_time @data_info@date@create_time 2020-01-15 19:40:21 @data_info@date@update_time @data_info@date@update_time 2021-03-24 13:53:16 @data_info@access_rights @data_info@access_rights open @data_info@contact_name@affiliation@organization @data_info@contact_name@affiliation@organization JASRI @data_info@contact_name@name @data_info@contact_name@name Industrial Application and Partnership Division @data_info@contact_name@role @data_info@contact_name@role organization @data_info@data_depositor@affiliation@organization @data_info@data_depositor@affiliation@organization JASRI @data_info@data_depositor@name @data_info@data_depositor@name Hironori Ofuchi @data_info@facility @data_info@facility SPring-8 @data_info@class_name @data_info@class_name BL14B2 @data_info@disk_name @data_info@disk_name XAFS_Standard @data_info@title_ja @data_info@title_ja 標準試料 @data_info@title @data_info@title Standard Sample @facility@ring@end_current @facility@ring@end_current 99.5 @facility@ring@end_current_unit @facility@ring@end_current_unit mA @facility@ring@energy @facility@ring@energy 8.0 @facility@ring@energy_unit @facility@ring@energy_unit GeV @facility@ring@filling_pattern @facility@ring@filling_pattern 2/29-filling + 26 bunches @facility@ring@filling_pattern_mode @facility@ring@filling_pattern_mode E @facility@ring@start_current @facility@ring@start_current 99.5 @facility@ring@start_current_unit @facility@ring@start_current_unit mA @sample_0@chemical_formula @sample_0@chemical_formula NbCl5 @sample_0@lot_number @sample_0@lot_number 4171646 @sample_0@model_number @sample_0@model_number NBH01XB @sample_0@name @sample_0@name Niobium(V) chloride Anhydrous @sample_0@supplier @sample_0@supplier KOJUNDO CHEMICAL LABORATORY @measurement@date@end_time @measurement@date@end_time 2017-04-19 05:53:00 @measurement@date@start_time @measurement@date@start_time 2017-04-19 05:48:00 @measurement@method@absorption_edge @measurement@method@absorption_edge Nb K-edge @measurement@method@category @measurement@method@category spectroscopy @measurement@method@detection @measurement@method@detection Transmission( 2) @measurement@method@sub_category @measurement@method@sub_category XAFS @measurement@scan_mode @measurement@scan_mode angle axis (1) @instrument@monochrometer@distance @instrument@monochrometer@distance 1.63747 @instrument@monochrometer@distance_unit @instrument@monochrometer@distance_unit A @instrument@monochrometer@net_plane @instrument@monochrometer@net_plane Si(311) @instrument@monochrometer@section_0@start_energy @instrument@monochrometer@section_0@start_energy 11.71 @instrument@monochrometer@section_0@start_energy_unit @instrument@monochrometer@section_0@start_energy_unit deg @instrument@monochrometer@section_0@step_energy @instrument@monochrometer@section_0@step_energy -0.00022 @instrument@monochrometer@section_0@step_energy_unit @instrument@monochrometer@section_0@step_energy_unit deg @instrument@monochrometer@section_0@end_energy @instrument@monochrometer@section_0@end_energy 10.635 @instrument@monochrometer@section_0@end_energy_unit @instrument@monochrometer@section_0@end_energy_unit deg @instrument@monochrometer@section_0@dwell_time @instrument@monochrometer@section_0@dwell_time 50.0 @instrument@monochrometer@section_0@dwell_time_unit @instrument@monochrometer@section_0@dwell_time_unit ms @instrument@slit_0@name @instrument@slit_0@name 4Dslit @instrument@slit_0@vertical_size @instrument@slit_0@vertical_size 1.0 @instrument@slit_0@vertical_size_unit @instrument@slit_0@vertical_size_unit mm @instrument@slit_0@horizontal_size @instrument@slit_0@horizontal_size 5.0 @instrument@slit_0@horizontal_size_unit @instrument@slit_0@horizontal_size_unit mm @instrument@xafs@I0@element_0@type @instrument@xafs@I0@element_0@type Ion Chamber @instrument@xafs@I0@element_0@gas @instrument@xafs@I0@element_0@gas N2 50% + Ar 50% @instrument@xafs@I0@element_0@HV @instrument@xafs@I0@element_0@HV 1000.0 @instrument@xafs@I0@element_0@HV_unit @instrument@xafs@I0@element_0@HV_unit V @instrument@xafs@I0@element_0@amp_gain @instrument@xafs@I0@element_0@amp_gain 100000000.0 @instrument@xafs@I0@element_0@amp_gain_unit @instrument@xafs@I0@element_0@amp_gain_unit V/A @instrument@xafs@I0@element_number @instrument@xafs@I0@element_number 1 @instrument@xafs@I1@element_0@type @instrument@xafs@I1@element_0@type Ion Chamber @instrument@xafs@I1@element_0@gas @instrument@xafs@I1@element_0@gas Ar 80% + Kr 20% @instrument@xafs@I1@element_0@HV @instrument@xafs@I1@element_0@HV 1000.0 @instrument@xafs@I1@element_0@HV_unit @instrument@xafs@I1@element_0@HV_unit V @instrument@xafs@I1@element_0@amp_gain @instrument@xafs@I1@element_0@amp_gain 10000000.0 @instrument@xafs@I1@element_0@amp_gain_unit @instrument@xafs@I1@element_0@amp_gain_unit V/A @instrument@xafs@I1@element_number @instrument@xafs@I1@element_number 1 @local@measurement_time @local@measurement_time 241.0 @local@measurement_time_unit @local@measurement_time_unit sec @local@xafs_filename_list_0 @local@xafs_filename_list_0 Nb-K_NbCl5_Si311_50ms_170419.dat @local@xafs_processed_data_format_0@extension @local@xafs_processed_data_format_0@extension ex3 @local@xafs_processed_data_format_0@format @local@xafs_processed_data_format_0@format Rex2000 @local@xafs_processed_data_format_0@columns_0@name @local@xafs_processed_data_format_0@columns_0@name photon energy @local@xafs_processed_data_format_0@columns_0@unit @local@xafs_processed_data_format_0@columns_0@unit eV @local@xafs_processed_data_format_0@columns_0@formula @local@xafs_processed_data_format_0@columns_0@formula 12398/(2*D*math.sin(columns[1])) @local@xafs_processed_data_format_0@columns_0@input@columns @local@xafs_processed_data_format_0@columns_0@input@columns xafs_raw_data_format[0].columns @local@xafs_processed_data_format_0@columns_0@input@D @local@xafs_processed_data_format_0@columns_0@input@D xafs_raw_data_format[0].parameter.D @local@xafs_processed_data_format_0@columns_1@name @local@xafs_processed_data_format_0@columns_1@name absorption coefficient mu*t @local@xafs_processed_data_format_0@columns_1@formula @local@xafs_processed_data_format_0@columns_1@formula math.log(columns[3]/columns[4]) @local@xafs_processed_data_format_0@columns_1@input@columns @local@xafs_processed_data_format_0@columns_1@input@columns xafs_raw_data_format[0].columns @local@xafs_processed_data_format_1@extension @local@xafs_processed_data_format_1@extension txt @local@xafs_processed_data_format_1@format @local@xafs_processed_data_format_1@format Athena 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@local@xafs_processed_data_format_1@columns_1@input@columns xafs_raw_data_format[0].columns @local@xafs_raw_data_format_0@extension @local@xafs_raw_data_format_0@extension dat @local@xafs_raw_data_format_0@format @local@xafs_raw_data_format_0@format PF9809 @local@xafs_raw_data_format_0@parameter@D @local@xafs_raw_data_format_0@parameter@D monochrometer distance @local@xafs_raw_data_format_0@columns_0@name @local@xafs_raw_data_format_0@columns_0@name monochrometer angle (setting value of PC) @local@xafs_raw_data_format_0@columns_0@unit @local@xafs_raw_data_format_0@columns_0@unit deg @local@xafs_raw_data_format_0@columns_1@name @local@xafs_raw_data_format_0@columns_1@name monochrometer angle (encoder value) @local@xafs_raw_data_format_0@columns_1@unit @local@xafs_raw_data_format_0@columns_1@unit deg @local@xafs_raw_data_format_0@columns_2@name @local@xafs_raw_data_format_0@columns_2@name dwell time @local@xafs_raw_data_format_0@columns_2@unit @local@xafs_raw_data_format_0@columns_2@unit sec @local@xafs_raw_data_format_0@columns_3@name @local@xafs_raw_data_format_0@columns_3@name intensity I0 @local@xafs_raw_data_format_0@columns_3@unit @local@xafs_raw_data_format_0@columns_3@unit count @local@xafs_raw_data_format_0@columns_4@name @local@xafs_raw_data_format_0@columns_4@name intensity I1 @local@xafs_raw_data_format_0@columns_4@unit @local@xafs_raw_data_format_0@columns_4@unit count measurement_raw spring8.c5d3ca66-cbcb-45b0-ac49-a9fe1fd70e0d 2014S0000 /SPring-8/BL14B2/XAFS_Standard/Nb/K/311/NbCl5 2020-01-15 19:40:21 2021-03-24 13:53:16 open JASRI Industrial Application and Partnership Division organization JASRI Hironori Ofuchi SPring-8 BL14B2 XAFS_Standard 標準試料 99.5 mA 8.0 GeV 2/29-filling + 26 bunches E 99.5 mA NbCl5 4171646 NBH01XB Niobium(V) chloride Anhydrous KOJUNDO CHEMICAL LABORATORY 2017-04-19 05:53:00 2017-04-19 05:48:00 Nb K-edge spectroscopy Transmission( 2) XAFS angle axis (1) 1.63747 A Si(311)

11.71 deg -0.00022 deg 10.635 deg 50.0 ms

4Dslit 1.0 mm 5.0 mm Ion Chamber N2 50% + Ar 50% 1000.0 V 100000000.0 V/A 1 Ion Chamber Ar 80% + Kr 20% 1000.0 V 10000000.0 V/A 1 241.0 sec Nb-K_NbCl5_Si311_50ms_170419.dat ex3 Rex2000 photon energy eV 12398/(2*D*math.sin(columns[1])) xafs_raw_data_format[0].columns xafs_raw_data_format[0].parameter.D absorption coefficient mu*t math.log(columns[3]/columns[4]) xafs_raw_data_format[0].columns txt Athena photon energy eV 12398/(2*D*math.sin(columns[1])) xafs_raw_data_format[0].columns xafs_raw_data_format[0].parameter.D absorption coefficient mu*t math.log(columns[3]/columns[4]) xafs_raw_data_format[0].columns dat PF9809 monochrometer distance monochrometer angle (setting value of PC) deg monochrometer angle (encoder value) deg dwell time sec intensity I0 count intensity I1 count