data_z00151320901_pl_jp_inc_om100_bkg1 _audit_creation_date 2022-07-14 _audit_creation_method ; Olex2 1.5-ac5-023 (compiled 2022.04.12 svn.rca3783a0 for Rigaku Oxford Diffraction, GUI svn.r6498) ; _shelx_SHELXL_version_number '2018/3' _audit_contact_author_address ? _audit_contact_author_email ? _audit_contact_author_name '' _audit_contact_author_phone ? _publ_contact_author_id_orcid ? _publ_section_references ; Dolomanov, O.V., Bourhis, L.J., Gildea, R.J, Howard, J.A.K. & Puschmann, H. (2009), J. Appl. Cryst. 42, 339-341. Sheldrick, G.M. (2015). Acta Cryst. A71, 3-8. Sheldrick, G.M. (2015). Acta Cryst. C71, 3-8. ; _chemical_name_common ? _chemical_name_systematic ? _chemical_formula_moiety 'Ca4 Li2 O13 Si4' _chemical_formula_sum 'Ca4 Li2 O13 Si4' _chemical_formula_weight 494.56 _chemical_melting_point ? _chemical_oxdiff_formula 'Li2 Ca4 Si4 O13' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Ca' 'Ca' 0.2262 0.3064 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Li' 'Li' -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _space_group_crystal_system 'triclinic' _space_group_IT_number 2 _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 7.1593(4) _cell_length_b 8.2192(4) _cell_length_c 10.4182(6) _cell_angle_alpha 70.737(5) _cell_angle_beta 89.858(4) _cell_angle_gamma 77.719(5) _cell_volume 563.96(6) _cell_formula_units_Z 2 _cell_measurement_reflns_used 7346 _cell_measurement_temperature 301.2(8) _cell_measurement_theta_max 52.1760 _cell_measurement_theta_min 2.6800 _shelx_estimated_absorpt_T_max 0.953 _shelx_estimated_absorpt_T_min 0.909 _exptl_absorpt_coefficient_mu 2.421 _exptl_absorpt_correction_T_max 0.995 _exptl_absorpt_correction_T_min 0.939 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.53a (Rigaku Oxford Diffraction, 2022) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_absorpt_special_details ? _exptl_crystal_colour 'light brown' _exptl_crystal_colour_lustre ? _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 2.912 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_description irregular _exptl_crystal_F_000 492 loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 4 4 13 0.0132 -10 -4 -3 0.0132 1 -3 -15 0.0119 -2 10 2 0.0150 7 -7 -6 0.0158 -5 -9 4 0.0145 2 -10 -2 0.0113 -8 4 7 0.0150 7 7 -6 0.0217 4 -4 9 0.0074 -4 4 -9 0.0112 10 -1 -2 0.0191 -4 -3 11 0.0160 1 10 11 0.0153 -3 -11 -9 0.0149 _exptl_crystal_size_max 0.04 _exptl_crystal_size_mid 0.03 _exptl_crystal_size_min 0.02 loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z 4.0143 4.0532 13.4781 0.2298 0.9642 0.1324 -9.7995 -3.7735 -3.4913 -0.1649 -0.6809 0.7135 1.2353 -2.6395 -14.5277 -0.1808 -0.7655 -0.6175 -1.8086 10.4740 2.0541 -0.9639 0.2306 0.1331 6.6103 -6.6943 -6.1071 0.6810 -0.1649 -0.7135 -4.9318 -9.0246 3.9348 0.7533 -0.1778 0.6332 2.1514 -10.3607 -2.3503 0.9578 -0.2293 -0.1734 -7.8385 4.2342 7.0776 -0.4742 0.1161 0.8727 6.9905 6.5772 -5.8529 -0.5086 0.1187 -0.8528 4.3920 -4.0133 8.5824 0.8234 0.5674 -0.0091 -4.3920 4.0133 -8.5824 -0.8234 -0.5674 0.0091 9.6285 -0.9333 -2.4604 0.3949 0.2687 -0.8785 -4.4247 -3.2782 11.1587 0.4832 0.3361 0.8084 0.8826 10.2376 10.7057 -0.5523 0.8002 0.2337 -3.0622 -10.8147 -9.1524 0.5674 -0.8234 0.0091 _exptl_transmission_factor_max ? _exptl_transmission_factor_min ? _diffrn_reflns_av_R_equivalents 0.0519 _diffrn_reflns_av_unetI/netI 0.0303 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -10 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 18107 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 30.507 _diffrn_reflns_theta_min 2.694 _diffrn_ambient_environment air _diffrn_ambient_temperature 301.2(8) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type 'HyPix-Arc 150' _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w 2.00 31.00 0.10 18.05 -- 0.09 21.00-127.97 290 2 \w 2.00 35.00 0.10 18.05 -- 0.09 21.00 94.63 330 3 \w 2.00 32.00 0.10 18.05 -- 0.09 20.00 161.64 300 4 \w -35.00 -8.00 0.10 18.05 -- 0.09 -21.00-156.25 270 5 \w -34.00 -6.00 0.10 18.05 -- 0.09 -21.00 12.06 280 6 \w 10.00 36.00 0.10 18.05 -- 0.09 23.00 19.80 260 7 \w -2.00 37.00 0.10 18.05 -- 2.00 19.00 -16.00 390 8 \w -23.00 6.00 0.10 18.05 -- 10.00 -19.00 -45.68 290 9 \w 19.00 50.00 0.10 18.05 -- 14.00 22.00 -94.31 310 10 \w -9.00 17.00 0.10 18.05 -- 18.00 -99.00 108.64 260 11 \w -8.00 17.00 0.10 18.05 -- 18.00-101.00 -15.35 250 12 \w -9.00 17.00 0.10 18.05 -- 18.00-100.00 38.30 260 13 \w -8.00 19.00 0.10 18.05 -- 18.00-101.00 -80.50 270 14 \w -9.00 17.00 0.10 18.05 -- 18.00 -99.00 164.21 260 15 \w -8.00 17.00 0.10 18.05 -- 18.00-101.00-144.45 250 16 \w -24.00 2.00 0.10 18.05 -- -30.00 22.00 -82.11 260 17 \w -28.00 -2.00 0.10 18.05 -- -30.00 21.00 103.57 260 18 \w -28.00 1.00 0.10 18.05 -- -30.00 21.00 47.24 290 19 \w -20.00 5.00 0.10 18.05 -- -30.00 23.00 69.62 250 20 \w -25.00 3.00 0.10 18.05 -- -30.00 17.00 24.31 280 21 \w -28.00 3.00 0.10 18.05 -- -30.00 21.00-140.83 310 22 \w -20.00 6.00 0.10 18.05 -- -30.00 23.00-167.29 260 23 \w -20.00 6.00 0.10 18.05 -- -30.00 23.00-127.36 260 24 \w -25.00 0.00 0.10 18.05 -- -30.00 22.00 125.80 250 25 \w -28.00 5.00 0.10 18.05 -- -30.00 21.00 -14.98 330 26 \w -24.00 5.00 0.10 18.05 -- -30.00 22.00 -53.99 290 27 \w -28.00 5.00 0.10 18.05 -- -30.00 21.00 160.68 330 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'ROD, Synergy Custom system, HyPix-Arc 150' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0404547000 _diffrn_orient_matrix_UB_12 -0.0914153000 _diffrn_orient_matrix_UB_13 0.0324918000 _diffrn_orient_matrix_UB_21 0.0432813000 _diffrn_orient_matrix_UB_22 0.0191156000 _diffrn_orient_matrix_UB_23 0.0528982000 _diffrn_orient_matrix_UB_31 -0.0826226000 _diffrn_orient_matrix_UB_32 -0.0088358000 _diffrn_orient_matrix_UB_33 0.0370884000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3039 _reflns_number_total 3412 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _reflns_threshold_expression 'I > 2\s(I)' _computing_cell_refinement 'CrysAlisPro 1.171.42.53a (Rigaku OD, 2022)' _computing_data_collection 'CrysAlisPro 1.171.42.53a (Rigaku OD, 2022)' _computing_data_reduction 'CrysAlisPro 1.171.42.53a (Rigaku OD, 2022)' _computing_molecular_graphics 'Olex2 1.5-ac5-023 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5-ac5-023 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _refine_diff_density_max 1.069 _refine_diff_density_min -0.673 _refine_diff_density_rms 0.158 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.202 _refine_ls_hydrogen_treatment undef _refine_ls_matrix_type full _refine_ls_number_parameters 208 _refine_ls_number_reflns 3412 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0533 _refine_ls_R_factor_gt 0.0450 _refine_ls_restrained_S_all 1.202 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0476P)^2^+1.1556P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1047 _refine_ls_wR_factor_ref 0.1085 _refine_special_details ? _olex2_refinement_description ; ; _atom_sites_solution_hydrogens . _atom_sites_solution_primary dual _atom_sites_solution_secondary ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Ca01 Ca 0.92881(8) 0.29223(8) 0.10560(6) 0.01033(13) Uani 1 1 d . . . . . Ca02 Ca 0.07009(8) 0.69707(8) 0.50534(6) 0.01015(13) Uani 1 1 d . . . . . Ca03 Ca 0.41678(8) 0.30573(8) 0.49700(6) 0.01070(13) Uani 1 1 d . . . . . Ca04 Ca 0.42446(8) 0.28960(8) 0.09733(6) 0.01048(13) Uani 1 1 d . . . . . Si01 Si 0.57438(12) 0.58482(11) 0.22141(8) 0.00860(16) Uani 1 1 d . . . . . Si02 Si 0.13667(12) 0.59303(11) 0.21937(8) 0.00882(16) Uani 1 1 d . . . . . Si03 Si 0.21748(12) 0.11724(11) 0.80437(8) 0.00912(16) Uani 1 1 d . . . . . Si04 Si 0.23332(12) 0.07255(11) 0.32133(8) 0.00987(17) Uani 1 1 d . . . . . Li01 Li 0.2535(13) 0.9079(9) 0.0922(7) 0.0318(16) Uani 1 1 d . . . . . Li02 Li 0.7275(17) 0.0749(10) 0.3856(9) 0.050(3) Uani 1 1 d . . . . . O01 O 0.0141(3) 0.1653(3) 0.3412(2) 0.0147(4) Uani 1 1 d . . . . . O02 O 0.7133(3) 0.1246(3) 0.5676(2) 0.0131(4) Uani 1 1 d . . . . . O03 O 0.4002(3) 0.1765(3) 0.3363(2) 0.0143(4) Uani 1 1 d . . . . . O04 O 0.3660(3) 0.5077(3) 0.6200(2) 0.0111(4) Uani 1 1 d . . . . . O05 O 0.1179(3) 0.5030(3) 0.3777(2) 0.0108(4) Uani 1 1 d . . . . . O06 O 0.1206(3) 0.4900(3) 0.1162(2) 0.0115(4) Uani 1 1 d . . . . . O07 O 0.6354(3) 0.4676(3) 0.1259(2) 0.0128(4) Uani 1 1 d . . . . . O08 O 0.2286(3) 0.0885(3) 0.1600(2) 0.0114(4) Uani 1 1 d . . . . . O09 O 0.0058(3) 0.2080(3) 0.8434(2) 0.0149(4) Uani 1 1 d . . . . . O10 O 0.3628(3) 0.2258(3) 0.8470(2) 0.0159(5) Uani 1 1 d . . . . . O11 O 0.7269(3) 0.0874(3) 0.1011(2) 0.0120(4) Uani 1 1 d . . . . . O12 O 0.2150(3) 0.1490(3) 0.6435(2) 0.0127(4) Uani 1 1 d . . . . . O13 O 0.3410(3) 0.6558(3) 0.1981(2) 0.0131(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ca01 0.0095(3) 0.0077(3) 0.0129(3) -0.0025(2) 0.0001(2) -0.0017(2) Ca02 0.0094(3) 0.0102(3) 0.0121(3) -0.0052(2) 0.0024(2) -0.0028(2) Ca03 0.0096(3) 0.0101(3) 0.0130(3) -0.0046(2) 0.0013(2) -0.0020(2) Ca04 0.0100(3) 0.0080(3) 0.0129(3) -0.0025(2) 0.0018(2) -0.0025(2) Si01 0.0094(4) 0.0070(4) 0.0097(3) -0.0028(3) 0.0011(3) -0.0026(3) Si02 0.0102(4) 0.0070(4) 0.0095(3) -0.0031(3) 0.0012(3) -0.0021(3) Si03 0.0095(4) 0.0068(4) 0.0108(4) -0.0024(3) 0.0013(3) -0.0021(3) Si04 0.0119(4) 0.0068(4) 0.0105(4) -0.0027(3) 0.0011(3) -0.0016(3) Li01 0.061(5) 0.015(3) 0.021(3) -0.008(3) 0.006(3) -0.008(3) Li02 0.098(8) 0.012(3) 0.041(5) -0.015(3) 0.006(5) -0.004(4) O01 0.0178(11) 0.0125(11) 0.0130(10) -0.0051(8) 0.0031(8) -0.0003(8) O02 0.0117(10) 0.0078(10) 0.0169(10) -0.0016(8) 0.0004(8) -0.0005(8) O03 0.0194(11) 0.0123(11) 0.0139(10) -0.0057(8) 0.0018(8) -0.0071(9) O04 0.0118(10) 0.0083(10) 0.0119(9) -0.0023(8) -0.0001(8) -0.0016(8) O05 0.0120(10) 0.0091(10) 0.0110(9) -0.0029(8) 0.0022(8) -0.0022(8) O06 0.0155(10) 0.0108(10) 0.0101(9) -0.0051(8) 0.0021(8) -0.0043(8) O07 0.0123(10) 0.0131(10) 0.0147(10) -0.0080(8) 0.0024(8) -0.0016(8) O08 0.0138(10) 0.0096(10) 0.0113(9) -0.0045(8) 0.0011(8) -0.0025(8) O09 0.0136(10) 0.0100(10) 0.0173(10) -0.0016(8) 0.0033(8) 0.0003(8) O10 0.0167(11) 0.0127(11) 0.0180(11) -0.0021(9) -0.0008(9) -0.0079(9) O11 0.0114(10) 0.0062(9) 0.0169(10) -0.0024(8) 0.0006(8) -0.0012(8) O12 0.0133(10) 0.0108(10) 0.0130(10) -0.0038(8) 0.0012(8) -0.0011(8) O13 0.0102(10) 0.0113(10) 0.0175(10) -0.0045(8) 0.0012(8) -0.0021(8) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Ca01 Ca04 3.5450(8) 1_655 ? Ca01 Si02 3.2069(10) 2_665 ? Ca01 Si04 2.9558(10) 1_655 ? Ca01 Li01 3.438(7) 2_665 ? Ca01 Li02 3.379(10) . ? Ca01 O01 2.352(2) 1_655 ? Ca01 O06 2.369(2) 1_655 ? Ca01 O06 2.382(2) 2_665 ? Ca01 O07 2.334(2) . ? Ca01 O08 2.363(2) 1_655 ? Ca01 O09 3.053(2) 1_654 ? Ca01 O11 2.452(2) . ? Ca02 Ca03 3.4908(8) 2_566 ? Ca02 Si02 3.3668(10) . ? Ca02 Si04 3.4906(10) 1_565 ? Ca02 Si04 3.4716(10) 2_566 ? Ca02 Li02 3.078(10) 2_666 ? Ca02 Li02 3.382(9) 1_465 ? Ca02 O01 2.258(2) 2_566 ? Ca02 O02 2.315(2) 2_666 ? Ca02 O04 2.392(2) . ? Ca02 O05 2.369(2) 2_566 ? Ca02 O05 2.365(2) . ? Ca02 O12 2.407(2) 2_566 ? Ca03 Si01 3.3939(10) . ? Ca03 Si01 3.3445(10) 2_666 ? Ca03 Si02 3.3869(10) . ? Ca03 Si04 3.4850(10) . ? Ca03 Li02 3.089(10) . ? Ca03 Li02 3.346(9) 2_656 ? Ca03 O02 2.281(2) . ? Ca03 O03 2.274(2) . ? Ca03 O04 2.382(2) . ? Ca03 O04 2.455(2) 2_666 ? Ca03 O05 2.441(2) . ? Ca03 O12 2.358(2) . ? Ca04 Si01 3.4489(10) . ? Ca04 Si01 3.1360(10) 2_665 ? Ca04 Si02 3.4604(10) . ? Ca04 Si04 2.9626(10) . ? Ca04 Li02 3.427(10) . ? Ca04 O03 2.373(2) . ? Ca04 O06 2.484(2) . ? Ca04 O07 2.481(2) 2_665 ? Ca04 O07 2.396(2) . ? Ca04 O08 2.322(2) . ? Ca04 O10 2.877(2) 1_554 ? Ca04 O11 2.425(2) . ? Si01 Li01 3.034(8) . ? Si01 O04 1.589(2) 2_666 ? Si01 O07 1.600(2) . ? Si01 O10 1.642(2) 2_666 ? Si01 O13 1.639(2) . ? Si02 Li01 2.794(7) . ? Si02 O05 1.588(2) . ? Si02 O06 1.590(2) . ? Si02 O09 1.653(2) 2_566 ? Si02 O13 1.643(2) . ? Si03 Li01 2.903(7) 1_546 ? Si03 Li02 2.891(8) 2_656 ? Si03 O09 1.654(2) . ? Si03 O10 1.654(2) . ? Si03 O11 1.607(2) 2_656 ? Si03 O12 1.608(2) . ? Si04 Li01 3.098(7) 1_545 ? Si04 Li02 2.879(9) 2_656 ? Si04 O01 1.637(2) . ? Si04 O02 1.616(2) 2_656 ? Si04 O03 1.645(2) . ? Si04 O08 1.642(2) . ? Li01 O08 1.820(7) 1_565 ? Li01 O09 2.264(9) 2_566 ? Li01 O11 2.006(7) 2_665 ? Li01 O13 1.961(7) . ? Li02 O01 2.322(12) 1_655 ? Li02 O02 2.066(9) . ? Li02 O03 2.311(12) . ? Li02 O12 1.922(8) 2_656 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Si02 Ca01 Ca04 93.58(2) 2_665 1_655 ? Si02 Ca01 Li01 49.58(12) 2_665 2_665 ? Si02 Ca01 Li02 138.26(18) 2_665 . ? Si04 Ca01 Ca04 53.29(2) 1_655 1_655 ? Si04 Ca01 Si02 137.80(3) 1_655 2_665 ? Si04 Ca01 Li01 118.05(13) 1_655 2_665 ? Si04 Ca01 Li02 70.64(19) 1_655 . ? Si04 Ca01 O09 110.21(5) 1_655 1_654 ? Li01 Ca01 Ca04 117.41(14) 2_665 1_655 ? Li02 Ca01 Ca04 123.52(19) . 1_655 ? Li02 Ca01 Li01 92.8(2) . 2_665 ? O01 Ca01 Ca04 81.58(6) 1_655 1_655 ? O01 Ca01 Si02 170.17(6) 1_655 2_665 ? O01 Ca01 Si04 33.55(6) 1_655 1_655 ? O01 Ca01 Li01 125.49(13) 1_655 2_665 ? O01 Ca01 Li02 43.4(2) 1_655 . ? O01 Ca01 O06 158.30(8) 1_655 2_665 ? O01 Ca01 O06 83.75(8) 1_655 1_655 ? O01 Ca01 O08 66.48(8) 1_655 1_655 ? O01 Ca01 O09 139.71(7) 1_655 1_654 ? O01 Ca01 O11 94.92(8) 1_655 . ? O06 Ca01 Ca04 88.62(6) 2_665 1_655 ? O06 Ca01 Ca04 44.37(6) 1_655 1_655 ? O06 Ca01 Si02 28.46(5) 2_665 2_665 ? O06 Ca01 Si02 98.83(6) 1_655 2_665 ? O06 Ca01 Si04 141.91(6) 2_665 1_655 ? O06 Ca01 Si04 76.10(6) 1_655 1_655 ? O06 Ca01 Li01 76.20(13) 2_665 2_665 ? O06 Ca01 Li01 146.62(13) 1_655 2_665 ? O06 Ca01 Li02 120.58(17) 1_655 . ? O06 Ca01 Li02 147.0(2) 2_665 . ? O06 Ca01 O06 75.78(8) 1_655 2_665 ? O06 Ca01 O09 107.57(7) 1_655 1_654 ? O06 Ca01 O09 56.12(7) 2_665 1_654 ? O06 Ca01 O11 178.33(8) 1_655 . ? O06 Ca01 O11 105.41(8) 2_665 . ? O07 Ca01 Ca04 141.18(6) . 1_655 ? O07 Ca01 Si02 93.56(6) . 2_665 ? O07 Ca01 Si04 128.55(6) . 1_655 ? O07 Ca01 Li01 95.84(15) . 2_665 ? O07 Ca01 Li02 70.18(18) . . ? O07 Ca01 O01 95.55(8) . 1_655 ? O07 Ca01 O06 80.03(8) . 2_665 ? O07 Ca01 O06 96.82(8) . 1_655 ? O07 Ca01 O08 162.04(8) . 1_655 ? O07 Ca01 O09 120.25(7) . 1_654 ? O07 Ca01 O11 82.29(8) . . ? O08 Ca01 Ca04 40.40(5) 1_655 1_655 ? O08 Ca01 Si02 104.35(6) 1_655 2_665 ? O08 Ca01 Si04 33.68(5) 1_655 1_655 ? O08 Ca01 Li01 94.82(15) 1_655 2_665 ? O08 Ca01 Li02 94.92(18) 1_655 . ? O08 Ca01 O06 116.64(8) 1_655 2_665 ? O08 Ca01 O06 81.92(8) 1_655 1_655 ? O08 Ca01 O09 76.80(7) 1_655 1_654 ? O08 Ca01 O11 98.49(8) 1_655 . ? O09 Ca01 Ca04 80.99(5) 1_654 1_655 ? O09 Ca01 Si02 30.49(5) 1_654 2_665 ? O09 Ca01 Li01 40.29(14) 1_654 2_665 ? O09 Ca01 Li02 129.52(15) 1_654 . ? O11 Ca01 Ca04 136.49(6) . 1_655 ? O11 Ca01 Si02 82.66(6) . 2_665 ? O11 Ca01 Si04 103.33(6) . 1_655 ? O11 Ca01 Li01 35.02(13) . 2_665 ? O11 Ca01 Li02 57.79(17) . . ? O11 Ca01 O09 74.10(7) . 1_654 ? Si02 Ca02 Ca03 94.30(2) . 2_566 ? Si02 Ca02 Si04 146.98(3) . 2_566 ? Si02 Ca02 Si04 84.01(2) . 1_565 ? Si02 Ca02 Li02 100.28(15) . 1_465 ? Si04 Ca02 Ca03 121.60(2) 1_565 2_566 ? Si04 Ca02 Ca03 60.07(2) 2_566 2_566 ? Si04 Ca02 Si04 92.15(2) 2_566 1_565 ? Li02 Ca02 Ca03 58.23(19) 1_465 2_566 ? Li02 Ca02 Ca03 127.6(2) 2_666 2_566 ? Li02 Ca02 Si02 129.15(19) 2_666 . ? Li02 Ca02 Si04 68.0(2) 2_666 2_566 ? Li02 Ca02 Si04 64.70(18) 1_465 1_565 ? Li02 Ca02 Si04 51.52(17) 2_666 1_565 ? Li02 Ca02 Si04 49.66(15) 1_465 2_566 ? Li02 Ca02 Li02 83.3(3) 2_666 1_465 ? O01 Ca02 Ca03 81.51(6) 2_566 2_566 ? O01 Ca02 Si02 165.23(7) 2_566 . ? O01 Ca02 Si04 86.16(6) 2_566 1_565 ? O01 Ca02 Si04 22.64(6) 2_566 2_566 ? O01 Ca02 Li02 48.7(2) 2_566 2_666 ? O01 Ca02 Li02 65.45(16) 2_566 1_465 ? O01 Ca02 O02 87.92(9) 2_566 2_666 ? O01 Ca02 O04 98.37(8) 2_566 . ? O01 Ca02 O05 166.10(9) 2_566 . ? O01 Ca02 O05 86.08(8) 2_566 2_566 ? O01 Ca02 O12 94.11(8) 2_566 2_566 ? O02 Ca02 Ca03 143.74(6) 2_666 2_566 ? O02 Ca02 Si02 87.21(6) 2_666 . ? O02 Ca02 Si04 101.56(6) 2_666 2_566 ? O02 Ca02 Si04 22.49(6) 2_666 1_565 ? O02 Ca02 Li02 42.15(19) 2_666 2_666 ? O02 Ca02 Li02 85.80(19) 2_666 1_465 ? O02 Ca02 O04 77.35(8) 2_666 . ? O02 Ca02 O05 168.72(8) 2_666 2_566 ? O02 Ca02 O05 105.52(8) 2_666 . ? O02 Ca02 O12 104.77(8) 2_666 2_566 ? O04 Ca02 Ca03 138.38(6) . 2_566 ? O04 Ca02 Si02 94.16(6) . . ? O04 Ca02 Si04 118.77(6) . 2_566 ? O04 Ca02 Si04 99.79(6) . 1_565 ? O04 Ca02 Li02 157.23(18) . 1_465 ? O04 Ca02 Li02 73.90(19) . 2_666 ? O04 Ca02 O12 167.43(8) . 2_566 ? O05 Ca02 Ca03 44.29(5) 2_566 2_566 ? O05 Ca02 Ca03 89.36(6) . 2_566 ? O05 Ca02 Si02 25.24(5) . . ? O05 Ca02 Si02 100.87(6) 2_566 . ? O05 Ca02 Si04 75.95(6) 2_566 2_566 ? O05 Ca02 Si04 164.95(6) 2_566 1_565 ? O05 Ca02 Si04 107.60(6) . 1_565 ? O05 Ca02 Si04 149.32(6) . 2_566 ? O05 Ca02 Li02 142.6(2) . 2_666 ? O05 Ca02 Li02 118.16(16) . 1_465 ? O05 Ca02 Li02 128.65(19) 2_566 2_666 ? O05 Ca02 Li02 100.31(19) 2_566 1_465 ? O05 Ca02 O04 81.51(8) . . ? O05 Ca02 O04 94.08(8) 2_566 . ? O05 Ca02 O05 80.08(8) . 2_566 ? O05 Ca02 O12 86.00(8) . 2_566 ? O05 Ca02 O12 85.20(8) 2_566 2_566 ? O12 Ca02 Ca03 42.35(5) 2_566 2_566 ? O12 Ca02 Si02 73.71(6) 2_566 . ? O12 Ca02 Si04 82.53(6) 2_566 1_565 ? O12 Ca02 Si04 73.27(6) 2_566 2_566 ? O12 Ca02 Li02 116.18(19) 2_566 2_666 ? O12 Ca02 Li02 33.75(17) 2_566 1_465 ? Si01 Ca03 Si01 114.27(2) 2_666 . ? Si01 Ca03 Si02 118.63(3) 2_666 . ? Si01 Ca03 Si04 96.26(2) . . ? Si01 Ca03 Si04 147.79(3) 2_666 . ? Si01 Ca03 Li02 101.36(15) 2_666 2_656 ? Si02 Ca03 Si01 54.79(2) . . ? Si02 Ca03 Si04 70.29(2) . . ? Li02 Ca03 Si01 73.26(16) . . ? Li02 Ca03 Si01 144.19(15) 2_656 . ? Li02 Ca03 Si01 130.7(2) . 2_666 ? Li02 Ca03 Si02 111.21(19) 2_656 . ? Li02 Ca03 Si02 105.30(18) . . ? Li02 Ca03 Si04 49.80(16) 2_656 . ? Li02 Ca03 Si04 66.2(2) . . ? Li02 Ca03 Li02 81.1(3) . 2_656 ? O02 Ca03 Si01 89.00(6) . 2_666 ? O02 Ca03 Si01 93.71(6) . . ? O02 Ca03 Si02 143.67(6) . . ? O02 Ca03 Si04 99.48(6) . . ? O02 Ca03 Li02 83.0(2) . 2_656 ? O02 Ca03 Li02 42.0(2) . . ? O02 Ca03 O04 107.74(8) . . ? O02 Ca03 O04 76.70(8) . 2_666 ? O02 Ca03 O05 169.02(8) . . ? O02 Ca03 O12 102.96(8) . . ? O03 Ca03 Si01 167.89(6) . 2_666 ? O03 Ca03 Si01 77.58(6) . . ? O03 Ca03 Si02 69.61(6) . . ? O03 Ca03 Si04 22.82(6) . . ? O03 Ca03 Li02 66.68(16) . 2_656 ? O03 Ca03 Li02 48.2(2) . . ? O03 Ca03 O02 87.67(9) . . ? O03 Ca03 O04 96.03(8) . 2_666 ? O03 Ca03 O04 163.32(9) . . ? O03 Ca03 O05 83.75(8) . . ? O03 Ca03 O12 95.09(8) . . ? O04 Ca03 Si01 25.90(5) . 2_666 ? O04 Ca03 Si01 25.67(5) 2_666 . ? O04 Ca03 Si01 94.52(6) 2_666 2_666 ? O04 Ca03 Si01 94.66(6) . . ? O04 Ca03 Si02 93.82(6) . . ? O04 Ca03 Si02 77.94(5) 2_666 . ? O04 Ca03 Si04 117.65(6) 2_666 . ? O04 Ca03 Si04 149.87(6) . . ? O04 Ca03 Li02 153.97(18) 2_666 2_656 ? O04 Ca03 Li02 72.92(18) 2_666 . ? O04 Ca03 Li02 120.38(16) . 2_656 ? O04 Ca03 Li02 143.9(2) . . ? O04 Ca03 O04 81.79(8) . 2_666 ? O04 Ca03 O05 80.15(8) . . ? O05 Ca03 Si01 100.77(6) . 2_666 ? O05 Ca03 Si01 77.78(5) . . ? O05 Ca03 Si02 25.64(5) . . ? O05 Ca03 Si04 74.89(6) . . ? O05 Ca03 Li02 127.65(19) . . ? O05 Ca03 Li02 99.7(2) . 2_656 ? O05 Ca03 O04 97.36(7) . 2_666 ? O12 Ca03 Si01 161.57(6) . . ? O12 Ca03 Si01 74.33(6) . 2_666 ? O12 Ca03 Si02 106.85(6) . . ? O12 Ca03 Si04 73.49(6) . . ? O12 Ca03 Li02 114.48(18) . . ? O12 Ca03 Li02 34.14(17) . 2_656 ? O12 Ca03 O04 168.84(8) . 2_666 ? O12 Ca03 O04 87.78(8) . . ? O12 Ca03 O05 84.67(8) . . ? Si01 Ca04 Si01 110.38(2) 2_665 . ? Si01 Ca04 Si02 113.89(3) 2_665 . ? Si01 Ca04 Si02 53.69(2) . . ? Si01 Ca04 Li02 141.11(18) 2_665 . ? Si04 Ca04 Si01 140.27(3) . 2_665 ? Si04 Ca04 Si01 105.82(3) . . ? Si04 Ca04 Si02 75.60(3) . . ? Si04 Ca04 Li02 68.30(18) . . ? Li02 Ca04 Si01 68.61(13) . . ? Li02 Ca04 Si02 96.81(15) . . ? O03 Ca04 Si01 75.29(6) . . ? O03 Ca04 Si01 173.92(6) . 2_665 ? O03 Ca04 Si02 67.33(6) . . ? O03 Ca04 Si04 33.67(6) . . ? O03 Ca04 Li02 42.27(19) . . ? O03 Ca04 O06 80.38(8) . . ? O03 Ca04 O07 152.23(8) . 2_665 ? O03 Ca04 O07 91.14(8) . . ? O03 Ca04 O10 143.04(7) . 1_554 ? O03 Ca04 O11 94.63(8) . . ? O06 Ca04 Si01 98.61(5) . 2_665 ? O06 Ca04 Si01 76.34(5) . . ? O06 Ca04 Si02 24.71(5) . . ? O06 Ca04 Si04 74.37(5) . . ? O06 Ca04 Li02 117.68(17) . . ? O06 Ca04 O10 104.31(7) . 1_554 ? O07 Ca04 Si01 94.94(6) . 2_665 ? O07 Ca04 Si01 86.04(6) 2_665 . ? O07 Ca04 Si01 30.34(5) 2_665 2_665 ? O07 Ca04 Si01 24.19(5) . . ? O07 Ca04 Si02 76.48(6) . . ? O07 Ca04 Si02 85.09(5) 2_665 . ? O07 Ca04 Si04 124.51(6) . . ? O07 Ca04 Si04 143.51(6) 2_665 . ? O07 Ca04 Li02 145.89(18) 2_665 . ? O07 Ca04 Li02 68.67(17) . . ? O07 Ca04 O06 96.84(8) . . ? O07 Ca04 O06 75.28(7) 2_665 . ? O07 Ca04 O07 78.84(8) . 2_665 ? O07 Ca04 O10 123.82(7) . 1_554 ? O07 Ca04 O10 58.21(7) 2_665 1_554 ? O07 Ca04 O11 81.60(8) . . ? O08 Ca04 Si01 107.18(6) . 2_665 ? O08 Ca04 Si01 138.06(6) . . ? O08 Ca04 Si02 94.18(6) . . ? O08 Ca04 Si04 33.51(5) . . ? O08 Ca04 Li02 93.07(18) . . ? O08 Ca04 O03 66.75(8) . . ? O08 Ca04 O06 80.29(8) . . ? O08 Ca04 O07 157.88(8) . . ? O08 Ca04 O07 120.84(8) . 2_665 ? O08 Ca04 O10 77.80(7) . 1_554 ? O08 Ca04 O11 99.26(8) . . ? O10 Ca04 Si01 31.32(5) 1_554 2_665 ? O10 Ca04 Si01 141.67(5) 1_554 . ? O10 Ca04 Si02 127.58(5) 1_554 . ? O10 Ca04 Si04 111.25(5) 1_554 . ? O10 Ca04 Li02 134.89(15) 1_554 . ? O11 Ca04 Si01 86.52(6) . 2_665 ? O11 Ca04 Si01 100.96(6) . . ? O11 Ca04 Si02 150.99(6) . . ? O11 Ca04 Si04 102.35(6) . . ? O11 Ca04 Li02 57.09(17) . . ? O11 Ca04 O06 174.77(8) . . ? O11 Ca04 O07 109.18(8) . 2_665 ? O11 Ca04 O10 80.62(7) . 1_554 ? Ca01 Si01 Ca02 68.82(2) . 2_666 ? Ca03 Si01 Ca01 103.31(3) . . ? Ca03 Si01 Ca01 130.07(3) 2_666 . ? Ca03 Si01 Ca02 62.98(2) 2_666 2_666 ? Ca03 Si01 Ca02 62.95(2) . 2_666 ? Ca03 Si01 Ca03 65.73(2) 2_666 . ? Ca03 Si01 Ca04 141.45(3) 2_666 . ? Ca03 Si01 Ca04 75.92(2) . . ? Ca04 Si01 Ca01 61.667(19) . . ? Ca04 Si01 Ca01 67.63(2) 2_665 . ? Ca04 Si01 Ca02 133.23(3) 2_665 2_666 ? Ca04 Si01 Ca02 103.33(3) . 2_666 ? Ca04 Si01 Ca03 146.88(3) 2_665 2_666 ? Ca04 Si01 Ca03 144.49(3) 2_665 . ? Ca04 Si01 Ca04 69.62(2) 2_665 . ? Li01 Si01 Ca01 136.84(13) . . ? Li01 Si01 Ca02 152.67(13) . 2_666 ? Li01 Si01 Ca03 109.05(14) . . ? Li01 Si01 Ca03 89.75(13) . 2_666 ? Li01 Si01 Ca04 99.36(14) . . ? Li01 Si01 Ca04 69.42(13) . 2_665 ? O04 Si01 Ca01 97.11(9) 2_666 . ? O04 Si01 Ca02 30.42(8) 2_666 2_666 ? O04 Si01 Ca03 40.90(8) 2_666 2_666 ? O04 Si01 Ca03 42.00(8) 2_666 . ? O04 Si01 Ca04 163.65(9) 2_666 2_665 ? O04 Si01 Ca04 109.15(9) 2_666 . ? O04 Si01 Li01 126.05(15) 2_666 . ? O04 Si01 O07 117.06(13) 2_666 . ? O04 Si01 O10 114.28(12) 2_666 2_666 ? O04 Si01 O13 109.35(12) 2_666 . ? O07 Si01 Ca01 28.87(8) . . ? O07 Si01 Ca02 93.68(9) . 2_666 ? O07 Si01 Ca03 103.58(9) . . ? O07 Si01 Ca03 156.61(9) . 2_666 ? O07 Si01 Ca04 51.55(9) . 2_665 ? O07 Si01 Ca04 37.85(8) . . ? O07 Si01 Li01 113.62(16) . . ? O07 Si01 O10 108.35(13) . 2_666 ? O07 Si01 O13 106.96(12) . . ? O10 Si01 Ca01 101.62(9) 2_666 . ? O10 Si01 Ca02 108.27(9) 2_666 2_666 ? O10 Si01 Ca03 147.46(10) 2_666 . ? O10 Si01 Ca03 82.24(9) 2_666 2_666 ? O10 Si01 Ca04 65.59(9) 2_666 2_665 ? O10 Si01 Ca04 135.18(9) 2_666 . ? O10 Si01 Li01 63.27(17) 2_666 . ? O13 Si01 Ca01 135.58(9) . . ? O13 Si01 Ca02 138.35(9) . 2_666 ? O13 Si01 Ca03 91.30(9) . 2_666 ? O13 Si01 Ca03 77.01(8) . . ? O13 Si01 Ca04 86.42(9) . 2_665 ? O13 Si01 Ca04 75.95(9) . . ? O13 Si01 Li01 36.01(17) . . ? O13 Si01 O10 99.12(12) . 2_666 ? Ca01 Si02 Ca01 66.07(2) 2_665 1_455 ? Ca01 Si02 Ca02 132.01(3) 2_665 2_566 ? Ca01 Si02 Ca02 149.11(3) 2_665 . ? Ca01 Si02 Ca03 144.16(3) 2_665 . ? Ca01 Si02 Ca04 68.75(2) 2_665 . ? Ca02 Si02 Ca01 68.51(2) 2_566 1_455 ? Ca02 Si02 Ca01 129.13(3) . 1_455 ? Ca02 Si02 Ca02 62.42(2) . 2_566 ? Ca02 Si02 Ca03 65.37(2) . . ? Ca02 Si02 Ca04 141.11(3) . . ? Ca03 Si02 Ca01 100.92(3) . 1_455 ? Ca03 Si02 Ca02 59.700(19) . 2_566 ? Ca03 Si02 Ca04 75.86(2) . . ? Ca04 Si02 Ca01 59.853(19) . 1_455 ? Ca04 Si02 Ca02 100.83(2) . 2_566 ? Li01 Si02 Ca01 69.51(15) . 2_665 ? Li01 Si02 Ca01 135.58(15) . 1_455 ? Li01 Si02 Ca02 152.34(14) . 2_566 ? Li01 Si02 Ca02 90.40(14) . . ? Li01 Si02 Ca03 115.55(17) . . ? Li01 Si02 Ca04 104.13(16) . . ? O05 Si02 Ca01 96.78(9) . 1_455 ? O05 Si02 Ca01 161.63(9) . 2_665 ? O05 Si02 Ca02 39.41(8) . . ? O05 Si02 Ca02 29.63(8) . 2_566 ? O05 Si02 Ca03 41.69(8) . . ? O05 Si02 Ca04 109.33(9) . . ? O05 Si02 Li01 127.21(16) . . ? O05 Si02 O06 120.64(12) . . ? O05 Si02 O09 112.22(12) . 2_566 ? O05 Si02 O13 108.97(12) . . ? O06 Si02 Ca01 28.60(8) . 1_455 ? O06 Si02 Ca01 45.58(8) . 2_665 ? O06 Si02 Ca02 95.20(8) . 2_566 ? O06 Si02 Ca02 157.38(9) . . ? O06 Si02 Ca03 107.51(9) . . ? O06 Si02 Ca04 40.79(8) . . ? O06 Si02 Li01 111.48(16) . . ? O06 Si02 O09 108.08(12) . 2_566 ? O06 Si02 O13 107.10(12) . . ? O09 Si02 Ca01 69.61(9) 2_566 2_665 ? O09 Si02 Ca01 107.75(9) 2_566 1_455 ? O09 Si02 Ca02 79.63(9) 2_566 . ? O09 Si02 Ca02 111.68(9) 2_566 2_566 ? O09 Si02 Ca03 144.02(9) 2_566 . ? O09 Si02 Ca04 137.84(9) 2_566 . ? O09 Si02 Li01 54.13(19) 2_566 . ? O13 Si02 Ca01 88.52(9) . 2_665 ? O13 Si02 Ca01 133.93(9) . 1_455 ? O13 Si02 Ca02 135.85(9) . 2_566 ? O13 Si02 Ca02 92.56(9) . . ? O13 Si02 Ca03 77.19(8) . . ? O13 Si02 Ca04 75.54(9) . . ? O13 Si02 Li01 43.5(2) . . ? O13 Si02 O09 97.16(12) . 2_566 ? Ca01 Si03 Ca04 60.693(19) 2_656 2_656 ? Ca02 Si03 Ca01 93.72(2) 2_566 2_656 ? Ca02 Si03 Ca04 125.42(3) 2_566 2_656 ? Ca03 Si03 Ca01 124.16(3) . 2_656 ? Ca03 Si03 Ca02 59.479(19) . 2_566 ? Ca03 Si03 Ca04 94.24(2) . 2_656 ? Li01 Si03 Ca01 63.23(15) 1_546 2_656 ? Li01 Si03 Ca02 147.91(17) 1_546 2_566 ? Li01 Si03 Ca03 151.70(18) 1_546 . ? Li01 Si03 Ca04 64.48(15) 1_546 2_656 ? Li02 Si03 Ca01 62.06(19) 2_656 2_656 ? Li02 Si03 Ca02 62.7(2) 2_656 2_566 ? Li02 Si03 Ca03 62.10(19) 2_656 . ? Li02 Si03 Ca04 62.7(2) 2_656 2_656 ? Li02 Si03 Li01 116.8(2) 2_656 1_546 ? O09 Si03 Ca01 88.51(9) . 2_656 ? O09 Si03 Ca02 74.59(9) . 2_566 ? O09 Si03 Ca03 122.84(9) . . ? O09 Si03 Ca04 141.90(9) . 2_656 ? O09 Si03 Li01 82.38(19) . 1_546 ? O09 Si03 Li02 124.4(3) . 2_656 ? O09 Si03 O10 103.22(13) . . ? O10 Si03 Ca01 145.09(9) . 2_656 ? O10 Si03 Ca02 121.01(9) . 2_566 ? O10 Si03 Ca03 76.70(9) . . ? O10 Si03 Ca04 92.88(9) . 2_656 ? O10 Si03 Li01 85.56(18) . 1_546 ? O10 Si03 Li02 128.4(3) . 2_656 ? O11 Si03 Ca01 35.88(8) 2_656 2_656 ? O11 Si03 Ca02 127.15(9) 2_656 2_566 ? O11 Si03 Ca03 125.67(9) 2_656 . ? O11 Si03 Ca04 33.65(8) 2_656 2_656 ? O11 Si03 Li01 41.52(16) 2_656 1_546 ? O11 Si03 Li02 75.37(19) 2_656 2_656 ? O11 Si03 O09 108.38(12) 2_656 . ? O11 Si03 O10 109.79(12) 2_656 . ? O11 Si03 O12 114.10(12) 2_656 . ? O12 Si03 Ca01 95.32(9) . 2_656 ? O12 Si03 Ca02 35.61(8) . 2_566 ? O12 Si03 Ca03 34.03(8) . . ? O12 Si03 Ca04 95.50(9) . 2_656 ? O12 Si03 Li01 155.53(16) . 1_546 ? O12 Si03 Li02 38.75(19) . 2_656 ? O12 Si03 O09 110.19(12) . . ? O12 Si03 O10 110.58(12) . . ? Ca01 Si04 Ca02 106.47(3) 1_455 1_545 ? Ca01 Si04 Ca02 78.43(3) 1_455 2_566 ? Ca01 Si04 Ca03 156.36(3) 1_455 2_656 ? Ca01 Si04 Ca03 114.36(3) 1_455 . ? Ca01 Si04 Ca04 73.59(3) 1_455 . ? Ca01 Si04 Li01 71.65(15) 1_455 1_545 ? Ca02 Si04 Ca02 87.85(2) 2_566 1_545 ? Ca02 Si04 Ca03 60.24(2) 2_566 . ? Ca02 Si04 Ca03 120.19(3) 2_566 2_656 ? Ca02 Si04 Ca03 63.17(2) 1_545 2_656 ? Ca03 Si04 Ca02 119.17(3) . 1_545 ? Ca03 Si04 Ca03 88.67(2) . 2_656 ? Ca04 Si04 Ca02 115.69(3) . 2_566 ? Ca04 Si04 Ca02 155.40(3) . 1_545 ? Ca04 Si04 Ca03 106.69(3) . 2_656 ? Ca04 Si04 Ca03 81.07(3) . . ? Ca04 Si04 Li01 73.26(14) . 1_545 ? Li01 Si04 Ca02 144.79(17) 1_545 2_566 ? Li01 Si04 Ca02 83.34(13) 1_545 1_545 ? Li01 Si04 Ca03 150.81(16) 1_545 . ? Li01 Si04 Ca03 85.66(15) 1_545 2_656 ? Li02 Si04 Ca01 137.7(2) 2_656 1_455 ? Li02 Si04 Ca02 63.55(19) 2_656 2_566 ? Li02 Si04 Ca02 56.82(19) 2_656 1_545 ? Li02 Si04 Ca03 56.73(19) 2_656 2_656 ? Li02 Si04 Ca03 62.58(18) 2_656 . ? Li02 Si04 Ca04 138.7(2) 2_656 . ? Li02 Si04 Li01 133.5(2) 2_656 1_545 ? O01 Si04 Ca01 52.54(8) . 1_455 ? O01 Si04 Ca02 80.10(9) . 1_545 ? O01 Si04 Ca02 32.07(8) . 2_566 ? O01 Si04 Ca03 90.66(9) . . ? O01 Si04 Ca03 137.00(9) . 2_656 ? O01 Si04 Ca04 115.65(9) . . ? O01 Si04 Li01 112.72(19) . 1_545 ? O01 Si04 Li02 85.3(2) . 2_656 ? O01 Si04 O03 116.13(13) . . ? O01 Si04 O08 104.00(12) . . ? O02 Si04 Ca01 138.52(9) 2_656 1_455 ? O02 Si04 Ca02 33.22(8) 2_656 1_545 ? O02 Si04 Ca02 101.88(9) 2_656 2_566 ? O02 Si04 Ca03 100.48(9) 2_656 . ? O02 Si04 Ca03 30.78(8) 2_656 2_656 ? O02 Si04 Ca04 136.33(9) 2_656 . ? O02 Si04 Li01 89.03(15) 2_656 1_545 ? O02 Si04 Li02 44.53(17) 2_656 2_656 ? O02 Si04 O01 107.99(12) 2_656 . ? O02 Si04 O03 108.50(12) 2_656 . ? O02 Si04 O08 116.90(12) 2_656 . ? O03 Si04 Ca01 112.98(9) . 1_455 ? O03 Si04 Ca02 89.98(9) . 2_566 ? O03 Si04 Ca02 139.17(9) . 1_545 ? O03 Si04 Ca03 32.42(8) . . ? O03 Si04 Ca03 83.28(9) . 2_656 ? O03 Si04 Ca04 53.11(8) . . ? O03 Si04 Li01 118.40(18) . 1_545 ? O03 Si04 Li02 86.0(2) . 2_656 ? O08 Si04 Ca01 52.93(8) . 1_455 ? O08 Si04 Ca02 131.14(9) . 2_566 ? O08 Si04 Ca02 108.30(8) . 1_545 ? O08 Si04 Ca03 132.08(9) . . ? O08 Si04 Ca03 108.03(9) . 2_656 ? O08 Si04 Ca04 51.32(8) . . ? O08 Si04 Li01 28.03(15) . 1_545 ? O08 Si04 Li02 161.43(18) . 2_656 ? O08 Si04 O03 103.60(12) . . ? Ca01 Li01 Ca01 112.8(2) 2_665 1_465 ? Ca01 Li01 Ca04 59.32(11) 1_465 1_565 ? Ca01 Li01 Ca04 146.2(2) 2_665 1_565 ? Ca01 Li01 Ca04 62.69(12) 2_665 2_665 ? Ca04 Li01 Ca01 147.7(2) 2_665 1_465 ? Ca04 Li01 Ca04 105.2(2) 2_665 1_565 ? Si01 Li01 Ca01 151.0(2) . 1_465 ? Si01 Li01 Ca01 92.27(18) . 2_665 ? Si01 Li01 Ca04 107.2(2) . 1_565 ? Si01 Li01 Ca04 56.66(13) . 2_665 ? Si01 Li01 Si04 98.8(2) . 1_565 ? Si02 Li01 Ca01 114.3(3) . 1_465 ? Si02 Li01 Ca01 60.91(14) . 2_665 ? Si02 Li01 Ca04 152.6(2) . 1_565 ? Si02 Li01 Ca04 91.96(18) . 2_665 ? Si02 Li01 Si01 64.59(15) . . ? Si02 Li01 Si03 128.6(3) . 1_564 ? Si02 Li01 Si04 102.2(2) . 1_565 ? Si03 Li01 Ca01 81.26(17) 1_564 1_465 ? Si03 Li01 Ca01 67.83(15) 1_564 2_665 ? Si03 Li01 Ca04 78.38(16) 1_564 1_565 ? Si03 Li01 Ca04 67.32(14) 1_564 2_665 ? Si03 Li01 Si01 123.3(3) 1_564 . ? Si03 Li01 Si04 123.0(2) 1_564 1_565 ? Si04 Li01 Ca01 153.2(3) 1_565 2_665 ? Si04 Li01 Ca01 52.31(11) 1_565 1_465 ? Si04 Li01 Ca04 51.65(11) 1_565 1_565 ? Si04 Li01 Ca04 142.8(3) 1_565 2_665 ? O08 Li01 Ca01 37.06(19) 1_565 1_465 ? O08 Li01 Ca01 149.8(4) 1_565 2_665 ? O08 Li01 Ca04 138.2(4) 1_565 2_665 ? O08 Li01 Ca04 33.30(17) 1_565 1_565 ? O08 Li01 Si01 117.3(4) 1_565 . ? O08 Li01 Si02 124.5(3) 1_565 . ? O08 Li01 Si03 97.9(3) 1_565 1_564 ? O08 Li01 Si04 25.09(13) 1_565 1_565 ? O08 Li01 O09 104.8(4) 1_565 2_566 ? O08 Li01 O11 129.5(4) 1_565 2_665 ? O08 Li01 O13 125.5(4) 1_565 . ? O09 Li01 Ca01 60.69(18) 2_566 2_665 ? O09 Li01 Ca01 80.9(2) 2_566 1_465 ? O09 Li01 Ca04 137.4(3) 2_566 1_565 ? O09 Li01 Ca04 117.0(3) 2_566 2_665 ? O09 Li01 Si01 100.6(2) 2_566 . ? O09 Li01 Si02 36.27(12) 2_566 . ? O09 Li01 Si03 112.0(3) 2_566 1_564 ? O09 Li01 Si04 93.1(2) 2_566 1_565 ? O11 Li01 Ca01 44.54(17) 2_665 2_665 ? O11 Li01 Ca01 110.5(3) 2_665 1_465 ? O11 Li01 Ca04 41.90(17) 2_665 2_665 ? O11 Li01 Ca04 104.4(3) 2_665 1_565 ? O11 Li01 Si01 97.4(3) 2_665 . ? O11 Li01 Si02 102.7(3) 2_665 . ? O11 Li01 Si03 32.07(12) 2_665 1_564 ? O11 Li01 Si04 154.3(3) 2_665 1_565 ? O11 Li01 O09 103.2(3) 2_665 2_566 ? O13 Li01 Ca01 77.4(2) . 2_665 ? O13 Li01 Ca01 140.4(3) . 1_465 ? O13 Li01 Ca04 131.3(3) . 1_565 ? O13 Li01 Ca04 71.8(2) . 2_665 ? O13 Li01 Si01 29.42(15) . . ? O13 Li01 Si02 35.22(14) . . ? O13 Li01 Si03 134.9(3) . 1_564 ? O13 Li01 Si04 100.9(3) . 1_565 ? O13 Li01 O09 71.2(2) . 2_566 ? O13 Li01 O11 103.0(3) . 2_665 ? Ca01 Li02 Ca02 99.9(3) . 1_645 ? Ca01 Li02 Ca04 64.20(16) . . ? Ca02 Li02 Ca01 78.3(2) 2_666 . ? Ca02 Li02 Ca02 96.7(3) 2_666 1_645 ? Ca02 Li02 Ca03 138.9(3) 2_666 2_656 ? Ca02 Li02 Ca03 73.02(17) 2_666 . ? Ca02 Li02 Ca04 117.0(2) 2_666 . ? Ca02 Li02 Ca04 136.6(3) 1_645 . ? Ca03 Li02 Ca01 136.9(3) 2_656 . ? Ca03 Li02 Ca01 116.1(2) . . ? Ca03 Li02 Ca02 62.52(14) 2_656 1_645 ? Ca03 Li02 Ca02 138.7(3) . 1_645 ? Ca03 Li02 Ca03 98.9(3) . 2_656 ? Ca03 Li02 Ca04 100.5(3) 2_656 . ? Ca03 Li02 Ca04 80.3(2) . . ? Si03 Li02 Ca01 68.8(2) 2_656 . ? Si03 Li02 Ca02 139.7(4) 2_656 2_666 ? Si03 Li02 Ca02 67.86(17) 2_656 1_645 ? Si03 Li02 Ca03 142.6(4) 2_656 . ? Si03 Li02 Ca03 68.09(17) 2_656 2_656 ? Si03 Li02 Ca04 68.7(2) 2_656 . ? Si04 Li02 Ca01 144.9(4) 2_656 . ? Si04 Li02 Ca02 71.7(2) 2_656 2_666 ? Si04 Li02 Ca02 66.80(19) 2_656 1_645 ? Si04 Li02 Ca03 72.1(2) 2_656 . ? Si04 Li02 Ca03 67.62(18) 2_656 2_656 ? Si04 Li02 Ca04 147.2(4) 2_656 . ? Si04 Li02 Si03 127.0(3) 2_656 2_656 ? O01 Li02 Ca01 44.06(18) 1_655 . ? O01 Li02 Ca02 46.91(19) 1_655 2_666 ? O01 Li02 Ca02 75.5(3) 1_655 1_645 ? O01 Li02 Ca03 116.6(3) 1_655 . ? O01 Li02 Ca03 137.8(4) 1_655 2_656 ? O01 Li02 Ca04 107.1(3) 1_655 . ? O01 Li02 Si03 92.8(3) 1_655 2_656 ? O01 Li02 Si04 101.0(4) 1_655 2_656 ? O02 Li02 Ca01 126.3(4) . . ? O02 Li02 Ca02 95.2(3) . 1_645 ? O02 Li02 Ca02 48.8(2) . 2_666 ? O02 Li02 Ca03 47.6(2) . . ? O02 Li02 Ca03 95.6(3) . 2_656 ? O02 Li02 Ca04 127.3(4) . . ? O02 Li02 Si03 160.3(4) . 2_656 ? O02 Li02 Si04 33.27(15) . 2_656 ? O02 Li02 O01 92.5(4) . 1_655 ? O02 Li02 O03 92.1(4) . . ? O03 Li02 Ca01 105.7(3) . . ? O03 Li02 Ca02 115.9(3) . 2_666 ? O03 Li02 Ca02 141.8(4) . 1_645 ? O03 Li02 Ca03 79.5(3) . 2_656 ? O03 Li02 Ca03 47.16(19) . . ? O03 Li02 Ca04 43.69(18) . . ? O03 Li02 Si03 95.5(3) . 2_656 ? O03 Li02 Si04 103.5(4) . 2_656 ? O03 Li02 O01 141.6(4) . 1_655 ? O12 Li02 Ca01 95.5(3) 2_656 . ? O12 Li02 Ca02 139.2(5) 2_656 2_666 ? O12 Li02 Ca02 44.1(2) 2_656 1_645 ? O12 Li02 Ca03 43.5(2) 2_656 2_656 ? O12 Li02 Ca03 141.0(5) 2_656 . ? O12 Li02 Ca04 95.1(4) 2_656 . ? O12 Li02 Si03 31.58(16) 2_656 2_656 ? O12 Li02 Si04 95.5(3) 2_656 2_656 ? O12 Li02 O01 101.8(5) 2_656 1_655 ? O12 Li02 O02 128.7(5) 2_656 . ? O12 Li02 O03 104.7(5) 2_656 . ? Ca02 O01 Ca01 124.67(10) 2_566 1_455 ? Ca02 O01 Li02 84.4(2) 2_566 1_455 ? Si04 O01 Ca01 93.91(10) . 1_455 ? Si04 O01 Ca02 125.28(13) . 2_566 ? Si04 O01 Li02 135.9(2) . 1_455 ? Li02 O01 Ca01 92.6(2) 1_455 1_455 ? Ca03 O02 Ca02 105.93(9) . 2_666 ? Si04 O02 Ca02 124.29(12) 2_656 2_666 ? Si04 O02 Ca03 127.96(12) 2_656 . ? Si04 O02 Li02 102.2(3) 2_656 . ? Li02 O02 Ca02 89.1(3) . 2_666 ? Li02 O02 Ca03 90.4(3) . . ? Ca03 O03 Ca04 129.83(10) . . ? Ca03 O03 Li02 84.7(2) . . ? Si04 O03 Ca03 124.76(13) . . ? Si04 O03 Ca04 93.22(10) . . ? Si04 O03 Li02 130.8(2) . . ? Li02 O03 Ca04 94.0(2) . . ? Ca02 O04 Ca03 98.39(8) . 2_666 ? Ca03 O04 Ca02 99.62(8) . . ? Ca03 O04 Ca03 98.21(8) . 2_666 ? Si01 O04 Ca02 129.92(12) 2_666 . ? Si01 O04 Ca03 112.33(11) 2_666 2_666 ? Si01 O04 Ca03 113.20(11) 2_666 . ? Ca02 O05 Ca02 99.92(8) . 2_566 ? Ca02 O05 Ca03 93.05(8) 2_566 . ? Ca02 O05 Ca03 98.70(8) . . ? Si02 O05 Ca02 131.00(12) . 2_566 ? Si02 O05 Ca02 115.35(12) . . ? Si02 O05 Ca03 112.67(11) . . ? Ca01 O06 Ca01 104.22(8) 1_455 2_665 ? Ca01 O06 Ca04 93.82(8) 1_455 . ? Ca01 O06 Ca04 101.53(8) 2_665 . ? Si02 O06 Ca01 105.96(11) . 2_665 ? Si02 O06 Ca01 132.66(12) . 1_455 ? Si02 O06 Ca04 114.50(12) . . ? Ca01 O07 Ca04 103.04(8) . 2_665 ? Ca01 O07 Ca04 99.76(9) . . ? Ca04 O07 Ca04 101.16(8) . 2_665 ? Si01 O07 Ca01 131.79(13) . . ? Si01 O07 Ca04 117.96(12) . . ? Si01 O07 Ca04 98.11(11) . 2_665 ? Ca04 O08 Ca01 98.34(8) . 1_455 ? Si04 O08 Ca01 93.38(10) . 1_455 ? Si04 O08 Ca04 95.17(10) . . ? Si04 O08 Li01 126.9(3) . 1_545 ? Li01 O08 Ca01 115.3(3) 1_545 1_455 ? Li01 O08 Ca04 121.2(3) 1_545 . ? Si02 O09 Ca01 79.90(9) 2_566 1_456 ? Si02 O09 Si03 133.18(15) 2_566 . ? Si02 O09 Li01 89.6(2) 2_566 2_566 ? Si03 O09 Ca01 125.13(12) . 1_456 ? Si03 O09 Li01 130.3(2) . 2_566 ? Li01 O09 Ca01 79.03(18) 2_566 1_456 ? Si01 O10 Ca04 83.09(10) 2_666 1_556 ? Si01 O10 Si03 137.01(16) 2_666 . ? Si03 O10 Ca04 131.24(12) . 1_556 ? Ca04 O11 Ca01 95.75(8) . . ? Si03 O11 Ca01 121.53(12) 2_656 . ? Si03 O11 Ca04 124.80(12) 2_656 . ? Si03 O11 Li01 106.4(2) 2_656 2_665 ? Li01 O11 Ca01 100.4(2) 2_665 . ? Li01 O11 Ca04 104.6(3) 2_665 . ? Ca03 O12 Ca02 94.20(8) . 2_566 ? Si03 O12 Ca02 121.51(12) . 2_566 ? Si03 O12 Ca03 123.53(12) . . ? Si03 O12 Li02 109.7(3) . 2_656 ? Li02 O12 Ca02 102.1(3) 2_656 2_566 ? Li02 O12 Ca03 102.4(3) 2_656 . ? Si01 O13 Si02 143.90(16) . . ? Si01 O13 Li01 114.6(3) . . ? Si02 O13 Li01 101.3(3) . . ? _shelx_res_file ; TITL z00151320901_pl_jp_inc_om100_bkg1_a.res in P-1 z00151320901_pl_jp_inc_om100_bkg1.res created by SHELXL-2018/3 at 13:44:21 on 14-Jul-2022 REM Old TITL REM SHELXT solution in P-1: R1 0.073, Rweak 0.005, Alpha 0.046 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: O13 Si4 Ca4 CELL 0.71073 7.1593 8.2192 10.4182 70.737 89.858 77.719 ZERR 2 0.0004 0.0004 0.0006 0.005 0.004 0.005 LATT 1 SFAC Ca Li O Si UNIT 8 4 26 8 L.S. 50 PLAN 5 SIZE 0.02 0.03 0.04 TEMP 28 fmap 2 acta REM REM REM WGHT 0.047600 1.155600 FVAR 0.45748 CA01 1 0.928807 0.292231 0.105595 11.00000 0.00947 0.00773 = 0.01293 -0.00246 0.00005 -0.00170 CA02 1 0.070094 0.697072 0.505338 11.00000 0.00940 0.01023 = 0.01214 -0.00518 0.00238 -0.00275 CA03 1 0.416779 0.305729 0.497005 11.00000 0.00956 0.01006 = 0.01296 -0.00465 0.00131 -0.00198 CA04 1 0.424465 0.289596 0.097332 11.00000 0.00995 0.00796 = 0.01293 -0.00245 0.00184 -0.00250 SI01 4 0.574383 0.584816 0.221409 11.00000 0.00944 0.00697 = 0.00974 -0.00279 0.00110 -0.00261 SI02 4 0.136674 0.593025 0.219371 11.00000 0.01022 0.00700 = 0.00953 -0.00305 0.00125 -0.00212 SI03 4 0.217476 0.117242 0.804374 11.00000 0.00948 0.00681 = 0.01080 -0.00243 0.00132 -0.00213 SI04 4 0.233325 0.072547 0.321331 11.00000 0.01191 0.00675 = 0.01051 -0.00267 0.00110 -0.00157 LI01 2 0.253507 0.907892 0.092178 11.00000 0.06083 0.01525 = 0.02087 -0.00835 0.00649 -0.00828 LI02 2 0.727454 0.074896 0.385597 11.00000 0.09816 0.01248 = 0.04105 -0.01460 0.00583 -0.00428 O01 3 0.014073 0.165273 0.341159 11.00000 0.01780 0.01254 = 0.01300 -0.00512 0.00311 -0.00030 O02 3 0.713266 0.124585 0.567646 11.00000 0.01169 0.00784 = 0.01694 -0.00158 0.00035 -0.00053 O03 3 0.400243 0.176526 0.336300 11.00000 0.01944 0.01235 = 0.01389 -0.00569 0.00180 -0.00714 O04 3 0.366009 0.507729 0.620015 11.00000 0.01180 0.00833 = 0.01192 -0.00229 -0.00008 -0.00158 O05 3 0.117892 0.502977 0.377712 11.00000 0.01197 0.00915 = 0.01095 -0.00291 0.00219 -0.00222 O06 3 0.120604 0.490018 0.116238 11.00000 0.01548 0.01080 = 0.01005 -0.00511 0.00208 -0.00426 O07 3 0.635439 0.467605 0.125937 11.00000 0.01235 0.01307 = 0.01475 -0.00795 0.00240 -0.00158 O08 3 0.228603 0.088524 0.159976 11.00000 0.01382 0.00964 = 0.01125 -0.00446 0.00111 -0.00247 O09 3 0.005769 0.207954 0.843413 11.00000 0.01364 0.00998 = 0.01735 -0.00155 0.00327 0.00032 O10 3 0.362848 0.225835 0.847022 11.00000 0.01672 0.01271 = 0.01803 -0.00205 -0.00082 -0.00787 O11 3 0.726932 0.087437 0.101074 11.00000 0.01137 0.00621 = 0.01688 -0.00241 0.00058 -0.00119 O12 3 0.214997 0.149006 0.643538 11.00000 0.01333 0.01084 = 0.01299 -0.00382 0.00122 -0.00114 O13 3 0.341007 0.655800 0.198107 11.00000 0.01016 0.01131 = 0.01750 -0.00448 0.00123 -0.00207 HKLF 4 REM z00151320901_pl_jp_inc_om100_bkg1_a.res in P-1 REM wR2 = 0.1085, GooF = S = 1.202, Restrained GooF = 1.202 for all data REM R1 = 0.0450 for 3039 Fo > 4sig(Fo) and 0.0533 for all 3412 data REM 208 parameters refined using 0 restraints END WGHT 0.0476 1.1554 REM Highest difference peak 1.069, deepest hole -0.673, 1-sigma level 0.158 Q1 1 0.2647 0.8905 0.1940 11.00000 0.05 1.07 Q2 1 0.0278 0.5969 0.2138 11.00000 0.05 1.04 Q3 1 0.7181 0.0627 0.3187 11.00000 0.05 0.86 Q4 1 -0.1015 0.1964 0.8348 11.00000 0.05 0.79 Q5 1 0.4533 0.2652 0.1436 11.00000 0.05 0.78 ; _shelx_res_checksum 72253 _shelx_hkl_file ; 0 0 -2 35.8338 1.41364 5 0 0 2 38.1116 3.37634 2 0 0 2 34.7398 1.43681 5 0 0 2 37.0338 2.45517 27 0 0 -2 37.2894 2.49315 27 0 0 -2 31.8745 1.25600 12 0 0 2 37.2866 1.36910 12 0 0 3 3105.39 25.0531 2 0 0 3 3082.96 17.4002 25 0 0 3 3077.06 14.1613 5 0 0 -3 3059.94 12.8623 5 0 0 3 3143.39 12.2993 12 0 0 -3 3126.60 22.0963 27 0 0 4 945.344 5.02970 14 0 0 -4 1003.60 15.1794 27 0 0 -4 981.513 14.2347 26 0 0 4 962.583 11.6588 25 0 0 4 996.056 16.6242 2 0 0 4 980.598 9.54258 5 0 0 5 757.994 9.71237 5 0 0 -5 767.355 15.4424 27 0 0 5 740.577 16.1555 24 0 0 -5 770.421 14.2634 26 0 0 5 746.575 12.2806 25 0 0 -5 789.573 7.38385 12 0 0 5 777.330 16.3052 2 0 0 6 340.430 11.9663 2 0 0 -6 330.831 5.35692 4 0 0 6 320.792 11.9418 24 0 0 6 327.963 7.29120 5 0 0 -6 321.116 10.2366 26 0 0 -6 320.467 11.4076 9 0 0 6 317.583 9.52715 25 0 0 -6 316.109 11.2616 27 0 0 -7 1433.90 21.5978 26 0 0 -7 1458.00 26.2336 27 0 0 7 1490.89 26.7147 24 0 0 7 1511.75 25.5267 2 0 0 -7 1440.74 24.8824 9 0 0 7 1472.69 21.1233 25 0 0 -7 1487.26 12.1650 4 0 0 8 284.490 7.19804 10 0 0 -8 274.602 13.3516 27 0 0 8 280.074 12.8117 24 0 0 -8 274.906 11.8715 9 0 0 -8 272.387 10.4408 26 0 0 8 271.980 11.1105 25 0 0 9 229.647 6.96897 10 0 0 -9 218.513 11.0860 9 0 0 -9 234.337 13.6774 27 0 0 9 236.553 11.9559 2 0 0 9 244.297 11.6932 25 0 0 -9 222.810 9.87077 26 0 0 9 222.961 12.3605 24 0 0 10 788.033 23.0635 24 0 0 -10 746.013 15.2452 8 0 0 10 757.859 13.2679 10 0 0 10 802.243 22.3586 2 0 0 -10 751.414 20.2020 9 0 0 -10 732.314 16.8086 26 0 0 10 796.434 20.8692 25 0 0 -10 723.845 24.5243 27 0 0 11 105.723 10.6049 25 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-10 789.205 10.1064 12 0 -3 -10 599.483 23.9688 22 0 -3 -10 741.461 13.1495 5 0 3 10 786.781 9.86136 14 0 -3 -11 50.0627 4.17662 5 0 3 11 50.9390 6.86253 27 0 -3 -11 37.9748 7.29897 3 0 -3 -11 53.0726 3.24480 12 0 3 11 53.1893 3.37578 14 0 3 11 45.6651 6.41369 20 0 3 11 48.1633 4.14655 10 0 -3 -11 41.0097 8.66112 22 0 3 12 309.060 14.0492 20 0 -3 -12 320.231 17.8122 3 0 -3 -12 387.111 7.62014 12 0 3 12 332.114 18.7050 2 0 3 12 370.420 17.1328 7 0 3 12 405.016 7.70018 14 0 -3 -12 357.203 9.94964 5 0 -3 -13 95.4780 11.4946 9 0 3 13 106.583 12.7041 24 0 3 13 90.2900 11.3483 2 0 3 13 105.797 6.63806 10 0 -3 -13 89.5473 11.5254 3 0 -3 -13 104.282 11.3923 26 0 3 13 104.605 11.3028 7 0 3 13 85.6986 8.91755 20 0 3 14 13.2356 8.47233 2 0 -3 -14 26.9623 8.90919 26 0 -3 -14 4.52443 8.40350 9 0 3 14 29.1260 9.79003 24 0 3 14 2.13924 2.82150 10 0 -3 -14 2.87275 7.27183 3 0 3 14-0.11104 7.52370 7 0 -4 11 83.9715 7.08662 5 0 -4 10 48.6530 5.19549 5 0 -4 10 38.9946 3.49924 10 0 -4 10 41.3404 8.04603 17 0 -4 10 47.8226 4.95179 12 0 4 -10 37.6534 6.55552 16 0 4 -9 119.140 9.20762 16 0 -4 9 106.749 4.77038 10 0 -4 9 116.632 6.56202 5 0 -4 9 111.964 10.3285 17 0 4 -8 2.52774 4.55113 27 0 -4 8 2.35454 1.66712 10 0 -4 8-0.95271 4.75568 17 0 4 -8 9.22164 4.66829 16 0 -4 8-0.57539 2.50859 5 0 -4 7 1.18903 1.59976 10 0 -4 7-0.42475 4.24145 17 0 4 -7 5.04515 6.08879 2 0 4 -7-0.80859 4.00165 16 0 -4 7 1.16872 2.26941 12 0 -4 7 1.93400 6.99315 26 0 4 -6 99.9722 7.59449 16 0 4 -6 92.5665 9.70675 2 0 4 -6 101.011 10.1694 24 0 -4 6 110.616 4.79112 12 0 -4 6 103.829 8.27900 17 0 -4 6 101.132 9.65345 26 0 -4 6 102.889 9.53611 9 0 -4 6 98.6223 3.60841 10 0 -4 5 342.426 13.7609 9 0 -4 5 373.537 13.7040 26 0 -4 5 370.637 13.5870 17 0 4 -5 346.405 14.5971 24 0 4 -5 341.068 14.6879 2 0 -4 5 356.797 7.47566 12 0 4 -4 204.546 10.3444 24 0 4 -4 212.783 13.5522 1 0 -4 4 202.250 7.14408 8 0 -4 4 216.433 9.95514 9 0 -4 4 212.289 9.48403 26 0 4 -4 210.459 10.4615 2 0 -4 4 225.857 10.0089 17 0 4 -3 72.6583 5.97724 24 0 4 -3 69.7616 7.80292 1 0 -4 3 61.1466 3.74415 8 0 -4 3 63.9842 8.07811 19 0 -4 2 2021.42 35.2507 19 0 -4 2 1903.82 12.7963 11 0 -4 2 1903.47 16.8422 8 0 4 -2 2007.33 31.8524 1 0 4 -2 1836.16 28.2650 17 0 -4 2 1921.94 30.0568 16 0 -4 1 1297.68 12.5788 8 0 4 -1 1396.70 23.6398 1 0 -4 1 1260.89 9.74943 11 0 4 -1 1236.13 20.5126 17 0 -4 1 1371.06 26.6674 19 0 -4 1 1325.41 22.1106 16 0 4 0 4.70610 2.66853 17 0 4 0 7.72700 5.31222 23 0 4 0 7.62549 3.00459 1 0 -4 0 8.68927 4.54006 1 0 -4 0 4.43274 3.32887 19 0 -4 0 9.64641 3.09601 16 0 -4 0 6.30316 4.90020 6 0 -4 -1 602.091 15.9540 1 0 -4 -1 589.020 17.8813 6 0 4 1 580.211 16.5378 19 0 -4 -1 611.969 4.18542 10 0 -4 -1 612.326 17.6454 18 0 4 2 0.86345 3.59055 21 0 -4 -2 1.40954 2.62432 1 0 -4 -2 6.07716 3.79487 18 0 -4 -2-2.32297 3.53873 6 0 4 2 0.68222 3.33000 23 0 -4 -2 0.99125 4.46044 23 0 4 2-0.40846 3.05247 19 0 -4 -3 250.196 8.84467 18 0 -4 -3 261.753 14.2188 23 0 4 3 233.634 11.4744 6 0 4 3 288.238 13.2155 21 0 4 4 589.380 16.8827 21 0 4 4 554.476 15.1783 18 0 4 4 544.252 15.5658 6 0 -4 -4 577.352 15.5805 20 0 4 4 593.458 19.7321 22 0 -4 -4 583.576 19.5085 23 0 4 4 614.865 7.82099 10 0 -4 -4 520.076 19.1619 21 0 4 5 1010.06 20.4886 3 0 4 5 1032.03 25.1204 22 0 4 5 960.862 19.5474 6 0 4 5 1054.59 11.2356 10 0 4 5 956.601 18.7424 18 0 -4 -5 915.262 25.3590 21 0 -4 -5 1003.36 20.3178 7 0 -4 -5 1018.71 18.7530 20 0 4 6 17.6527 3.44807 18 0 4 6 17.4394 3.80299 3 0 -4 -6 16.1626 4.15126 7 0 4 6 21.9064 4.63850 22 0 4 6 16.6884 1.46424 15 0 -4 -6 17.5500 5.05179 21 0 4 6 19.5403 2.13105 10 0 4 7 382.287 14.6639 20 0 4 7 400.246 7.18626 4 0 -4 -7 407.737 11.2545 7 0 4 7 433.426 8.36362 10 0 -4 -7 371.262 16.8269 21 0 -4 -8 1435.21 32.7386 21 0 -4 -8 1361.61 35.6725 22 0 4 8 1732.34 15.0680 4 0 4 8 1670.40 33.4586 27 0 -4 -8 1685.17 27.9499 25 0 4 8 1567.92 29.5493 20 0 4 8 1665.72 17.5120 10 0 -4 -9 38.7222 8.34976 22 0 4 9 53.6807 2.99353 4 0 4 9 51.2507 7.79973 27 0 -4 -9 40.0528 6.28218 25 0 -4 -9 48.9233 4.31467 5 0 -4 -9 33.3167 6.33740 21 0 4 9 49.9774 7.19374 20 0 4 9 50.3329 3.66506 10 0 4 10 1.75081 4.93069 27 0 -4 -10 0.30913 2.01613 12 0 -4 -10 0.46274 4.05712 21 0 4 10 6.11605 5.35210 20 0 4 10 4.55487 2.19248 10 0 4 10 1.24927 2.53591 14 0 -4 -10 4.48310 2.70825 5 0 -4 -10 4.57332 6.43423 22 0 -4 -10 0.67674 5.04250 25 0 -4 -10-3.52501 5.44426 3 0 4 11 44.5320 3.60555 14 0 -4 -11 28.3543 7.90544 3 0 4 11 45.1599 4.17639 10 0 -4 -11 50.2505 3.33978 12 0 -4 -11 27.2668 8.73633 22 0 4 11 32.1621 6.66715 27 0 -4 -11 43.1093 4.29021 5 0 -4 -11 27.2280 6.23596 21 0 4 11 30.0745 6.89831 20 0 4 12 63.3207 8.10336 27 0 4 12 86.7687 4.62808 14 0 4 12 57.6879 8.26837 20 0 -4 -12 70.0755 5.22087 5 0 -4 -12 60.3636 9.86877 3 0 -4 -12 77.2864 3.87980 12 0 -4 -13 76.0836 11.4073 3 0 4 13 87.9349 6.24999 10 0 4 13 68.6801 10.7956 2 0 4 13 72.5859 8.42931 27 0 4 13 69.0671 9.23085 20 0 4 13 100.616 4.95889 14 0 -4 -13 77.9801 5.50863 5 0 -4 -13 99.1360 4.41692 12 0 4 14 223.239 10.2472 10 0 -4 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1006.91 16.0750 10 0 5 11 144.826 11.9414 27 0 -5 -11 144.791 9.63115 25 0 5 11 167.205 5.93380 14 0 5 11 118.180 11.2831 20 0 -5 -11 150.365 7.58619 5 0 -5 -11 136.837 13.6503 21 0 -5 -12 310.614 12.2822 25 0 -5 -12 349.794 7.63338 12 0 -5 -12 318.604 10.6614 5 0 5 12 251.977 15.5479 20 0 5 12 291.958 15.9851 27 0 5 12 359.773 8.46880 14 0 5 13 231.557 14.4860 27 0 -5 -13 269.849 6.76620 12 0 5 13 242.753 10.0313 10 0 -5 -13 243.252 9.49192 5 0 -5 -14 83.9033 6.19042 5 0 5 14 83.1698 6.64117 10 0 5 14 78.7676 9.61880 27 0 -6 9 156.914 7.89150 12 0 -6 9 164.278 8.24763 5 0 -6 8 292.068 9.91080 5 0 6 -8 267.887 20.7569 2 0 -6 8 302.850 10.0313 12 0 -6 8 270.232 21.6590 19 0 6 -7 118.101 12.6959 1 0 -6 7 141.375 6.56530 12 0 6 -7 144.426 14.6562 2 0 -6 7 154.160 14.0776 26 0 -6 7 117.899 14.6958 19 0 -6 7 116.610 3.98761 10 0 -6 6 338.438 21.5372 19 0 -6 6 314.653 5.72712 10 0 6 -6 305.324 18.2459 1 0 6 -6 372.353 19.6437 2 0 -6 6 392.498 17.5194 26 0 6 -5 39.8963 7.85195 2 0 6 -5 44.3845 8.22277 24 0 6 -5 31.2898 7.14621 1 0 -6 5 48.9611 8.26287 26 0 -6 5 37.1964 8.90037 19 0 -6 5 34.4989 1.95676 10 0 -6 5 44.5395 7.65809 9 0 6 -4 107.112 9.52689 24 0 6 -4 100.181 9.84148 1 0 -6 4 101.465 11.5258 19 0 -6 4 105.572 8.79355 9 0 6 -4 89.6857 8.76066 2 0 -6 4 100.891 6.10395 8 0 -6 4 114.254 8.80869 26 0 -6 4 87.3233 2.40428 10 0 6 -4 100.693 2.92437 14 0 6 -3 142.398 9.48998 24 0 -6 3 110.446 2.10554 10 0 6 -3 136.393 9.31573 2 0 -6 3 131.721 12.0984 19 0 6 -3 121.559 9.85513 1 0 -6 2 29.9946 2.70406 11 0 -6 2 20.8884 6.91289 16 0 -6 2 32.1276 6.70039 19 0 6 -2 24.6598 6.21119 17 0 6 -2 26.4292 5.25394 1 0 -6 1 616.140 25.5997 6 0 -6 1 629.004 8.74853 11 0 6 -1 579.418 17.9282 17 0 -6 1 667.264 21.6407 19 0 -6 1 608.860 19.5138 16 0 6 -1 591.956 28.2307 23 0 -6 1 629.170 10.9681 8 0 -6 0 16.6035 4.52602 16 0 6 0 3.12111 5.14095 23 0 6 0 14.6933 4.14643 17 0 6 1 73.1605 9.88505 23 0 -6 -1 52.9071 8.01045 18 0 -6 -2 2656.67 41.9283 18 0 6 2 2596.68 50.9107 21 0 -6 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1.33543 7.81850 19 0 -7 6 11.3308 8.15203 9 0 7 -6 15.9646 8.38540 2 0 -7 6 13.7903 3.02993 12 0 7 -6 6.07333 5.61894 1 0 -7 5 41.8490 3.96427 12 0 7 -5 31.6598 7.22247 1 0 7 -5 54.0057 9.32782 2 0 -7 5 41.8347 9.56020 19 0 -7 5 61.9006 9.08103 26 0 7 -4 17.8538 2.13985 14 0 -7 4 30.6000 7.15224 26 0 7 -4 16.8707 6.30204 2 0 -7 4 20.1606 3.70170 8 0 -7 4 24.4197 7.56146 19 0 7 -4 20.4311 5.98666 1 0 7 -3 223.489 20.4502 23 0 7 -3 287.131 13.7135 24 0 7 -3 292.788 15.8705 1 0 -7 3 287.735 17.4207 19 0 -7 3 287.348 9.88772 8 0 -7 3 240.455 20.0422 6 0 7 -3 282.365 14.1030 2 0 -7 2 182.184 13.8203 16 0 -7 2 180.150 16.8077 6 0 -7 2 204.842 14.2171 19 0 7 -2 181.796 12.9902 17 0 7 -2 165.317 17.4855 23 0 -7 2 195.686 7.64508 8 0 -7 2 194.152 5.72035 11 0 7 -1 234.746 19.3865 23 0 7 -1 266.663 13.7967 17 0 -7 1 266.901 19.0222 6 0 -7 1 284.365 6.53352 11 0 -7 1 277.107 15.2120 16 0 -7 0 300.829 18.4100 18 0 -7 0 328.417 19.7167 6 0 7 0 296.904 20.5266 23 0 -7 0 313.592 6.48042 11 0 -7 0 315.876 14.7266 16 0 7 0 301.225 13.4284 17 0 -7 -1 323.733 13.8862 16 0 7 1 331.837 12.9302 17 0 -7 -1 361.274 19.1704 18 0 -7 -1 332.024 18.3322 6 0 -7 -1 321.010 19.8759 1 0 7 1 350.371 20.8662 23 0 7 2 27.7610 7.80231 19 0 7 2 21.2266 7.18114 21 0 7 2 27.0465 6.73987 23 0 -7 -2 25.3161 6.26052 18 0 -7 -2 25.6228 6.65246 1 0 -7 -2 30.2808 6.58511 6 0 -7 -3 329.285 16.0002 6 0 7 3 275.571 15.5372 19 0 7 3 332.241 19.6515 21 0 -7 -3 337.455 15.5030 18 0 -7 -3 336.663 17.2353 1 0 -7 -4 533.490 20.3296 1 0 -7 -4 531.969 17.6901 18 0 7 4 564.929 24.8871 21 0 7 4 470.283 19.2227 19 0 -7 -5 208.258 18.5062 23 0 7 5 223.018 14.5698 21 0 7 5 226.814 17.3118 22 0 -7 -5 245.452 13.7134 1 0 7 5 207.503 12.3793 19 0 -7 -5 248.063 15.2955 20 0 -7 -6 143.853 15.6279 23 0 -7 -6 161.831 13.3970 7 0 7 6 168.181 15.0027 22 0 7 6 174.116 13.0627 3 0 7 6 144.368 11.4458 21 0 -7 -6 177.867 12.2804 20 0 -7 -7 501.892 20.3725 7 0 -7 -7 433.486 25.1128 23 0 7 7 518.503 20.7427 3 0 7 7 470.348 21.9416 6 0 7 7 494.427 23.6480 22 0 -7 -7 520.702 18.3772 20 0 7 8 755.732 8.18039 15 0 7 8 691.143 22.8977 3 0 -7 -8 627.279 30.1842 23 0 7 8 676.100 27.2833 22 0 7 8 608.573 23.3090 18 0 -7 -8 715.906 22.7699 7 0 7 8 652.034 25.3541 6 0 7 9 143.824 3.92250 15 0 -7 -9 109.084 13.6325 23 0 -7 -9 115.118 13.9889 21 0 7 9 135.474 10.1115 3 0 -7 -9 144.028 10.6022 7 0 7 9 127.837 11.3918 18 0 7 9 123.166 12.2768 6 0 7 10 77.4476 10.0121 6 0 7 10 85.3198 4.91024 4 0 7 10 69.4661 7.69321 3 0 -7 -10 74.2503 7.74948 7 0 7 10 52.1439 8.22177 18 0 -7 -11 77.6181 7.55706 7 0 7 11 79.3710 4.79729 4 0 -7 -11 83.0474 11.2671 25 0 7 11 72.1996 9.33247 18 0 7 11 53.8300 8.80864 6 0 7 11 74.3729 11.9717 27 0 7 12 21.1482 8.74022 27 0 -7 -12 28.2696 8.84577 25 0 7 12 28.1892 7.39363 18 0 7 12 27.0792 7.28273 6 0 7 12 36.9623 3.68949 4 0 7 12 26.7648 4.08315 10 0 7 13 114.630 12.8476 27 0 -7 -13 110.899 10.2983 25 0 -7 -13 137.882 8.60513 5 0 7 13 115.721 11.4770 6 0 7 14 232.217 8.62905 14 0 -7 -14 195.934 9.90670 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288.881 19.9597 18 0 8 0 268.852 14.6127 17 0 -8 0 261.662 18.9200 6 0 -8 0 270.330 6.63353 11 0 8 0 247.577 19.7551 23 0 8 1 91.7743 8.77447 17 0 -8 -1 86.9304 11.1285 6 0 -8 -1 93.9755 9.31133 16 0 8 1 83.4631 11.4359 23 0 8 1 89.8173 12.7586 21 0 -8 -1 88.5284 11.4093 18 0 -8 -2 367.808 18.6618 18 0 -8 -2 404.304 16.3775 16 0 8 2 397.847 14.8879 17 0 -8 -2 352.803 22.1647 1 0 8 2 414.433 22.6240 23 0 8 2 367.628 22.9909 21 0 -8 -2 383.478 19.7650 6 0 8 3 61.8382 9.99778 19 0 -8 -3 76.2848 10.7394 1 0 8 3 63.1069 10.3184 21 0 -8 -3 65.6449 8.55262 18 0 8 4 236.399 15.9688 19 0 -8 -4 263.953 16.9553 1 0 -8 -4 270.161 14.2428 18 0 8 4 282.189 19.5648 21 0 8 5 937.426 32.4442 21 0 8 5 869.897 27.6335 19 0 -8 -5 948.761 29.4887 1 0 -8 -5 974.796 31.2039 20 0 8 6-7.17347 6.78737 22 0 8 6-5.07049 4.80047 21 0 -8 -6 3.71077 6.14759 20 0 8 6-0.63811 5.08947 19 0 -8 -6-1.01501 4.09337 1 0 -8 -6 4.14999 8.17530 7 0 -8 -6 5.72225 8.36190 23 0 -8 -7 197.745 15.4716 7 0 -8 -7 207.885 13.6606 20 0 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6.39461 7.39986 22 0 -10 -8 4.77399 5.69989 1 0 10 8 1.85103 6.91692 3 0 10 9 43.8137 9.42660 3 0 10 9 50.3030 11.3300 22 0 -10 -9 55.8842 9.07327 20 0 -10 -9 39.1051 8.90647 1 0 10 9 54.1337 3.98079 15 0 -10 -9 58.8105 11.6623 7 0 -10 -10 794.922 27.9196 7 0 10 10 752.062 28.1015 3 0 -10 -10 702.769 30.4544 1 0 -10 -11 2.95412 5.73645 1 0 10 11-1.49213 3.82272 14 0 10 11 4.33419 5.45572 3 0 11 1 83.9283 5.48998 14 0 -11 -1 63.8157 5.79646 8 0 -11 -1 60.5703 11.7845 6 0 -11 -1 65.8851 4.64807 11 0 11 2 104.465 5.95004 14 0 -11 -2 91.6202 5.13650 11 0 -11 -2 95.2543 6.55508 8 0 -11 -3-1.50747 6.15195 18 0 11 3 4.05902 3.94048 14 0 11 3 0.24972 7.90326 21 0 -11 -3 4.91283 2.63127 11 0 11 4 236.313 21.0643 21 0 -11 -4 199.281 22.2037 1 0 -11 -4 241.806 15.9136 18 0 -11 -4 196.177 19.3209 20 0 11 5 116.217 14.3495 21 0 -11 -5 114.388 16.6420 1 0 -11 -5 110.402 15.6185 20 0 -11 -6 13.5114 9.83765 1 0 -11 -6 25.7701 9.86012 20 0 -11 -6 26.2421 12.3672 7 0 11 7 578.397 29.9427 3 0 -11 -7 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695.570 11.6400 8 2 -6 0 615.149 22.7204 16 -2 6 0 625.358 19.2479 17 -2 6 0 660.291 9.38436 14 2 -6 0 708.903 22.0081 19 2 -6 1 122.393 3.46262 11 -2 6 -1 120.853 10.7091 1 -2 6 -1 89.2615 9.15612 17 -2 6 -1 114.283 8.20647 2 -2 6 -1 113.262 4.21882 14 2 -6 1 116.703 10.9781 19 -2 6 -2 169.785 10.6904 2 2 -6 2 185.216 13.9605 19 -2 6 -2 157.996 12.4857 1 -2 6 -2 170.042 10.1696 24 2 -6 2 191.807 11.2792 26 2 -6 2 172.767 4.15266 11 -2 6 -3 643.596 21.6274 2 2 -6 3 594.506 25.2008 19 2 -6 3 647.709 20.4116 26 -2 6 -3 616.927 19.6624 24 2 -6 3 615.414 14.4422 8 -2 6 -4 18.2885 6.97292 1 2 -6 4 16.8402 7.80960 19 -2 6 -4 18.8556 6.94699 2 -2 6 -4 12.1708 6.75677 24 2 -6 4 26.9362 8.26562 26 -2 6 -5 372.702 20.1427 2 2 -6 5 381.417 23.0293 19 2 -6 5 416.092 20.4175 9 -2 6 -6 193.882 16.6829 2 2 -6 6 202.942 18.6268 19 2 -6 6 203.310 16.3118 9 -2 6 -6 154.844 15.8086 1 2 -6 7 17.7297 3.41930 12 2 -6 7 14.6436 9.42610 19 2 -6 7 28.5703 10.6004 9 -2 6 -7 18.1832 10.4633 2 -2 6 -7 21.1710 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5 8 1537.57 16.7927 14 -2 5 8 1521.09 35.2392 22 -2 5 7 302.430 16.7272 22 2 -5 -7 259.688 18.3099 23 2 -5 -7 312.048 10.7578 20 -2 5 7 321.255 7.72279 14 2 -5 -7 298.134 12.8941 7 -2 5 6 207.472 6.15146 14 -2 5 6 206.618 12.5098 21 2 -5 -6 218.717 5.95613 10 2 -5 -6 161.506 15.2613 23 -2 5 6 223.885 15.0430 22 -2 5 6 194.270 5.20952 15 2 -5 -6 218.564 10.3348 20 2 -5 -5 389.599 14.6644 20 2 -5 -5 418.166 7.73179 10 -2 5 5 389.945 7.86828 14 -2 5 5 381.400 6.81062 15 -2 5 5 442.657 20.1075 21 -2 5 5 382.382 13.4390 19 2 -5 -4 308.033 12.2636 6 -2 5 4 281.059 12.2738 19 -2 5 4 294.740 6.78470 14 2 -5 -4 321.947 6.64338 10 -2 5 4 317.378 17.4772 21 2 -5 -4 320.600 11.4516 18 -2 5 3 44.8281 7.60049 23 -2 5 3 34.3770 7.31215 21 2 -5 -3 45.8267 5.89663 18 2 -5 -3 50.3971 2.80860 10 -2 5 3 43.6050 3.13269 14 2 -5 -3 46.6449 6.78917 6 2 -5 -3 49.0193 5.77367 16 2 -5 -2 2.76791 5.13535 6 -2 5 2 17.0912 6.49196 23 2 -5 -2 6.46970 4.17102 16 -2 5 2 7.62306 2.18042 14 -2 5 2 12.4017 3.58763 17 -2 5 1 754.338 17.0591 17 -2 5 1 787.793 31.8386 23 -2 5 1 754.210 4.85659 13 2 -5 -1 845.676 20.1383 19 2 -5 -1 773.372 21.5680 16 -2 5 1 762.765 9.71223 14 2 -5 0 5.89970 1.71626 8 -2 5 0 6.31292 4.41070 17 -2 5 0 6.27757 2.18231 14 2 -5 0 7.64332 4.42672 19 2 -5 0 7.51008 4.94833 16 -2 5 -1 747.989 20.7321 17 2 -5 1 714.273 23.9367 16 2 -5 1 812.998 24.4703 19 -2 5 -1 814.828 24.1645 1 2 -5 1 810.955 12.4070 8 -2 5 -1 773.827 9.11372 14 -2 5 -2 616.169 17.3789 2 2 -5 2 627.234 12.0951 8 2 -5 2 669.619 17.9282 26 2 -5 2 641.991 6.77809 11 2 -5 2 643.844 23.9119 19 -2 5 -2 631.676 16.8427 24 -2 5 -2 599.680 22.7948 1 -2 5 -3 211.233 15.0821 1 2 -5 3 241.558 12.2699 26 2 -5 3 233.298 12.3658 9 -2 5 -3 235.049 11.7141 24 2 -5 3 236.603 15.9603 19 -2 5 -3 233.898 12.3860 2 2 -5 4 4.45670 6.32900 19 2 -5 4 14.7048 6.20418 9 2 -5 4 15.9526 7.24767 26 -2 5 -4 17.6520 6.27610 24 -2 5 -4 7.34558 5.42765 2 -2 5 -4 1.43882 5.56504 1 2 -5 5 27.0506 8.64848 26 -2 5 -5 18.1955 7.38220 24 -2 5 -5 35.5114 7.91641 2 -2 5 -5 15.5386 7.40887 1 2 -5 6 23.8223 5.72650 17 -2 5 -6 7.30051 6.89652 1 -2 5 -6 15.6112 8.16197 2 2 -5 6 28.3101 10.2511 26 -2 5 -7 26.6454 9.74493 1 2 -5 7 23.6038 9.57470 9 2 -5 7 23.7498 6.20155 17 2 -5 8 32.6536 7.37407 17 -2 5 -8 23.6100 10.4287 1 2 -5 8 35.3651 4.05485 12 2 -5 8 37.1925 4.35800 5 -2 5 -9 38.8467 11.4819 1 2 -5 9 46.9506 5.25416 5 2 -5 9 56.0801 4.85316 12 2 -4 -14 28.0601 3.69576 12 2 -4 -14 24.5392 4.07892 5 -2 4 14 27.7468 8.47225 2 2 -4 -13 16.9856 3.71822 5 -2 4 13 9.20433 5.42649 27 -2 4 13 16.1840 7.57918 2 2 -4 -13 17.8035 3.23179 12 -2 4 12 83.5495 10.4858 2 -2 4 12 81.9560 8.98140 27 2 -4 -12 88.4926 5.63305 5 2 -4 -12 93.0716 5.21100 12 2 -4 -11 34.3308 8.21907 21 -2 4 11 29.8207 4.54241 18 -2 4 11 37.1635 6.98865 27 -2 4 11 30.6393 4.97352 6 2 -4 -11 44.0666 4.37646 5 2 -4 -10 61.4590 5.58247 25 -2 4 10 69.1049 8.50703 27 -2 4 10 66.8202 4.60546 14 -2 4 10 54.8250 5.29641 18 2 -4 -10 50.8445 8.75747 23 2 -4 -10 65.4765 5.06754 5 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4.78196 3.80931 24 2 -4 2 5.32221 2.01879 8 2 -4 2 4.66401 4.24456 26 2 -4 3 3.11236 4.89963 26 -2 4 -3 6.09945 4.56008 24 2 -4 3 6.10112 4.38625 9 2 -4 3 3.03089 2.15741 8 -2 4 -3 7.95974 3.82866 16 -2 4 -3 3.73671 4.37293 2 2 -4 3 1.54815 3.33538 17 2 -4 4 48.4329 5.78383 17 2 -4 4 45.5168 7.68362 26 -2 4 -4 36.4310 8.07192 1 -2 4 -4 36.8743 6.85067 2 2 -4 4 40.4236 6.95650 9 -2 4 -4 44.6338 7.08461 24 -2 4 -4 42.7250 6.08814 16 2 -4 5 1701.42 30.6358 17 -2 4 -5 1630.57 33.3151 24 2 -4 5 1657.47 33.9319 9 2 -4 5 1757.21 34.2127 26 -2 4 -5 1585.35 35.2690 2 -2 4 -5 1701.06 32.3909 16 2 -4 6 17.8201 5.32403 17 2 -4 6 28.1832 9.24628 26 -2 4 -6 23.1193 5.91682 16 -2 4 -6 30.2753 8.31458 2 2 -4 6 20.8127 8.15176 9 2 -4 7 136.710 5.39612 12 -2 4 -7 124.044 10.4585 16 2 -4 7 131.007 10.5433 17 -2 4 -8 718.965 23.7634 16 2 -4 8 773.584 24.7846 17 2 -4 8 806.148 15.6703 5 2 -4 9 25.6905 4.26310 5 -2 4 -9 17.5916 6.47627 16 2 -4 9 26.1731 3.47678 12 2 -4 9 22.2216 6.97153 17 2 -4 10 21.4524 3.97295 12 2 -4 10 20.0547 4.51369 5 -2 4 -10 8.76182 6.33803 16 2 -3 -14 5.25170 2.99251 12 -2 3 14 0.87592 7.68617 24 -2 3 14 15.1202 7.39612 2 2 -3 -13 213.257 7.78363 5 -2 3 13 211.977 15.5749 24 -2 3 13 180.470 12.7894 2 2 -3 -13 226.602 7.19109 12 2 -3 -12 11.1455 8.26905 22 -2 3 12 32.2815 5.94485 27 2 -3 -12 23.1661 3.36195 12 -2 3 12 30.3056 7.63256 2 2 -3 -12 19.3085 6.93164 21 2 -3 -12 24.8852 3.55674 5 2 -3 -11 12.5088 2.92814 12 -2 3 11 14.5229 7.00018 2 2 -3 -11 8.17296 2.91365 5 2 -3 -11 6.74731 7.42245 22 -2 3 11 12.8077 5.12794 20 -2 3 11-1.91646 4.35733 27 2 -3 -11 3.94060 5.10721 21 2 -3 -10 1098.21 15.8557 5 -2 3 10 1094.25 23.8913 27 2 -3 -9 156.283 6.32341 5 -2 3 9 158.709 9.92531 27 2 -3 -9 134.395 11.5336 21 2 -3 -8 151.094 6.60265 25 2 -3 -8 134.301 10.9096 21 -2 3 8 134.074 6.50203 6 -2 3 8 163.449 10.2430 27 -2 3 8 169.034 5.50153 14 2 -3 -7 1.51649 2.39719 7 -2 3 7 4.75057 3.03651 6 -2 3 7 3.34744 4.88330 27 -2 3 7 5.73551 2.53505 18 2 -3 -7 0.97903 3.68660 23 2 -3 -7 4.06776 4.54437 25 2 -3 -7-2.09588 4.10350 21 -2 3 7-1.27379 2.45496 14 -2 3 7 3.16049 1.82279 4 2 -3 -6 26.5841 2.31848 10 -2 3 6 29.3824 5.09388 22 2 -3 -6 18.4441 5.22943 23 2 -3 -6 23.4796 3.89402 7 -2 3 6 26.4789 3.74453 3 2 -3 -6 22.1811 5.65736 21 -2 3 6 19.7950 3.37685 18 -2 3 6 25.2218 2.71544 14 -2 3 6 21.2158 3.96756 6 2 -3 -5 1609.78 34.8138 23 -2 3 5 1726.62 27.2106 21 2 -3 -5 1624.84 14.6854 10 2 -3 -5 1670.83 18.2222 20 -2 3 5 1626.30 13.9283 14 -2 3 5 1742.22 23.9287 3 -2 3 5 1806.88 31.2806 22 -2 3 4 10.7065 3.88166 21 2 -3 -4 3.84859 4.75456 23 -2 3 4 1.66935 2.01939 15 2 -3 -4 2.89968 1.29821 10 -2 3 4 3.14909 1.84979 14 2 -3 -3 2277.70 26.3470 6 2 -3 -3 2063.95 8.21862 13 -2 3 3 2335.52 36.1358 23 2 -3 -3 2277.84 29.0081 1 -2 3 3 2057.10 13.0546 15 2 -3 -3 2231.29 22.2035 18 -2 3 3 2199.95 14.8128 14 -2 3 3 2209.29 36.2850 21 -2 3 3 2204.36 23.4017 19 -2 3 2 915.332 25.5474 23 2 -3 -2 838.522 15.9057 16 -2 3 2 808.809 8.69262 14 2 -3 -2 850.141 20.2327 1 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1057.07 26.3082 26 -2 3 -5 1071.77 14.2359 8 -2 3 -5 1067.91 26.2229 16 2 -3 5 1038.26 26.0992 9 -2 3 -6 43.0080 3.42468 8 2 -3 6 47.1281 6.95472 17 2 -3 6 46.6419 8.91213 26 2 -3 6 32.6884 7.78735 9 -2 3 -6 41.3501 7.14481 16 -2 3 -7 144.213 9.47315 27 2 -3 7 160.071 5.31894 12 2 -3 7 148.579 6.23827 5 -2 3 -7 139.730 6.02103 8 2 -3 7 143.445 10.9282 17 -2 3 -7 139.090 11.5699 16 -2 3 -8 189.921 13.5086 16 2 -3 8 218.856 6.56179 12 -2 3 -8 189.481 7.29053 8 2 -3 8 205.873 13.5005 17 -2 3 -8 177.231 11.0503 27 2 -3 8 200.023 7.78286 5 -2 3 -9 22.9511 7.28673 16 2 -3 9 15.3013 6.78436 17 -2 3 -9 18.4403 3.06743 8 2 -3 9 17.0605 3.66150 5 2 -3 10 100.317 6.86665 5 2 -3 10 85.7802 10.6331 17 -2 3 -10 84.2110 5.63476 8 -2 3 -10 84.1031 10.6659 16 -2 3 -11 155.388 13.5719 16 2 -3 11 158.179 9.03071 5 2 -3 11 179.390 7.57433 12 -2 3 -11 156.996 7.29608 4 -2 3 -11 141.333 7.39193 8 -2 2 14 189.082 13.9181 24 2 -2 -14 168.202 8.52176 8 -2 2 14 155.203 11.5333 2 2 -2 -14 162.196 14.7274 3 -2 2 13 242.581 13.4527 2 2 -2 -13 213.081 15.4185 3 2 -2 -13 266.743 7.66695 12 -2 2 13 249.169 15.2821 24 2 -2 -12 68.4063 9.58669 3 -2 2 12 89.7131 9.13174 2 2 -2 -12 92.9505 4.83925 12 -2 2 12 78.5741 10.0459 24 2 -2 -12 82.6312 9.36292 9 2 -2 -12 66.0214 10.8458 22 2 -2 -12 61.6253 8.64969 21 2 -2 -11 126.853 5.44653 12 2 -2 -11 108.826 10.2205 3 2 -2 -11 116.701 5.36460 5 2 -2 -11 100.847 7.78900 26 2 -2 -11 80.6678 8.85651 21 2 -2 -11 98.1342 11.4948 22 -2 2 11 102.027 10.4632 24 -2 2 11 118.839 9.98901 2 -2 2 11 91.2951 7.08566 20 2 -2 -10 12.6593 4.66651 21 2 -2 -10 24.4304 2.96763 5 -2 2 10 18.0792 4.12167 20 2 -2 -10 27.0000 7.43896 22 2 -2 -10 27.3189 3.06109 12 2 -2 -10 17.5208 5.65151 3 -2 2 10 25.6480 5.00075 27 2 -2 -9 17.4602 2.71745 12 2 -2 -9 15.1827 5.09597 3 2 -2 -9 14.3518 6.36105 22 2 -2 -9 13.7926 4.58604 21 -2 2 9 12.9978 4.37108 27 -2 2 9 14.2042 3.85965 20 2 -2 -8 180.583 10.6778 21 -2 2 8 190.373 7.96706 20 -2 2 8 216.750 9.67816 27 -2 2 8 210.645 10.6097 2 2 -2 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2 585.765 6.52082 15 2 -2 -2 637.793 11.8935 16 2 -2 -2 625.958 14.1980 1 2 -2 -2 626.870 6.72101 14 -2 2 2 620.061 7.20613 14 -2 2 2 685.193 18.8748 23 -2 2 1 788.524 15.0454 1 2 -2 -1 751.049 18.2216 1 2 -2 -1 728.286 14.5689 16 -2 2 1 728.326 10.0402 17 -2 2 1 709.669 5.49863 13 2 -2 -1 750.824 12.4109 19 2 -2 -1 709.616 6.83295 14 -2 2 1 701.158 7.11318 15 -2 2 0 11.3379 3.28871 17 2 -2 0 2.37545 3.57188 16 -2 2 0 9.63965 3.02505 16 2 -2 0 9.67572 1.33150 8 -2 2 0 9.89824 3.92744 1 -2 2 0 8.65440 2.38801 2 2 -2 1 1495.33 19.6322 26 2 -2 1 1482.64 17.7077 17 -2 2 -1 1464.80 17.9365 2 -2 2 -1 1495.19 17.0603 24 2 -2 1 1520.45 12.4651 8 -2 2 -1 1555.70 23.0133 16 -2 2 -2 906.398 15.9146 24 -2 2 -2 920.708 16.8719 2 2 -2 2 950.719 16.6042 17 -2 2 -2 1021.05 20.8043 16 2 -2 2 955.131 17.4495 9 2 -2 2 953.084 17.8568 26 -2 2 -3 1249.67 21.8585 24 2 -2 3 1291.16 22.0058 17 2 -2 3 1276.55 22.9446 26 -2 2 -3 1320.68 25.6051 16 -2 2 -3 1200.06 22.0131 2 2 -2 3 1273.86 22.7897 9 2 -2 4 4.15736 3.00580 2 -2 2 -4 6.35236 1.59654 8 2 -2 4 3.80953 4.45499 9 -2 2 -4-2.48603 4.67318 16 2 -2 4 1.22994 5.28949 26 2 -2 4-0.18989 3.79082 17 2 -2 5 483.425 17.6891 9 -2 2 -5 456.392 17.5815 16 -2 2 -5 480.174 9.43033 8 2 -2 5 462.887 16.3256 17 2 -2 5 429.837 16.7206 26 2 -2 6 61.3593 3.68435 5 -2 2 -6 60.4035 3.92989 8 2 -2 6 66.3938 6.14843 2 -2 2 -6 68.2725 6.16021 27 -2 2 -6 68.9508 8.54390 16 2 -2 6 63.6777 7.65343 17 2 -2 7 30.6028 3.23927 5 2 -2 7 31.2810 5.06965 2 -2 2 -7 29.0558 7.20196 16 2 -2 7 31.2798 2.69006 12 -2 2 -7 28.2643 3.17520 8 -2 2 -7 39.1742 5.81674 27 2 -2 7 22.8306 6.39602 17 -2 2 -8 212.303 14.5363 16 2 -2 8 258.108 6.53553 12 -2 2 -8 224.810 12.0542 27 2 -2 8 246.035 15.0396 17 -2 2 -8 231.018 8.11425 8 -2 2 -8 245.278 4.25353 11 2 -2 8 237.483 8.12784 5 2 -2 8 244.168 12.1851 2 2 -2 8 259.016 11.8365 25 2 -2 9 15.0106 6.78371 17 2 -2 9 27.7551 6.61272 25 -2 2 -9 28.5500 1.93630 11 -2 2 -9 27.1007 3.57652 8 2 -2 9 28.8100 3.23526 12 -2 2 -9 26.0223 8.11372 16 2 -2 9 21.9137 3.82186 5 2 -2 10 4.82038 6.56773 17 -2 2 -10 0.64086 2.34114 8 -2 2 -10 0.68601 2.33443 4 2 -2 10-1.97973 3.23787 5 -2 2 -11 236.803 16.9360 16 2 -2 11 259.955 17.6585 17 -2 2 -11 271.700 8.93686 4 2 -2 11 264.076 11.1638 5 -2 2 -11 241.800 9.48979 8 -2 2 -12 18.6774 5.44213 4 2 -2 12 15.3825 3.23697 10 -2 2 -12 11.7472 3.14175 8 2 -2 12 22.5211 5.32487 5 -2 2 -12 12.0631 7.96119 16 -2 1 14 10.3508 6.00090 2 2 -1 -14 7.42676 3.43636 8 2 -1 -14 6.11225 6.57718 3 -2 1 14 10.3174 6.81344 24 -2 1 13 159.562 12.1510 24 2 -1 -13 137.476 7.30357 8 -2 1 13 143.299 10.3555 2 2 -1 -13 139.072 12.1836 3 2 -1 -12 302.101 15.4554 3 2 -1 -12 368.319 8.64228 12 -2 1 12 340.944 16.0053 24 2 -1 -12 249.037 16.8361 22 2 -1 -12 317.169 10.2556 8 -2 1 12 332.854 14.2587 2 2 -1 -12 302.023 13.1729 9 2 -1 -11 1.82401 2.26638 12 -2 1 11 18.8829 5.44897 7 -2 1 11 11.3477 5.17031 2 2 -1 -11 5.28105 5.83689 22 2 -1 -11 7.23611 5.64961 9 -2 1 11 4.96665 6.28390 24 2 -1 -11 6.25335 4.61251 3 2 -1 -11 8.74119 3.93196 26 2 -1 -10 792.905 20.7704 3 2 -1 -10 728.220 12.9831 26 -2 1 10 741.060 15.4962 7 2 -1 -10 702.252 24.0914 22 -2 1 10 841.564 22.8445 24 -2 1 10 814.529 15.0770 10 2 -1 -10 760.088 18.9699 9 -2 1 10 871.133 20.7965 2 2 -1 -10 870.166 12.2219 12 2 -1 -9 45.5987 5.06935 26 -2 1 9 41.0002 5.22451 7 2 -1 -9 36.1333 5.30316 3 -2 1 9 35.1913 3.47294 10 2 -1 -9 40.7541 3.16349 12 2 -1 -9 28.8618 6.11212 22 -2 1 9 42.0791 6.62475 24 2 -1 -8 41.1604 6.54897 22 -2 1 8 40.1680 4.79151 7 2 -1 -8 42.9262 3.19425 12 -2 1 8 45.4281 5.88189 2 2 -1 -7 1551.90 22.3728 3 2 -1 -7 1480.80 24.6625 21 2 -1 -7 1543.12 13.6648 5 2 -1 -7 1523.04 28.8079 22 -2 1 7 1596.76 23.3223 2 -2 1 7 1625.14 21.5489 27 2 -1 -6 376.214 13.6383 22 -2 1 6 395.826 7.60961 20 -2 1 6 390.721 11.1473 2 2 -1 -6 385.293 6.77786 5 -2 1 6 412.532 10.5573 27 2 -1 -6 391.317 10.8903 3 2 -1 -6 388.882 7.34569 10 2 -1 -6 351.945 11.3602 21 2 -1 -5 1433.57 10.5776 14 -2 1 5 1498.90 18.8291 27 2 -1 -5 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2 2 -1 7 135.640 8.99810 24 2 -1 7 128.128 5.46307 5 -2 1 -7 122.304 5.72897 8 -2 1 -8 987.372 21.4149 26 2 -1 8 942.277 22.9197 24 2 -1 8 967.606 21.5834 25 2 -1 8 1023.21 11.9153 12 -2 1 -8 981.899 13.4352 4 -2 1 -8 908.011 15.8920 8 -2 1 -8 863.604 22.5465 27 2 -1 8 899.925 22.6082 2 -2 1 -8 927.298 22.0608 9 2 -1 8 928.007 15.4600 5 2 -1 9 48.3557 6.94775 24 2 -1 9 54.7838 3.63949 12 -2 1 -9 51.1159 3.77509 4 2 -1 9 50.2731 4.71224 5 -2 1 -9 55.9538 8.45246 27 -2 1 -9 49.1996 6.79408 9 -2 1 -9 42.7568 4.26365 8 2 -1 9 57.5583 8.01204 25 2 -1 9 49.2227 6.89780 2 2 -1 10 300.305 14.8066 24 2 -1 10 298.258 10.7371 5 2 -1 10 276.954 14.2273 2 2 -1 10 290.240 14.8459 25 -2 1 -10 280.966 9.92507 8 -2 1 -10 335.656 9.16952 4 2 -1 11 351.060 12.5551 5 2 -1 11 327.488 16.2250 2 2 -1 12 9.28844 8.50327 17 -2 1 -12 20.5108 4.03662 4 2 -1 12 16.6548 6.04247 2 -2 1 -12 13.7551 3.63183 8 2 0 -13 227.888 13.9149 3 -2 0 13 249.131 16.3314 17 2 0 -13 242.430 9.15329 8 -2 0 13 269.475 14.5152 24 -2 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5.64232 12 -2 0 7 213.256 6.48023 10 2 0 -7 204.451 10.6147 27 -2 0 7 216.249 5.56867 7 -2 0 7 217.760 9.77422 24 2 0 -7 212.052 5.15698 26 -2 0 7 231.909 8.69766 2 -2 0 6 197.392 7.45563 2 -2 0 6 184.399 8.30345 24 2 0 -6 185.057 9.23757 27 -2 0 6 183.696 4.49613 7 2 0 -6 176.399 3.88025 14 2 0 -6 187.294 4.97230 12 2 0 -6 168.841 4.23328 26 2 0 -5 883.523 16.6202 27 2 0 -5 877.617 10.0533 10 2 0 -5 891.210 9.91618 12 -2 0 5 904.833 15.5493 24 2 0 -5 887.196 8.04095 14 -2 0 5 919.947 13.5144 2 2 0 -5 917.657 5.28348 4 -2 0 5 869.084 7.65346 7 2 0 -5 865.440 8.14671 5 2 0 -4 15.0851 1.61456 10 2 0 -4 14.8842 2.17862 3 -2 0 4 10.8612 2.43393 2 -2 0 4 12.9894 3.27494 24 2 0 -4 12.8705 1.40132 5 2 0 -4 11.9412 2.73976 22 2 0 -3 897.260 9.32153 10 -2 0 3 916.084 10.8104 24 -2 0 3 933.410 9.37921 27 2 0 -3 1012.74 10.0483 3 2 0 -3 1001.83 14.1646 22 2 0 -3 908.559 6.54085 5 -2 0 3 934.680 8.77441 2 2 0 -3 1063.31 13.9215 21 2 0 -2 334.746 5.55378 1 -2 0 2 342.641 5.59185 21 2 0 -2 321.888 4.96875 26 -2 0 2 337.204 4.60187 27 -2 0 1 94.3019 3.95713 16 -2 0 1 97.5454 3.62917 1 2 0 -1 105.224 3.33793 9 2 0 -1 106.091 3.35475 25 -2 0 1 104.734 1.82879 4 2 0 -1 93.1352 4.28631 26 -2 0 1 97.3627 3.38431 26 -2 0 0 18.9276 1.41206 13 2 0 0 19.7796 2.47194 25 -2 0 0 20.4613 1.22987 4 2 0 0 16.3390 2.85293 9 -2 0 0 19.6425 3.50630 26 2 0 1 222.406 5.71555 24 2 0 1 225.964 5.92034 25 -2 0 -1 223.753 7.42854 26 2 0 1 224.264 7.32255 9 -2 0 -1 196.643 3.61246 15 -2 0 -1 217.786 6.43556 9 -2 0 -1 228.427 3.43626 4 2 0 2 817.359 15.1778 9 2 0 2 794.863 13.7313 2 -2 0 -2 844.135 14.7990 26 -2 0 -2 741.517 6.18776 15 2 0 2 819.767 11.9644 25 2 0 2 812.269 12.6064 24 2 0 2 817.195 6.87859 5 -2 0 -2 842.376 10.8567 27 2 0 3 5.30749 3.82048 2 -2 0 -3 1.63729 2.48045 27 2 0 3 2.80719 3.87928 24 2 0 3-0.18848 1.24340 5 -2 0 -3-0.12571 4.21455 26 2 0 3 0.92067 2.80377 25 -2 0 -3 1.21035 1.67080 15 -2 0 -4 540.361 12.1304 27 2 0 4 556.653 13.9517 24 2 0 4 548.219 7.68894 5 -2 0 -4 557.326 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7.94472 21 2 5 10 63.5009 8.82857 20 -2 -5 -10 82.6230 2.72478 12 2 5 10 72.7732 8.91229 27 2 5 10 87.1077 4.53878 4 2 5 11 29.2805 9.87444 7 2 5 11 34.7518 7.92319 20 2 5 11 24.2767 6.69492 27 -2 -5 -11 34.7632 7.01013 25 -2 -5 -11 27.8553 3.96877 5 2 5 12 57.0319 4.66541 10 2 5 12 59.0938 11.3759 7 2 5 12 46.7585 7.84960 27 -2 -5 -12 60.1789 10.7574 3 -2 -5 -12 59.0730 5.14572 5 2 5 13 24.8807 6.91365 27 2 5 13 23.0892 3.55267 10 2 5 13 7.25945 9.51495 7 -2 -5 -13 22.1218 3.88716 5 -2 -5 -13 22.0763 9.02464 3 -2 -5 -14 23.9568 4.10678 5 2 5 14 18.5168 3.70232 10 2 5 14 13.4794 10.0133 2 -2 -6 9 35.0515 11.7737 6 -2 -6 9 63.1747 5.38127 5 -2 -6 9 56.7318 11.9862 19 2 6 -9 61.2964 13.0292 2 -2 -6 8 18.0017 3.89583 12 2 6 -8 21.0344 9.41772 2 2 6 -8 19.3714 6.02422 1 -2 -6 8 34.3655 11.2651 6 -2 -6 8 22.8184 3.73157 5 -2 -6 8 22.8825 8.58924 19 2 6 -7 12.9650 5.16600 1 -2 -6 7 18.5585 9.81768 6 -2 -6 7 10.6631 3.26424 12 2 6 -7 20.5773 8.05360 2 -2 -6 7 6.96609 7.33770 19 2 6 -6 39.7425 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193.441 11.2953 7 2 6 6 191.871 12.0793 6 -2 -6 -6 204.559 11.0347 20 2 6 7 318.867 13.0710 3 -2 -6 -7 307.851 17.7408 21 2 6 7 307.673 14.1198 18 -2 -6 -8 1264.57 32.8219 25 2 6 8 1276.10 16.8499 4 -2 -6 -8 1287.76 24.6132 7 2 6 8 1206.64 24.8915 3 -2 -6 -8 1151.72 34.3755 21 2 6 8 1121.99 25.5964 18 -2 -6 -9 29.5058 8.30226 25 -2 -6 -9 39.9261 8.14540 21 2 6 9 37.2365 3.73977 4 2 6 9 26.9218 5.50816 18 2 6 9 33.4944 3.09044 10 2 6 9 38.6906 8.50935 27 2 6 10 13.2549 7.37432 20 -2 -6 -10 19.9142 1.98543 12 2 6 10 17.7378 2.66158 10 2 6 10 19.0466 7.32060 27 -2 -6 -10 20.6578 7.91251 25 -2 -6 -10 22.1399 6.89522 21 2 6 10 37.7107 5.40878 4 -2 -6 -10 16.8861 3.87781 5 -2 -6 -11 6.97640 7.27203 25 -2 -6 -11 4.17676 3.20102 5 2 6 11 21.3754 8.58645 20 2 6 11 5.10307 2.43768 4 2 6 11 1.21927 5.97711 27 -2 -6 -12 9.10382 3.54978 5 2 6 12 16.6288 6.95997 27 -2 -6 -12 14.4541 6.88603 25 2 6 12 5.72541 2.54158 10 2 6 13 99.3309 6.36056 10 -2 -6 -13 103.493 6.84295 5 2 6 13 76.2320 10.1187 27 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9.13056 7 2 7 9 68.2896 4.07905 10 2 7 9 64.9302 7.21139 3 2 7 9 57.5143 8.21105 18 2 7 9 64.9262 9.08948 6 -2 -7 -9 75.1400 7.61141 7 -2 -7 -9 65.6437 11.8012 25 -2 -7 -9 66.5560 10.6722 21 2 7 9 74.3985 4.97826 4 2 7 10 156.490 6.84168 4 2 7 10 118.741 10.6723 18 2 7 10 150.124 6.09714 10 2 7 10 139.592 13.9211 27 -2 -7 -10 138.299 13.7861 25 -2 -7 -11 18.9416 8.94801 25 2 7 11 12.8661 4.89972 4 -2 -7 -11 2.04101 3.52496 5 2 7 11-0.58524 7.13675 27 -2 -7 -12 840.700 18.8077 5 2 7 12 840.662 16.1771 10 2 7 12 735.262 27.8943 27 2 7 12 894.485 14.7037 4 -2 -7 -12 782.305 25.1263 25 2 7 13 23.1846 8.33827 27 2 7 13 27.4770 3.93097 10 -2 -7 -13 27.1872 4.84929 5 -2 -7 -13 30.1816 8.28758 25 2 7 14 23.8366 4.07295 10 -2 -7 -14 34.1406 5.35910 5 -2 -7 -14 17.6213 7.58251 25 -2 -8 6 264.881 9.84669 12 2 8 -6 299.743 19.2090 2 -2 -8 6 274.712 22.4489 6 -2 -8 5 181.552 18.1568 6 2 8 -5 187.619 14.1777 2 -2 -8 5 187.926 9.77778 8 -2 -8 5 180.802 7.71463 12 -2 -8 5 207.743 11.8716 26 2 8 -4 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194.390 13.9118 1 -2 -8 -2 172.981 12.3745 18 2 8 2 156.777 13.7251 19 2 8 2 186.467 14.5638 21 2 8 3 494.086 21.9545 19 2 8 3 540.012 22.6501 21 -2 -8 -3 532.662 24.7516 20 -2 -8 -3 536.497 19.6817 18 -2 -8 -3 504.651 20.0021 1 -2 -8 -4 413.577 21.6902 7 2 8 4 398.671 18.6538 19 2 8 4 433.240 23.4662 22 -2 -8 -4 449.086 21.6459 20 -2 -8 -4 458.728 18.9084 1 2 8 4 415.585 18.7194 21 2 8 5 55.3029 9.78642 22 2 8 5 52.3417 10.4043 6 -2 -8 -5 54.4201 10.0031 7 2 8 5 43.8091 7.69429 19 -2 -8 -5 45.6619 10.4160 23 -2 -8 -5 55.7191 8.84722 20 -2 -8 -6 30.9093 7.01571 20 2 8 6 29.5058 9.41035 6 2 8 6 27.8803 2.34841 10 2 8 6 39.3775 7.94386 3 -2 -8 -6 19.7646 8.20646 23 2 8 6 29.3051 8.08575 22 -2 -8 -6 32.7919 8.67177 7 -2 -8 -7 26.6145 7.45027 7 2 8 7 32.1251 7.78958 22 -2 -8 -7 28.5843 6.43114 20 2 8 7 38.8812 7.37195 3 2 8 7 21.5681 8.30311 6 2 8 7 23.7004 8.40084 18 2 8 7 27.6639 2.63070 10 -2 -8 -7 26.6465 8.94221 23 -2 -8 -8 71.0200 11.7525 21 2 8 8 100.957 11.6371 22 2 8 8 70.0776 10.7328 6 -2 -8 -8 74.6211 11.5940 23 2 8 8 71.5680 10.7610 18 -2 -8 -8 94.3488 10.0637 7 2 8 8 94.4772 4.40818 10 2 8 8 79.4117 8.79435 3 -2 -8 -8 98.7408 3.35994 13 2 8 9 78.3015 11.0778 6 2 8 9 92.5750 9.16640 3 2 8 9 68.6896 9.92626 18 -2 -8 -9 112.375 3.60516 13 2 8 9 104.628 4.95026 10 -2 -8 -9 104.159 9.80289 7 2 8 10 138.478 5.98260 10 -2 -8 -10 136.316 4.05853 13 2 8 10 150.581 7.12243 4 2 8 10 124.061 10.2409 3 -2 -8 -10 140.757 15.5346 25 -2 -8 -10 149.304 10.7208 7 2 8 10 122.917 13.1289 6 -2 -8 -11 87.0563 3.71124 13 2 8 11 107.160 6.40123 4 -2 -8 -11 97.9904 13.4970 25 2 8 11 73.2836 10.8816 6 2 8 11 76.8095 12.6005 27 2 8 12 63.3648 5.03025 10 2 8 12 54.1668 11.3503 27 2 8 12 56.7301 10.2102 6 -2 -8 -12 61.5672 6.46843 5 -2 -8 -12 69.1971 11.7396 25 2 8 13 60.4988 4.82750 4 -2 -8 -13 58.5002 6.49608 5 2 8 13 50.2936 10.1214 6 2 8 13 51.2301 5.04506 10 -2 -8 -13 58.9263 10.3928 25 -2 -9 5 7.69706 3.99281 8 -2 -9 5 6.49538 3.12910 12 -2 -9 5-4.02980 6.63218 9 2 9 -5 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1.74673 5.97266 2 3 -8 1 3.26116 9.23632 6 3 -8 1 0.92474 2.84455 8 -3 8 -1 7.22011 9.35971 23 -3 8 -2 20.3784 12.3564 23 3 -8 2 14.0365 7.26451 19 -3 8 -2 19.6285 7.05701 1 3 -8 2 17.7577 4.24107 8 -3 8 -2 38.2385 9.22256 2 3 -8 2 18.1403 7.47087 9 -3 8 -3 13.9104 6.78776 1 3 -8 3 2.81528 7.24322 9 -3 8 -3 11.0800 11.3538 23 -3 8 -3 33.0376 9.72828 2 3 -8 3 2.45826 6.92479 19 -3 8 -4 13.0255 9.55539 2 3 -8 4 0.82786 8.66583 9 -3 8 -4-7.43727 6.21881 1 3 -7 -12 12.4760 6.06121 1 -3 7 12 21.6443 9.47790 27 3 -7 -11 4.83229 5.40564 1 -3 7 11 5.93468 3.99626 14 -3 7 11 11.4288 9.13951 27 3 -7 -10 3.23979 5.24019 1 3 -7 -10 7.74209 5.93105 7 -3 7 10-6.39408 4.07423 14 -3 7 10-1.14860 5.97179 22 -3 7 10-3.34222 4.43970 3 3 -7 -9 115.706 10.8768 7 3 -7 -9 99.6953 11.0139 1 -3 7 9 105.141 12.7040 22 -3 7 9 125.871 10.6305 3 -3 7 9 121.108 6.85699 14 3 -7 -8 54.9290 9.93255 7 -3 7 8 19.1659 7.37025 22 3 -7 -8 46.4568 8.31110 1 -3 7 8 37.5301 7.50103 3 3 -7 -8 48.9132 6.54715 20 -3 7 8 44.4957 7.20419 19 -3 7 7 78.8592 4.97800 15 -3 7 7 62.5242 9.22915 21 3 -7 -7 83.6492 4.36322 10 3 -7 -7 63.0619 9.72505 1 -3 7 7 69.1996 8.31967 19 3 -7 -7 87.1068 8.73356 20 -3 7 7 78.4155 12.3843 22 -3 7 7 72.1086 10.2509 3 3 -7 -6 216.311 6.41897 10 3 -7 -6 199.133 12.3240 16 -3 7 6 211.966 6.74960 15 3 -7 -6 172.168 15.3001 1 -3 7 6 182.859 15.8623 21 3 -7 -6 204.484 13.6485 20 3 -7 -5 45.2844 5.86909 18 3 -7 -5 46.9356 3.28751 10 3 -7 -5 50.5070 10.4185 1 -3 7 5 46.7394 4.44904 14 -3 7 5 38.6762 8.94074 21 3 -7 -5 38.4658 7.04592 16 -3 7 5 48.9520 4.35232 15 -3 7 4-3.22585 6.50573 21 -3 7 4 6.91749 3.59986 15 -3 7 4 7.95297 6.48667 23 3 -7 -4-0.08686 4.50671 18 -3 7 4 11.0777 4.55741 17 3 -7 -4 5.39959 5.31972 16 3 -7 -4 11.8598 6.39362 6 -3 7 4 2.09070 3.14246 14 3 -7 -4 3.80278 7.09656 1 3 -7 -4 6.05304 1.88951 10 -3 7 3 14.7510 7.39710 21 3 -7 -3 31.8525 8.15384 6 3 -7 -3 26.0826 7.71686 16 -3 7 3 23.1390 3.74314 14 3 -7 -3 16.5793 6.49206 18 3 -7 -3 22.1421 2.49974 10 -3 7 3 30.7143 8.99608 23 -3 7 3 16.0690 5.27532 17 -3 7 2 13.7123 8.47090 23 3 -7 -2 15.6647 7.38737 16 -3 7 2 15.9401 3.66478 14 3 -7 -2 30.3895 8.26903 18 3 -7 -2 25.1654 8.77791 6 -3 7 2 21.1555 5.95109 17 -3 7 1 7.64048 6.18979 17 -3 7 1-3.75714 8.15261 23 3 -7 -1 4.82722 7.72067 6 3 -7 -1 3.92393 7.09622 16 -3 7 1 10.1469 4.72043 2 -3 7 0-5.81027 8.85256 23 -3 7 0 4.70589 4.61658 2 -3 7 0 6.54094 1.29197 13 3 -7 0 4.96006 2.49590 8 3 -7 0 6.94099 5.51406 19 3 -7 1 107.923 3.33375 11 3 -7 1 114.233 11.3475 19 3 -7 1 107.060 6.35351 8 -3 7 -1 121.730 9.84912 24 -3 7 -1 108.643 9.76014 2 -3 7 -1 96.8479 10.8626 1 3 -7 2-0.90971 5.80135 9 -3 7 -2 9.13618 5.75429 1 -3 7 -2 7.15908 5.81325 2 3 -7 2-4.98000 6.50850 19 3 -7 2 2.15804 2.94784 8 3 -7 3 100.464 12.8092 19 3 -7 3 95.1629 11.1611 9 -3 7 -3 95.7573 11.4457 2 -3 7 -3 71.0069 10.3449 1 3 -7 4 7.30152 7.80623 9 -3 7 -4 14.1731 8.57632 2 -3 7 -4 1.04645 5.64955 1 3 -7 4 15.0852 8.61734 19 3 -7 5-2.82789 8.28367 9 -3 7 -5 2.27108 6.78385 1 3 -7 5 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83.0150 8.72388 20 3 -6 -5 15.5737 3.98194 18 3 -6 -5 9.35301 4.89494 16 3 -6 -5 12.2548 5.91968 1 -3 6 5 11.2339 3.20701 14 3 -6 -5 12.1619 2.17579 10 -3 6 5 9.60865 3.13329 15 -3 6 5 8.92203 5.53306 21 -3 6 4 15.1551 3.10262 14 3 -6 -4 20.9967 2.52366 10 -3 6 4 13.0961 6.55455 21 3 -6 -4 10.0847 6.10854 1 -3 6 4 10.8076 6.00835 23 3 -6 -4 12.6578 4.42695 18 -3 6 4 19.6396 3.27637 15 3 -6 -4 15.9282 5.20225 16 -3 6 3 66.3072 10.6484 21 3 -6 -3 91.4647 9.35758 16 3 -6 -3 88.2274 9.10937 18 -3 6 3 84.1489 6.81241 17 3 -6 -3 76.9706 11.3392 1 -3 6 3 78.0039 11.6685 23 -3 6 3 77.0081 4.57215 14 -3 6 2 134.049 5.47683 14 -3 6 2 123.330 8.56293 17 3 -6 -2 128.616 12.4362 6 3 -6 -2 133.807 11.4757 16 -3 6 2 113.119 14.1249 23 -3 6 1 242.473 12.3932 17 -3 6 1 241.307 20.9191 23 3 -6 -1 268.951 7.24610 8 3 -6 -1 225.423 15.2915 16 3 -6 0 159.876 11.4508 19 -3 6 0 139.178 11.3143 1 -3 6 0 146.298 8.97714 2 -3 6 0 143.491 3.16546 13 3 -6 1 174.918 3.62162 11 3 -6 1 194.449 13.9265 19 3 -6 1 185.806 11.4649 26 -3 6 -1 183.599 10.3014 24 -3 6 -1 171.000 10.5148 2 -3 6 -1 157.726 12.7206 1 3 -6 2 99.4415 11.3015 19 -3 6 -2 103.919 9.55711 2 -3 6 -2 103.404 8.99255 24 3 -6 2 109.809 10.3172 26 3 -6 2 102.868 6.09012 8 -3 6 -2 79.2868 9.66091 1 -3 6 -3 34.7281 7.68245 24 3 -6 3 15.6917 6.40137 9 -3 6 -3 15.4820 6.66032 2 -3 6 -3 15.9068 6.06205 1 3 -6 3 17.8648 7.86197 19 -3 6 -4 6.56081 7.16572 2 3 -6 4 2.59636 6.94378 19 -3 6 -4-0.53020 6.09849 1 3 -6 4-0.64165 6.49072 9 -3 6 -5 242.835 18.1267 2 3 -6 5 289.975 18.8880 9 3 -6 5 243.003 19.4087 19 -3 6 -6 14.9932 8.11952 1 3 -6 6 24.7560 9.81156 9 -3 6 -6 33.4417 10.5382 2 3 -6 6 38.5436 11.5438 19 -3 6 -7 67.3954 12.8900 1 3 -6 7 115.800 15.7357 9 3 -5 -13 23.9512 4.30222 5 -3 5 13 25.8156 7.80284 2 -3 5 13 23.1527 6.38454 27 3 -5 -12 11.3584 3.74638 5 -3 5 12 11.7658 6.79191 27 3 -5 -11 0.20128 7.06088 23 -3 5 11 12.3401 6.69776 27 3 -5 -11 6.29525 3.60374 5 3 -5 -10 15.5653 8.40878 23 3 -5 -10-4.94500 5.39653 25 -3 5 10 15.7788 7.78782 27 -3 5 9-0.12151 1.37898 4 3 -5 -9 10.6338 8.05398 23 -3 5 9 4.73006 3.72812 3 3 -5 -9 2.61300 3.83069 7 -3 5 9 5.03169 3.44819 14 3 -5 -8 2.78044 1.86318 10 3 -5 -8 8.31735 7.99314 23 -3 5 8 0.98728 3.47349 3 -3 5 8 0.97481 3.08961 14 -3 5 8 5.11717 5.89513 22 3 -5 -8 8.11711 5.18264 7 3 -5 -8 0.19785 3.91467 1 -3 5 7 143.295 6.18495 14 -3 5 7 128.583 7.95884 19 3 -5 -7 131.887 5.30992 10 3 -5 -7 138.061 10.3913 1 -3 5 7 135.721 12.1167 22 3 -5 -7 122.313 9.41846 7 3 -5 -7 101.397 13.5030 23 3 -5 -7 135.883 7.31471 20 3 -5 -6 25.4325 5.44397 1 3 -5 -6 35.6161 5.74763 20 -3 5 6 28.2111 5.88611 21 3 -5 -6 31.9157 2.82476 10 -3 5 6 39.3811 5.36346 19 -3 5 6 27.5765 7.39350 22 -3 5 6 27.3300 3.28389 15 -3 5 6 29.4435 3.44656 14 3 -5 -5 21.2905 4.90370 16 -3 5 5 21.2126 3.05714 15 3 -5 -5 15.2853 5.50513 1 -3 5 5 23.6944 6.27867 21 -3 5 5 26.2327 3.20046 14 3 -5 -5 26.1151 2.63453 10 3 -5 -4 15.2336 4.96900 6 -3 5 4 14.1360 2.88022 14 -3 5 4 16.4615 5.63577 23 3 -5 -4 12.1684 5.71779 1 3 -5 -4 12.0362 4.24702 16 -3 5 4 13.6902 2.91712 15 -3 5 4 23.8355 6.73582 21 3 -5 -4 10.4534 3.58352 18 3 -5 -4 13.5720 2.10942 10 3 -5 -3 3.86618 5.08374 6 3 -5 -3 7.43203 4.81576 18 -3 5 3 9.28094 2.79389 14 -3 5 3 5.70259 2.66473 15 3 -5 -3 9.01579 4.40016 16 -3 5 3 4.59684 3.19710 17 3 -5 -3 2.54470 5.12189 1 -3 5 3 8.54663 5.94152 23 3 -5 -2 225.790 12.7718 16 -3 5 2 232.973 17.9868 23 -3 5 2 230.406 6.48947 14 -3 5 2 250.690 10.1330 17 -3 5 1 92.5129 8.43440 1 3 -5 -1 102.395 7.94116 19 3 -5 -1 92.9831 3.94736 8 -3 5 1 88.7810 7.40134 17 3 -5 -1 88.6434 9.42047 16 -3 5 1 57.5450 11.1844 23 -3 5 1 88.8322 2.46028 13 -3 5 0 11.6362 4.62940 1 -3 5 0-1.10395 1.27524 13 3 -5 0 10.5448 4.83093 19 3 -5 0 0.93020 1.66845 8 3 -5 1 58.9784 7.10464 26 3 -5 1 58.8352 8.16342 19 -3 5 -1 55.3544 7.68832 1 -3 5 -1 53.6335 6.19429 2 -3 5 -1 57.4668 6.21367 24 3 -5 1 57.2374 3.92786 8 3 -5 2 38.3431 6.30511 9 3 -5 2 46.2549 8.59178 19 -3 5 -2 43.3093 6.54279 24 -3 5 -2 51.3597 6.96459 2 3 -5 2 43.5327 7.35007 26 -3 5 -2 36.6061 7.35288 1 3 -5 3 20.3992 7.17025 19 3 -5 3 36.2149 8.36512 26 -3 5 -3 36.6791 8.05244 1 -3 5 -3 36.7663 7.37702 2 -3 5 -3 34.9737 6.92290 24 -3 5 -4 110.951 12.8849 1 -3 5 -4 134.039 12.2554 2 -3 5 -4 146.372 11.7686 24 3 -5 4 143.956 12.4505 26 -3 5 -5 127.017 12.2580 24 -3 5 -5 119.360 12.7263 2 -3 5 -5 122.901 14.8509 1 3 -5 5 135.718 13.1429 9 -3 5 -6 67.9852 8.64198 16 3 -5 6 67.5508 11.4159 9 -3 5 -6 59.9386 11.5143 1 3 -5 7 43.6587 7.56731 17 -3 5 -7 24.4189 9.56809 1 -3 5 -7 37.3748 7.59761 16 -3 5 -8 24.8304 7.45890 16 3 -5 8 11.1062 3.51015 5 3 -5 8 22.8072 3.47460 12 -3 5 -8 21.3757 9.61849 1 3 -5 8 10.2570 6.15468 17 3 -4 -14 101.519 5.97294 5 3 -4 -14 104.485 5.84850 12 -3 4 14 104.840 12.6476 24 -3 4 13 3.49922 4.97120 27 -3 4 13 8.27795 5.88578 2 3 -4 -13 3.91062 3.05835 5 3 -4 -13 2.72708 3.10578 12 3 -4 -12 44.7043 9.76641 23 3 -4 -12 55.6344 4.82890 5 3 -4 -12 53.2524 10.3011 21 -3 4 12 41.2523 7.46124 2 -3 4 12 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7.54301 3 -3 4 5 76.2339 5.90882 19 3 -4 -4 15.3381 3.18493 18 3 -4 -4 28.2619 4.73845 16 -3 4 4 18.4074 2.72126 15 -3 4 4 20.6891 2.77100 14 3 -4 -4 18.7199 4.19712 6 -3 4 4 16.5980 5.05658 23 -3 4 4 17.2614 5.37616 21 -3 4 3 130.802 11.8561 23 -3 4 3 115.567 4.43320 15 3 -4 -3 108.423 8.76281 6 3 -4 -3 130.360 8.29730 18 3 -4 -3 114.332 8.12784 16 -3 4 3 120.236 4.72659 14 -3 4 2 17.0896 2.67504 15 3 -4 -2 18.1307 5.02844 16 -3 4 2 16.2042 6.47668 23 -3 4 2 17.7377 3.55356 17 -3 4 1 112.411 2.80000 13 -3 4 1 104.181 6.88827 17 3 -4 -1 113.581 3.88438 8 3 -4 -1 100.261 9.05862 16 3 -4 -1 122.272 8.03015 19 -3 4 0 0.48236 2.95539 2 -3 4 0 1.88790 1.17643 13 3 -4 0-0.31051 1.48634 8 3 -4 0 3.31404 4.17100 19 3 -4 1-0.36129 4.49765 26 -3 4 -1-0.67181 3.51190 24 3 -4 1-0.83938 4.62175 19 3 -4 1 1.72113 1.78840 8 3 -4 2 108.073 8.45052 9 3 -4 2 111.889 8.90267 26 -3 4 -2 123.780 8.80083 16 3 -4 2 105.163 5.07961 8 -3 4 -2 87.7138 10.1135 1 -3 4 -2 94.3329 7.55009 24 3 -4 3 37.2666 7.23219 26 -3 4 -3 32.6339 6.23941 24 3 -4 3 35.7853 5.11072 17 -3 4 -3 33.6635 5.64431 16 -3 4 -3 38.3252 6.60137 2 -3 4 -3 36.1763 8.30118 1 3 -4 3 30.5337 6.03624 9 -3 4 -4 15.0302 6.21508 2 3 -4 4 16.8049 7.45518 26 -3 4 -4 4.49893 4.33541 16 3 -4 4 21.6750 6.89971 9 -3 4 -4 18.8647 6.58097 24 -3 4 -4 17.8303 7.30024 1 3 -4 4 13.0583 4.53225 17 -3 4 -5 2.68965 6.69744 2 -3 4 -5 5.12554 4.78211 16 3 -4 5 0.33052 8.42859 26 3 -4 5 2.17798 4.18641 17 -3 4 -6 27.2473 6.56819 16 3 -4 6 28.9509 9.69641 26 3 -4 6 27.2181 5.97430 17 3 -4 7 13.0444 3.08892 5 3 -4 7 10.8581 5.60309 17 3 -4 8 60.1517 5.19571 5 3 -4 8 56.0756 8.59300 17 -3 4 -8 64.7630 9.25976 16 3 -4 9 21.5862 7.26019 17 3 -4 9 23.5619 4.41335 5 -3 4 -9 21.3114 7.48836 16 3 -4 9 27.3250 3.66979 12 3 -4 10 9.87529 4.05888 5 3 -4 10 15.2094 3.66580 12 -3 3 14 38.3251 8.86334 24 3 -3 -14 37.5819 4.01819 12 -3 3 14 31.9253 6.76611 2 -3 3 13 15.8200 5.91129 2 3 -3 -13 9.13306 3.23316 12 3 -3 -13 5.73387 2.72941 5 3 -3 -12 51.0944 4.20768 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5.28553 5.19970 2 4 -8 -2 4.71001 2.82874 8 4 -8 -2 5.94859 8.70643 6 4 -8 -2 7.98908 7.36275 18 -4 8 2 3.11024 3.90479 15 -4 8 2 13.2079 9.60277 23 -4 8 1 11.6994 6.07179 2 4 -8 -1 7.16691 3.05589 8 -4 8 1 11.4681 8.92691 23 -4 8 1 7.56899 4.10652 15 4 -8 -1 20.8491 9.97159 6 4 -8 0 94.8402 10.8300 9 4 -8 0 93.0765 6.49281 8 4 -8 0 79.6598 14.3249 6 -4 8 0 94.2614 10.3718 2 -4 8 0 82.7610 16.7063 23 4 -8 1 49.2380 9.61002 9 4 -8 1 50.5399 5.67199 8 -4 8 -1 56.5492 10.2696 2 -4 8 -1 52.2995 15.4583 23 -4 8 -2 11.7913 6.46853 1 -4 8 -2 23.4687 9.21782 2 4 -8 2 20.1165 7.33455 19 4 -8 2 21.8433 8.91009 9 -4 7 11 35.3393 10.5267 27 4 -7 -11 19.8335 7.53304 1 -4 7 10 17.1355 7.79189 22 -4 7 10 8.05289 4.78269 3 4 -7 -10 22.6489 7.84225 1 -4 7 9 72.4144 11.4783 22 -4 7 9 77.8192 8.53380 3 4 -7 -9 61.9655 10.5845 1 4 -7 -8 24.5667 5.61656 20 4 -7 -8 23.2852 8.23761 1 4 -7 -8 21.9212 2.99721 10 -4 7 8 31.2447 7.35049 3 -4 7 8 13.7967 7.91973 22 4 -7 -8 35.5036 9.46233 7 -4 7 8 12.3133 5.64214 21 4 -7 -7 201.298 12.1249 20 4 -7 -7 191.547 6.83483 10 -4 7 7 159.711 14.4627 21 4 -7 -7 171.127 16.7668 1 -4 7 7 191.687 17.6332 22 -4 7 7 204.601 14.5119 3 4 -7 -6-0.45571 1.88074 10 -4 7 6 8.92819 6.28398 21 -4 7 6 6.70668 4.05938 17 4 -7 -6 5.00892 6.52072 20 4 -7 -6 6.91911 7.81459 1 -4 7 5 391.530 13.6148 17 4 -7 -5 411.604 14.2153 18 -4 7 5 362.478 23.5769 21 4 -7 -5 426.467 9.81553 10 4 -7 -5 415.461 16.9774 6 4 -7 -4 214.555 14.4600 6 4 -7 -4 218.143 12.2891 18 -4 7 4 217.397 11.1313 17 -4 7 4 188.035 18.2677 21 -4 7 4 201.868 18.0401 23 4 -7 -4 229.466 7.32983 10 4 -7 -3-1.83041 5.90617 18 -4 7 3 4.93903 6.79032 23 -4 7 3 17.5652 8.54397 21 -4 7 3 11.0515 5.64942 17 4 -7 -3 13.5926 7.78417 6 -4 7 2 226.823 13.2010 17 -4 7 2 213.099 21.2409 23 4 -7 -2 233.927 16.5052 18 4 -7 -2 227.148 18.0032 6 -4 7 2 273.486 12.0445 2 4 -7 -1 89.8173 13.3582 6 4 -7 -1 87.5827 5.36650 8 -4 7 1 70.7354 13.9188 23 -4 7 1 94.2880 8.51616 2 -4 7 0 156.623 10.6305 24 -4 7 0 155.576 11.3672 2 4 -7 0 150.920 7.30307 8 -4 7 -1 6.39258 5.62467 1 -4 7 -1 9.20406 6.65631 2 4 -7 1 0.48807 5.56064 9 4 -7 1 6.49086 3.12541 8 -4 7 -1-4.91006 9.85299 23 4 -7 1-2.28222 6.22057 19 4 -7 2 1.49182 6.51337 19 -4 7 -2 19.6671 7.88420 2 4 -7 2-0.67083 6.25945 9 -4 7 -2 4.61584 5.90210 1 -4 7 -3 229.128 17.2356 2 -4 7 -3 176.885 16.0494 1 4 -7 3 216.866 17.7520 19 4 -7 3 235.772 17.6458 9 4 -7 4 16.1300 8.67744 19 4 -7 4 12.6296 8.46051 9 -4 7 -4 15.3073 9.78757 2 -4 7 -4 8.74334 6.51352 1 4 -6 -12 25.9955 4.92243 5 -4 6 12 21.3838 8.13467 27 4 -6 -12 25.8743 7.34707 1 -4 6 11 85.7631 11.6192 27 4 -6 -11 81.3102 10.3416 1 -4 6 10 71.8574 11.0904 27 4 -6 -10 54.2665 8.46465 1 -4 6 9 63.0487 6.93948 3 4 -6 -9 56.0426 8.95834 1 4 -6 -9 48.5022 7.27197 16 -4 6 9 51.1056 8.94923 22 4 -6 -8 359.200 15.4151 16 4 -6 -8 389.278 9.87625 10 -4 6 8 370.196 21.0124 22 4 -6 -8 362.493 19.8694 1 -4 6 8 410.425 16.3248 3 -4 6 7 152.494 15.0246 22 4 -6 -7 150.340 10.8351 16 4 -6 -7 164.033 14.6135 1 -4 6 7 144.957 12.5415 21 4 -6 -7 159.560 6.33409 10 -4 6 7 187.968 12.7393 3 4 -6 -7 173.983 9.65243 20 4 -6 -6 44.6919 3.63001 10 -4 6 6 49.6004 9.56448 21 -4 6 6 47.5417 10.0871 22 4 -6 -6 41.1937 7.21077 20 -4 6 6 49.3156 4.73088 15 4 -6 -6 47.3746 7.46737 16 4 -6 -6 51.5180 9.60660 1 4 -6 -5 210.205 13.4361 16 -4 6 5 222.888 7.24165 15 -4 6 5 212.489 9.09860 17 -4 6 5 194.501 16.5912 21 4 -6 -5 194.679 16.9078 1 4 -6 -5 230.097 7.40947 10 4 -6 -5 214.098 9.22663 18 -4 6 4 194.217 6.77436 15 -4 6 4 196.990 9.53280 17 4 -6 -4 211.192 7.01601 10 4 -6 -4 189.362 13.3881 16 -4 6 4 192.603 17.1692 21 4 -6 -4 195.295 10.8019 18 -4 6 4 212.866 17.2087 23 -4 6 3 363.622 24.2657 23 4 -6 -3 356.390 18.6246 6 4 -6 -3 382.936 8.01639 8 -4 6 3 388.548 9.12178 15 -4 6 3 356.045 13.1691 17 4 -6 -3 345.190 16.5522 18 4 -6 -3 336.314 17.9106 16 4 -6 -2 26.6340 8.11514 16 -4 6 2 13.1123 3.55374 15 -4 6 2 10.4659 4.22355 2 -4 6 2 6.67011 5.23577 17 -4 6 2 18.7018 8.68480 23 4 -6 -2 10.8378 2.34650 8 -4 6 1 41.6699 6.01799 2 -4 6 1 41.3409 4.12353 15 4 -6 -1 46.7361 7.82093 26 -4 6 1 33.1411 10.8542 23 4 -6 0 360.061 16.0089 26 -4 6 0 345.369 14.4915 2 -4 6 0 302.762 17.3292 1 4 -6 0 339.502 16.1470 19 -4 6 0 336.322 13.2231 24 -4 6 0 339.614 5.62124 13 -4 6 -1 135.800 10.6681 2 -4 6 -1 121.600 12.1119 1 4 -6 1 126.202 10.8324 9 4 -6 1 126.610 12.0826 19 -4 6 -1 128.254 9.90720 24 -4 6 -1 134.229 3.84019 13 4 -6 2 138.148 12.1323 9 -4 6 -2 131.981 11.7710 2 -4 6 -2 108.450 12.0796 1 -4 6 -2 146.675 11.4103 24 4 -6 2 131.921 13.0029 19 4 -6 3 305.486 18.0757 9 4 -6 3 292.348 19.3578 19 -4 6 -3 245.821 18.1672 1 -4 6 -3 278.081 17.5143 2 4 -6 4-2.14067 7.66836 19 4 -6 4 5.31620 7.72007 9 -4 6 -4-9.71110 7.01272 1 -4 6 -4 12.4249 8.78169 2 4 -6 5 13.6840 9.10171 19 4 -6 5 19.2299 9.74877 9 -4 6 -5 3.57615 6.53548 1 4 -6 6 12.1331 9.77215 19 -4 6 -6 11.2746 8.45485 1 4 -6 6 16.7971 10.3040 9 -4 5 13 21.7729 6.49046 27 4 -5 -13 1.59398 3.31218 5 -4 5 12 8.23680 6.35693 27 4 -5 -12 20.8923 4.06649 5 4 -5 -12 18.8603 6.24911 1 4 -5 -11 161.412 12.2748 1 4 -5 -11 177.591 8.08275 5 -4 5 11 171.961 12.3059 27 4 -5 -10 0.34251 4.59171 1 -4 5 10-0.62599 6.68397 27 4 -5 -10 9.27133 8.98828 23 -4 5 9 164.625 9.30911 3 4 -5 -9 156.953 6.54780 10 4 -5 -9 141.115 11.4049 1 4 -5 -8 1.66988 1.87268 10 4 -5 -8 3.26801 1.85360 13 4 -5 -8 10.8797 5.58772 7 4 -5 -8-1.32135 4.31081 1 -4 5 8 2.16022 3.62159 3 -4 5 8 5.13531 5.71055 22 4 -5 -8 3.49155 4.25781 16 4 -5 -7 328.050 9.81615 20 -4 5 7 345.377 14.2418 3 4 -5 -7 307.390 16.7279 1 4 -5 -7 315.199 5.04843 13 -4 5 7 337.229 18.4173 22 4 -5 -7 311.822 8.63728 10 -4 5 7 318.714 16.0664 21 4 -5 -7 285.856 12.8159 16 4 -5 -6 42.7984 8.06771 1 4 -5 -6 34.8870 6.19112 16 -4 5 6 39.5502 8.34156 22 -4 5 6 39.0484 7.36541 21 4 -5 -6 40.9016 3.63156 10 4 -5 -6 28.1209 5.56299 20 4 -5 -5 15.0665 5.84196 16 4 -5 -5 18.2598 4.63231 6 -4 5 5 9.99689 5.85748 21 4 -5 -5 10.0299 2.42867 10 -4 5 5 8.62994 3.41576 15 4 -5 -5 11.1427 6.22540 1 4 -5 -4 46.7335 8.93514 1 -4 5 4 50.2925 4.94398 17 4 -5 -4 49.6173 6.89230 6 4 -5 -4 61.4579 7.97577 16 -4 5 4 50.7659 4.14592 15 -4 5 4 62.0504 9.98373 21 4 -5 -4 52.4967 5.75278 18 -4 5 4 56.3701 9.23784 23 -4 5 3 151.538 5.84261 15 -4 5 3 146.926 15.0284 23 4 -5 -3 130.643 11.2671 6 4 -5 -3 138.727 10.2013 18 -4 5 3 144.661 7.98620 17 4 -5 -3 126.800 10.9839 16 4 -5 -2 1068.29 12.5396 8 4 -5 -2 930.497 28.0732 16 -4 5 2 993.893 38.3534 23 -4 5 2 1074.00 13.9023 15 -4 5 2 1006.57 20.9328 17 4 -5 -1 42.5812 6.61043 26 4 -5 -1 44.0833 6.20232 19 -4 5 1 44.5607 4.05244 15 -4 5 1 46.9694 6.88116 1 4 -5 -1 44.0272 3.25784 8 -4 5 1 36.0946 10.1798 23 4 -5 0 7.87062 2.43717 8 -4 5 0 4.98449 4.48375 1 -4 5 0 4.18272 1.53902 13 4 -5 0 12.1888 6.14069 26 -4 5 0 5.04101 3.04016 15 4 -5 0 8.11116 5.50351 19 -4 5 0 8.58503 4.59370 24 4 -5 1 141.592 11.8774 19 -4 5 -1 131.790 11.7800 1 4 -5 1 135.394 2.42234 11 4 -5 1 154.250 11.5912 26 4 -5 1 143.750 6.35063 8 -4 5 -1 150.905 4.07806 13 -4 5 -1 165.394 6.41468 15 -4 5 -1 144.219 9.31598 24 -4 5 -1 155.067 10.3969 2 -4 5 -2 4.00511 4.88104 1 4 -5 2 14.8459 7.63592 26 4 -5 2 5.89554 6.88570 19 -4 5 -2 10.0987 5.98137 24 -4 5 -2-5.17625 6.22218 2 -4 5 -3 219.516 17.6276 1 4 -5 3 281.787 16.7184 26 -4 5 -3 252.598 15.4097 2 4 -5 3 219.941 16.4051 19 -4 5 -3 259.591 14.0661 24 -4 5 -4 99.7346 11.1088 24 -4 5 -4 88.1565 12.5620 1 4 -5 4 90.1930 11.4391 9 -4 5 -4 94.7644 11.5632 2 -4 5 -5 33.7028 7.44942 16 -4 5 -5 30.6524 9.68542 1 4 -5 5 32.5722 9.64453 9 4 -5 6 162.964 16.4392 9 -4 5 -6 130.408 16.6982 1 -4 5 -6 177.753 13.5788 16 -4 5 -7 138.093 12.6155 16 4 -5 7 155.909 7.75789 5 4 -5 8 344.512 9.57008 12 4 -5 8 308.552 11.1937 5 -4 4 13 127.986 9.61396 27 4 -4 -13 150.691 7.25594 12 4 -4 -13 131.734 6.29589 5 -4 4 13 122.720 11.5062 24 4 -4 -12 257.854 8.49167 5 -4 4 12 241.093 12.3073 27 4 -4 -11 24.7591 9.13540 23 4 -4 -11 20.5584 3.67878 5 -4 4 11 22.2990 6.31376 27 -4 4 10 564.361 18.4913 27 -4 4 10 540.188 15.2395 2 4 -4 -10 606.709 12.8529 5 4 -4 -9 97.5637 13.1859 23 -4 4 9 122.218 10.2213 27 4 -4 -9 114.367 9.33524 1 4 -4 -9 117.716 5.75809 10 4 -4 -8 146.592 6.17185 10 4 -4 -8 160.814 6.49527 7 4 -4 -8 157.363 10.6221 1 4 -4 -7 52.3804 6.12551 16 4 -4 -7 54.2031 6.95589 1 4 -4 -7 53.9950 3.94031 10 -4 4 7 48.3070 7.58622 22 4 -4 -7 62.7726 6.65295 7 -4 4 6 27.4256 6.84517 22 4 -4 -6 31.7708 3.22274 10 4 -4 -6 33.3907 2.28182 13 4 -4 -6 27.2433 4.98582 16 4 -4 -6 34.6345 4.00941 20 -4 4 6 34.0578 5.99885 21 -4 4 6 33.3825 5.19375 3 4 -4 -5 1672.71 29.1674 16 -4 4 5 1812.76 39.1574 21 -4 4 5 1729.52 28.9751 3 4 -4 -5 1768.50 11.1470 13 4 -4 -5 1846.08 20.4015 10 -4 4 4 181.388 13.6527 21 -4 4 4 206.497 14.1373 23 -4 4 4 186.162 6.74691 17 4 -4 -4 179.342 9.89081 6 -4 4 4 191.896 6.12011 15 4 -4 -4 183.765 10.9893 16 4 -4 -4 193.731 7.40498 18 -4 4 3 138.500 5.35974 15 4 -4 -3 125.762 10.1706 16 -4 4 3 139.026 13.3732 23 -4 4 3 117.145 6.33572 17 -4 4 2 658.590 12.4654 2 -4 4 2 670.160 10.4004 15 -4 4 2 610.484 14.7474 17 -4 4 2 640.967 29.0339 23 4 -4 -2 679.009 8.89375 8 4 -4 -2 618.252 21.2408 16 4 -4 -1 140.737 8.94418 26 4 -4 -1 146.824 4.77042 8 -4 4 1 140.225 5.47858 15 -4 4 1 137.469 7.13353 2 4 -4 -1 153.953 9.38286 19 -4 4 0 2077.63 39.2620 1 -4 4 0 2011.38 17.8740 15 4 -4 0 2031.10 31.7872 26 -4 4 0 2019.80 13.3927 13 -4 4 0 1974.94 25.5423 24 4 -4 0 2010.88 34.7653 19 -4 4 0 1966.31 27.0972 2 4 -4 0 2031.70 18.7075 8 -4 4 -1 275.183 5.28938 13 -4 4 -1 273.716 7.15789 15 4 -4 1 283.029 13.2516 9 -4 4 -1 256.358 10.8642 24 4 -4 1 218.020 13.4185 19 4 -4 1 271.552 13.5199 26 4 -4 1 258.492 7.54911 8 -4 4 -1 251.232 15.6268 1 -4 4 -2 280.020 7.49997 15 4 -4 2 261.275 14.4127 26 -4 4 -2 251.249 12.0190 24 -4 4 -2 240.720 12.8813 2 -4 4 -2 276.593 13.7589 16 4 -4 2 241.800 13.1056 9 -4 4 -2 232.666 16.5249 1 -4 4 -3 408.397 22.8414 1 -4 4 -3 467.493 19.1337 2 -4 4 -3 488.202 18.6021 16 4 -4 3 502.347 20.1937 26 -4 4 -3 475.842 17.6492 24 -4 4 -4 172.059 12.1505 16 4 -4 4 188.550 10.5127 17 4 -4 4 171.191 14.2526 26 -4 4 -4 140.406 15.1355 1 -4 4 -5 280.045 15.6688 16 4 -4 5 289.309 18.3594 9 -4 4 -5 241.813 20.4968 1 4 -4 5 291.984 13.7496 17 4 -4 6 106.741 9.54393 17 -4 4 -6 87.6058 10.1981 16 4 -4 6 110.312 13.4734 9 4 -4 7 104.827 6.19640 5 4 -4 7 102.338 10.0402 17 -4 4 -7 97.5462 10.9877 16 4 -4 8 149.164 12.1616 17 -4 4 -8 126.016 12.5160 16 4 -4 8 148.911 7.80687 5 4 -4 8 166.305 6.42767 12 -4 4 -9-0.25771 4.08164 15 4 -4 9 2.83478 3.66490 5 4 -4 9 0.96541 2.75720 12 4 -3 -13 141.670 6.82794 12 -4 3 13 124.972 10.7242 24 4 -3 -12 5.32047 2.71520 5 4 -3 -12 1.31317 3.07030 12 -4 3 12 1.74459 6.30999 24 -4 3 11 45.5330 6.07477 27 -4 3 11 38.6631 7.41951 24 4 -3 -11 21.4567 8.28438 23 4 -3 -11 42.9616 3.89272 5 -4 3 10 5.91479 4.64879 27 -4 3 10 5.06567 4.00937 2 4 -3 -10 2.09590 2.62363 5 4 -3 -10 5.17947 6.40167 23 4 -3 -9 2.75582 6.45238 23 4 -3 -9 3.76084 2.09230 10 -4 3 9 5.82248 4.75189 27 -4 3 9 9.98834 4.15668 2 4 -3 -8 1155.33 35.7182 23 -4 3 8 1245.83 18.8485 2 -4 3 8 1421.50 25.6501 27 4 -3 -8 1349.52 17.7787 10 4 -3 -7 73.8124 4.43892 10 4 -3 -7 77.1566 3.98630 7 4 -3 -7 73.5598 5.94729 16 -4 3 7 81.9982 8.05681 27 4 -3 -6-2.49750 3.44840 16 -4 3 6 0.16773 4.03641 22 4 -3 -6 2.83603 1.83114 10 -4 3 6 3.88741 2.70373 3 4 -3 -5 499.345 17.1754 1 -4 3 5 556.761 18.6481 21 -4 3 5 562.730 19.7930 22 -4 3 5 554.388 13.9410 3 4 -3 -5 501.895 9.85594 20 4 -3 -5 503.221 14.7405 16 4 -3 -5 550.446 10.9671 10 4 -3 -5 542.610 7.39033 13 4 -3 -4 370.646 11.1358 6 4 -3 -4 412.382 7.63213 14 -4 3 4 407.766 17.4848 21 -4 3 4 440.714 17.8338 23 4 -3 -4 391.357 14.0510 16 -4 3 4 394.293 7.58406 17 4 -3 -4 415.141 5.87288 13 4 -3 -4 382.046 16.4792 1 -4 3 3 15.6068 2.28204 2 -4 3 3 18.0177 3.11806 17 4 -3 -3 22.4763 5.60288 16 4 -3 -3 20.3695 2.41884 14 -4 3 3 27.7669 6.72804 23 -4 3 2 103.400 7.44309 1 4 -3 -2 89.1487 6.59194 26 -4 3 2 82.7482 10.6378 23 -4 3 2 90.9590 4.59444 2 4 -3 -2 91.7243 3.01686 8 4 -3 -2 85.3713 3.78077 14 -4 3 2 88.2283 4.28978 15 4 -3 -1 454.893 13.6729 26 -4 3 1 421.072 14.9827 1 4 -3 -1 457.054 13.2595 19 4 -3 -1 451.860 7.24740 8 -4 3 1 447.464 10.7571 2 4 -3 -1 433.495 7.40750 14 -4 3 1 436.979 8.08325 15 4 -3 0 22.7512 4.74429 9 -4 3 0 17.8643 3.79345 24 -4 3 0 22.4728 4.33787 16 -4 3 0 19.8376 1.91018 13 4 -3 0 13.8411 2.02975 14 4 -3 0 24.3367 5.70229 26 -4 3 0 13.5748 2.55919 15 4 -3 0 18.9145 2.18720 8 -4 3 0 15.8464 4.40511 2 4 -3 1 486.919 15.7183 9 -4 3 -1 464.538 13.1908 24 -4 3 -1 476.873 14.5001 2 4 -3 1 477.488 7.17236 14 4 -3 1 475.074 16.3716 26 -4 3 -1 484.309 16.1383 16 -4 3 -1 485.291 8.68204 15 -4 3 -1 483.477 6.87099 13 -4 3 -2 577.774 18.8653 16 -4 3 -2 588.569 16.6662 24 4 -3 2 604.773 14.5774 17 4 -3 2 596.427 7.56275 14 4 -3 2 595.929 18.8648 9 -4 3 -2 606.795 9.67832 15 -4 3 -2 551.485 24.2409 1 4 -3 2 603.203 19.9040 26 -4 3 -3 145.410 5.34202 15 -4 3 -3 127.084 10.2244 16 4 -3 3 139.372 8.46008 17 4 -3 3 139.970 10.8712 9 4 -3 3 143.117 12.0775 26 -4 3 -4 10.5628 3.17081 15 4 -3 4 9.07731 6.37618 9 4 -3 4 5.64601 7.48474 26 4 -3 4 4.09639 4.53355 17 -4 3 -4 12.4362 5.69809 16 -4 3 -5 272.023 7.17181 15 4 -3 5 262.506 13.2731 17 -4 3 -5 236.244 14.9828 16 -4 3 -6 106.567 8.57209 27 4 -3 6 108.610 5.56403 5 -4 3 -6 103.912 11.3454 16 -4 3 -6 108.771 5.38070 8 4 -3 6 121.482 10.3270 17 -4 3 -6 125.103 5.52196 15 4 -3 7 10.4696 3.04998 5 -4 3 -7 4.72313 3.42360 15 4 -3 7 2.74922 5.43991 17 -4 3 -7 3.65565 2.20125 8 -4 3 -7 8.37562 6.71918 16 4 -3 8 14.8445 6.61679 17 -4 3 -8 11.6805 2.78995 8 4 -3 8 11.0796 3.44974 5 -4 3 -8 19.0986 7.98693 16 -4 3 -9 33.0129 9.29925 16 4 -3 9 25.7972 7.64878 17 4 -3 9 39.0655 5.02808 5 -4 3 -9 36.3192 4.28362 4 -4 3 -9 33.7337 3.95524 8 -4 3 -10 56.7197 5.00699 8 4 -3 10 78.0731 5.07715 12 -4 3 -10 67.9068 5.57362 4 4 -3 10 69.5479 6.71925 5 4 -2 -13 69.7466 5.09896 12 -4 2 13 68.1211 8.26735 24 -4 2 12 354.236 14.8276 24 4 -2 -12 321.322 9.19409 8 -4 2 11 9.85843 6.11387 24 4 -2 -11 11.4209 3.12029 12 4 -2 -11 11.5052 2.53781 5 4 -2 -10 229.570 15.5744 23 -4 2 10 232.686 8.51028 2 4 -2 -10 267.237 6.91878 5 -4 2 10 264.403 12.6002 24 4 -2 -10 194.698 13.9968 21 4 -2 -10 298.095 6.40611 15 4 -2 -9 68.9390 9.42940 23 -4 2 9 77.1413 6.13291 27 -4 2 9 69.0360 5.09207 2 -4 2 9 76.5604 7.73452 24 4 -2 -9 80.7690 4.09691 15 4 -2 -8 53.3532 3.39563 5 4 -2 -8 48.8914 8.10644 23 4 -2 -8 66.9750 3.70274 15 4 -2 -8 52.9835 3.84661 10 -4 2 8 59.0962 4.58649 2 -4 2 8 51.6812 5.39898 27 4 -2 -7 467.093 11.2571 16 4 -2 -7 523.299 10.8025 10 4 -2 -7 479.516 13.8849 1 4 -2 -7 564.828 9.03275 15 -4 2 7 483.516 9.51277 2 4 -2 -7 444.905 20.3818 23 -4 2 7 522.258 13.3216 27 4 -2 -6 170.761 7.32020 16 4 -2 -6 188.468 5.33680 15 -4 2 6 203.202 9.09056 27 4 -2 -6 171.225 8.45808 1 4 -2 -6 185.596 6.50012 10 -4 2 6 176.318 4.93252 2 4 -2 -6 195.265 5.78412 14 -4 2 5 311.842 11.0562 21 4 -2 -5 290.862 11.3174 1 4 -2 -5 302.301 6.19009 15 4 -2 -5 307.865 6.71784 14 -4 2 5 253.318 4.42957 2 -4 2 5 331.270 12.6193 22 4 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-5 -7 178.791 8.14782 13 -8 -5 -7 140.445 16.8000 26 8 5 7 157.229 16.5220 7 -8 -5 -7 116.705 12.9761 9 8 5 8 8.84490 9.98311 7 -8 -5 -8 9.70491 8.92573 9 -8 -5 -8 8.29659 3.45578 13 -8 -5 -8-9.67063 11.4722 26 -8 -5 -9 47.8414 10.9542 9 -8 -5 -9 32.2548 4.48409 13 8 5 9 20.8230 11.5648 7 8 6 -4 70.5119 5.52943 13 8 6 -3 86.9042 5.55268 13 8 6 -2 38.3948 3.93047 4 8 6 -2 37.2067 4.10646 13 -8 -6 2 47.7266 7.83886 25 8 6 -1 49.9116 4.39561 4 -8 -6 1 52.5793 8.14930 25 8 6 -1 42.9645 4.04861 13 8 6 -1 49.8079 10.9784 6 -8 -6 0 32.9226 8.14370 25 8 6 0 15.6501 6.95385 19 8 6 0 20.6996 3.53607 4 8 6 0 27.2746 9.21443 6 -8 -6 -1 26.9364 7.71417 25 8 6 1 30.1445 4.01130 4 8 6 1 21.6789 8.34567 6 8 6 1 17.8591 6.38294 19 8 6 2 46.4295 9.56953 18 8 6 2 77.3940 6.21206 4 -8 -6 -2 61.8000 9.19848 25 -8 -6 -2 57.6165 7.86271 9 8 6 2 53.2090 9.48733 6 -8 -6 -3 103.868 10.3849 9 -8 -6 -3 92.5867 10.2109 25 8 6 4 319.019 9.55030 4 -8 -6 -4 318.120 16.1924 25 -8 -6 -5 75.9438 9.98706 25 -8 -6 -5 71.9548 10.8543 9 8 6 5 77.3298 5.55747 15 8 6 5 71.1606 5.07437 4 -8 -6 -6 20.0492 8.83613 9 8 6 6 25.9734 11.4024 7 8 6 6 12.3707 3.32159 4 -8 -6 -6 6.76653 7.11893 25 8 6 6 19.4848 4.27851 15 8 6 7 16.4366 10.8301 7 -8 -6 -7 4.14801 8.79660 9 -8 -6 -7 3.46049 3.35507 13 -8 -6 -8 416.220 23.2589 9 8 6 8 477.540 28.1684 7 8 7 -3 337.099 9.86072 13 -8 -7 2 11.0326 8.03674 25 8 7 -2 14.3410 3.47633 4 8 7 -2 14.5693 3.52724 13 8 7 -1 94.7389 5.77799 4 8 7 -1 107.821 5.63103 13 -8 -7 1 116.908 11.9254 25 8 7 0 1285.58 18.8461 4 -8 -7 0 1352.17 32.0604 25 8 7 1 97.3889 5.99574 4 8 7 1 97.5449 13.8634 6 -8 -7 -1 109.304 12.5196 25 8 7 2 73.8974 5.59009 4 -8 -7 -2 82.6207 11.4141 25 8 7 2 67.6809 11.9136 6 8 7 3 163.770 7.70120 4 -8 -7 -3 141.517 12.0135 9 8 7 3 137.826 14.3840 6 -8 -7 -3 181.338 14.1440 25 8 7 4 6.38425 4.46791 4 8 7 4-1.15767 6.48448 6 -8 -7 -4 3.81599 8.10123 25 -8 -7 -5 402.048 19.7373 25 -8 -7 -5 446.329 11.4459 11 -8 -7 -6 38.7529 10.1625 9 8 7 6 35.6873 4.41577 4 -8 -7 -6 37.3302 4.00076 11 8 7 6 31.4315 5.89857 27 8 7 6 39.2934 4.69002 15 -8 -7 -6 32.7278 9.13772 25 -8 -7 -7 130.844 14.5139 9 8 7 7 113.256 8.64205 27 8 7 7 129.780 7.08871 4 -8 -7 -7 118.767 12.2159 25 -8 -7 -7 135.265 6.23358 11 -8 -7 -8 16.0968 3.19485 11 -8 -7 -8-2.09773 9.51805 9 8 8 -1 38.0357 4.10658 13 -8 -8 1 43.7115 11.1487 25 -8 -8 0 3.91734 9.49240 25 8 8 0 2.42971 3.39290 4 8 8 1 6.47566 9.39993 6 8 8 1 14.1120 3.93101 4 8 8 2 154.898 17.7438 6 8 8 2 160.994 7.96874 4 -8 -8 -2 183.237 16.0060 25 8 8 3 30.0082 10.5156 6 8 8 3 41.7335 4.92567 4 -8 -8 -3 50.3215 11.5345 25 -8 -8 -4 184.471 15.9953 25 8 8 4 153.416 16.5496 6 8 8 4 181.749 8.64578 4 -8 -8 -4 190.585 8.29235 11 -8 -8 -5 8.73748 8.95258 25 8 8 5 2.51444 7.80986 6 -8 -8 -5 11.0619 3.42274 11 8 8 5 3.97178 3.69980 4 8 8 6 88.4889 13.2467 6 -8 -8 -6 110.594 6.25510 11 -8 -8 -6 81.2039 12.0526 25 8 8 7 220.031 12.3805 27 8 8 7 194.660 18.0362 6 -8 -8 -7 295.832 9.48934 11 8 8 7 281.442 10.7596 4 -8 -8 -7 200.059 17.4486 9 8 9 2 29.6840 4.72619 4 8 9 2 28.6606 12.6764 6 -8 -9 -2 56.7894 13.2576 25 8 9 3 243.652 10.0877 4 -8 -9 -3 244.787 19.1530 25 8 9 4 19.2853 10.9492 6 -8 -9 -4 24.9757 4.34713 11 8 9 4 34.0687 5.18713 4 9 -3 -3 56.0019 11.0823 9 9 -3 -3 39.3177 4.79348 14 -9 3 3 35.0807 8.95694 23 -9 3 2 36.5218 8.98692 21 9 -3 -2 69.6900 12.1062 9 9 -3 -2 64.6429 5.38658 14 -9 3 2 67.8015 13.0972 23 9 -3 -1 23.0898 10.2084 9 -9 3 1 6.77044 9.34971 23 9 -3 -1 3.66387 3.79523 14 9 -2 -6 23.8189 3.54546 11 9 -2 -4 27.5406 4.77103 14 -9 2 3 38.9863 8.03993 23 9 -2 -3 39.1368 4.82714 14 9 -2 -2 5.58230 3.85194 14 -9 2 2-0.36650 6.54495 23 -9 2 2-5.70017 5.96631 21 9 -2 -1 8.67394 4.16114 14 -9 2 1 16.6282 9.11852 23 -9 2 0 170.709 6.91209 4 -9 2 0 167.700 13.0042 1 9 -2 0 203.348 7.68492 14 9 -2 1 36.5782 4.64908 14 -9 2 -1 24.1616 6.93236 1 -9 2 -1 30.5575 4.29323 4 -9 2 -2 34.0972 8.77574 1 9 -2 2 54.3763 4.80533 14 -9 2 -2 47.0317 4.92035 4 -9 2 -2 43.3079 8.67072 16 9 -1 -6 58.8143 4.17336 13 9 -1 -6 53.4360 4.42774 11 9 -1 -5 98.1008 6.51087 14 9 -1 -5 67.4164 4.47045 11 9 -1 -4 9.78681 2.67710 11 9 -1 -4 16.3928 4.28894 14 9 -1 -3 45.3412 5.17866 14 -9 1 2 9.27410 6.49420 23 9 -1 -2 8.39106 4.20885 14 -9 1 1 7.79337 7.84390 23 9 -1 -1 13.9129 4.18085 14 9 -1 -1-1.40054 4.44838 7 -9 1 0 9.67357 5.13262 1 9 -1 0 7.02151 3.91656 14 9 -1 0 16.6409 5.35419 7 -9 1 -1 18.3452 6.64482 16 9 -1 1 19.7587 4.28939 14 -9 1 -1 17.9875 6.67742 1 -9 1 -2 1.00247 6.08761 16 -9 1 -2 5.32942 6.79346 1 9 -1 2 13.9846 3.94738 14 9 -1 3 10.5464 3.81865 14 -9 1 -3 1.59903 3.34275 4 -9 1 -3 1.56111 7.21900 1 -9 1 -4 25.1864 4.56604 4 -9 1 -4 35.8798 4.74356 13 9 -1 4 34.7838 4.37426 14 -9 1 -4 38.9224 11.3709 1 9 0 -7-2.35410 2.52930 13 9 0 -7-1.46853 2.68727 12 9 0 -7 3.71871 2.73483 11 9 0 -6 74.5684 6.05284 10 9 0 -6 101.718 6.16407 15 9 0 -6 110.799 6.78536 14 9 0 -6 75.7441 4.93456 11 9 0 -6 99.8333 5.24145 13 9 0 -5 145.737 7.39572 15 9 0 -5 126.105 7.14169 14 9 0 -5 108.767 5.41165 11 9 0 -5 133.332 5.84142 13 9 0 -4 37.0619 3.50495 11 9 0 -4 41.9891 5.17688 15 9 0 -4 44.0749 5.20284 14 9 0 -3 59.7001 5.59344 14 9 0 -3 54.3758 5.34597 15 9 0 -3 49.4325 3.63038 11 9 0 -2 146.280 7.41138 14 9 0 -1 140.615 7.14070 14 -9 0 1 121.507 12.9186 23 9 0 0 50.7263 7.37196 7 -9 0 0 40.6359 7.08042 16 9 0 1 25.2621 6.29822 7 -9 0 -1 19.1070 7.13837 16 -9 0 -1 13.4514 6.18415 1 -9 0 -2 97.9871 12.1279 1 -9 0 -2 112.082 11.8948 16 9 0 2 131.312 9.81712 7 9 0 3 94.4378 9.07545 7 -9 0 -3 78.2710 11.4583 16 -9 0 -3 80.8810 12.7438 1 9 0 4-2.94599 5.51137 7 -9 0 -4 4.44599 7.58213 16 -9 0 -4 3.39316 3.44504 13 -9 0 -4 16.9104 9.85400 1 -9 0 -5 47.7597 5.19327 13 9 0 5 46.9516 4.80837 14 9 0 5 38.3962 7.77334 7 9 1 -6-1.47680 2.45442 11 9 1 -6 2.16597 2.34926 13 9 1 -6 3.11130 2.55778 10 9 1 -6-0.70461 3.93719 15 9 1 -6 6.53142 3.81201 14 9 1 -6 3.03967 2.88364 12 9 1 -5 24.0089 3.87883 12 9 1 -5 15.7655 2.90794 13 9 1 -5 21.7977 4.88041 14 9 1 -5 24.7201 5.23116 15 9 1 -5 15.0180 3.03943 11 9 1 -4 190.448 8.20001 14 9 1 -4 203.862 8.19795 15 9 1 -4 167.067 6.26086 11 9 1 -4 189.356 6.88641 13 9 1 -3 7.36873 2.42465 11 9 1 -3 3.24897 4.03727 15 9 1 -2 122.668 6.63343 15 9 1 -1 76.2793 5.82493 15 -9 -1 1 65.5277 7.00898 16 -9 -1 0 34.8003 6.90271 16 9 1 0 57.9891 8.15468 7 9 1 0 47.9256 4.87648 15 9 1 1 38.8477 7.38506 7 -9 -1 -1 30.5534 7.87965 16 -9 -1 -1 22.6809 6.21478 1 9 1 2 26.9668 6.66270 7 -9 -1 -2 37.1745 9.10463 16 -9 -1 -2 22.7729 7.89320 1 -9 -1 -3 50.2075 10.4351 16 9 1 3 55.1483 8.24524 7 -9 -1 -4 5.60000 8.03916 16 -9 -1 -4 13.5058 3.93940 13 9 1 4 14.5733 6.56088 7 -9 -1 -5 21.2374 10.1851 16 -9 -1 -5 21.0600 4.23223 13 9 1 5 3.12508 6.25476 7 9 1 6 89.8638 10.7218 7 -9 -1 -6 111.782 7.21436 13 9 2 -6 0.14488 2.27560 11 9 2 -6 4.76232 2.74121 13 9 2 -6 1.74769 2.43276 12 9 2 -6 4.96242 3.46936 14 9 2 -6 5.47027 4.12336 15 9 2 -6 6.76846 2.62805 10 9 2 -5 13.9905 3.22385 12 9 2 -5 20.0222 5.26518 15 9 2 -5 9.65639 2.81980 13 9 2 -5 9.74747 2.60730 11 9 2 -4 5.31069 3.03176 12 9 2 -4 4.93844 4.25145 15 9 2 -4 9.04952 2.75384 13 9 2 -4 8.15653 2.55051 11 9 2 -3 5.37158 2.70095 12 9 2 -3 1.40988 2.10071 11 9 2 -3 4.49826 2.56663 13 9 2 -3-1.85278 4.19064 15 9 2 -2 36.6562 3.65172 12 9 2 -2 32.3146 4.90971 15 9 2 -1 16.6800 4.65624 15 -9 -2 1 10.1609 4.43401 16 9 2 0 11.2010 7.52052 7 9 2 0 16.0276 4.41835 15 -9 -2 0 22.3332 6.39960 16 -9 -2 -1 55.2988 9.06497 16 9 2 1 71.0576 5.54888 15 9 2 1 74.8827 9.58065 7 9 2 2 40.3752 4.61061 15 9 2 2 51.1885 9.06248 7 -9 -2 -2 48.9348 8.17577 26 -9 -2 -2 51.6497 10.0341 16 -9 -2 -2 21.3620 6.92262 1 -9 -2 -3 25.5314 7.58866 26 -9 -2 -3 30.1587 9.25928 16 9 2 3 10.5474 7.00679 7 9 2 4 17.6311 7.75254 7 -9 -2 -4 19.5574 7.86816 26 -9 -2 -5 80.1264 6.12602 13 9 2 5 68.8341 10.2682 7 -9 -2 -5 80.8118 10.6500 26 9 2 6 13.9972 7.66225 7 -9 -2 -6 18.7397 4.22019 13 9 3 -6 143.695 6.40669 11 9 3 -6 144.565 7.54191 10 9 3 -6 159.866 6.34673 12 9 3 -5 28.4735 3.40731 12 9 3 -5 26.3583 4.08106 10 9 3 -5 25.7884 3.20476 11 9 3 -5 32.2513 4.09331 13 9 3 -4 25.6023 2.93220 11 9 3 -4 27.0675 3.33348 12 9 3 -4 30.1302 3.76897 13 9 3 -4 37.8834 5.88453 15 9 3 -3 3.94518 2.53069 12 9 3 -3 5.39694 2.89290 13 9 3 -3 5.36327 5.02086 15 9 3 -2 143.902 5.37060 12 9 3 -2 153.801 7.80251 15 9 3 -1 33.1907 4.90348 15 9 3 -1 35.9828 3.13980 12 9 3 0 4.02626 4.19827 15 -9 -3 0-1.20380 5.16405 16 9 3 0 3.57474 8.34806 7 -9 -3 0 13.8232 6.06294 26 9 3 1 24.1564 4.63110 15 -9 -3 -1 17.2679 7.12103 16 9 3 1 34.0141 9.91574 7 -9 -3 -1 28.1093 7.37046 26 9 3 2 37.9978 9.27732 7 9 3 2 31.9989 4.67556 15 -9 -3 -2 36.8338 8.67767 26 9 3 3 39.9902 9.50782 7 9 3 3 36.8974 4.75278 15 -9 -3 -3 39.8814 9.18930 26 9 3 4-4.72982 7.51368 7 -9 -3 -4 9.16597 8.34978 26 -9 -3 -5 188.502 8.76460 13 -9 -3 -5 167.521 14.5296 26 9 3 5 154.870 13.9230 7 -9 -3 -6 4.66750 8.64045 26 9 3 6 6.32613 7.02639 2 -9 -3 -6 3.96002 3.43737 13 9 3 6 9.34730 8.19369 7 9 4 -5 64.8407 4.18563 12 9 4 -5 60.0870 5.04375 10 9 4 -4 9.17936 3.40886 13 9 4 -4-0.93467 2.36988 12 9 4 -3 6.98878 2.93277 13 9 4 -3 13.4034 2.72047 12 9 4 -2 27.3961 3.58762 13 9 4 -2 31.9284 3.05720 12 -9 -4 1 30.0250 5.88330 26 -9 -4 0 106.799 9.37703 26 9 4 0 95.4239 10.2468 6 9 4 0 107.715 6.84642 15 -9 -4 -1 5.68369 7.33001 26 9 4 1 21.1414 5.09282 15 -9 -4 -2 311.051 16.6744 26 9 4 2 356.388 9.81284 15 9 4 2 320.765 19.3984 7 9 4 3 9.24471 4.30622 15 9 4 3 8.25872 9.12297 7 -9 -4 -3 15.2264 8.48476 26 9 4 3-3.57725 5.34486 18 -9 -4 -4 70.4474 8.66613 9 -9 -4 -4 70.1640 11.8121 26 9 4 4 95.7238 13.0354 7 9 4 4 92.9267 5.89923 15 9 4 5 33.4324 4.70592 15 9 4 5 37.0148 10.9643 7 -9 -4 -5 36.6009 10.9413 26 -9 -4 -5 24.1674 7.53121 9 9 4 6 21.7606 8.80571 2 -9 -4 -6-4.31960 9.19952 26 9 4 6-0.16210 9.17132 7 -9 -4 -6 2.15234 3.45612 13 -9 -4 -6 6.67302 6.85161 9 9 4 7 17.3789 8.42575 2 9 4 7 15.9821 9.60489 7 -9 -4 -7 15.6582 7.81458 9 -9 -4 -7 16.9682 4.19132 13 9 5 -4 7.44550 3.10370 10 9 5 -3 95.6732 5.82350 13 9 5 -2 42.6058 4.27086 13 9 5 -1 38.6088 10.0065 6 -9 -5 0 1.20040 6.70092 26 9 5 0 13.9657 7.61886 6 -9 -5 -1 62.7836 9.67297 26 9 5 1 48.7142 9.43896 6 9 5 2 34.7058 5.23864 15 -9 -5 -2 39.5741 10.4303 26 -9 -5 -3 6.60238 5.63069 9 9 5 3 4.91808 4.54879 15 -9 -5 -4 50.1135 11.8931 26 9 5 4 58.0970 12.5466 7 9 5 4 54.2978 5.29408 15 -9 -5 -4 35.1559 7.74019 9 -9 -5 -5 25.9599 10.8207 26 -9 -5 -5 44.5430 8.78247 9 9 5 5 39.6893 12.3860 7 9 5 5 45.3908 4.91774 15 9 5 6 188.985 18.4319 7 9 5 6 228.395 7.32524 15 -9 -5 -6 180.526 14.1921 9 -9 -5 -6 181.132 17.7408 26 9 6 -2 11.8401 3.34363 13 9 6 -1 14.9139 9.30160 6 -9 -6 1 13.3601 5.63060 25 -9 -6 0 53.4873 9.55244 26 9 6 0 52.1837 11.2660 6 -9 -6 0 54.5516 7.81418 25 9 6 0 46.6541 4.10654 4 -9 -6 -1 29.7872 9.56401 26 -9 -6 -1 22.8835 6.75808 25 9 6 1 26.5156 3.59188 4 9 6 1 19.3807 8.96904 6 -9 -6 -2-5.80137 9.27749 26 -9 -6 -2 3.17691 6.53063 25 9 6 2 5.77387 6.69961 6 9 6 2 3.08081 2.60923 4 9 6 3 7.24305 7.17008 6 -9 -6 -3 3.33649 10.1857 26 9 6 3 12.9037 3.32678 4 -9 -6 -4 28.1421 11.3501 26 -9 -6 -4 31.4833 8.08041 9 9 6 4 31.8745 5.02376 15 -9 -6 -5 52.0093 13.1412 26 -9 -6 -5 40.4159 9.04459 9 9 6 5 54.8236 5.11801 15 -9 -6 -6 12.8351 12.1155 26 -9 -6 -6 13.4194 8.44534 9 -9 -7 1 25.0153 7.38595 25 9 7 0 53.1743 12.5800 6 -9 -7 0 51.0298 8.98263 25 9 7 0 70.9459 6.27453 4 9 7 1 25.1771 10.8764 6 -9 -7 -1 29.9679 8.30939 25 9 7 2 13.9051 4.08542 4 9 7 2 14.1728 9.21321 6 -9 -7 -2 10.0014 7.28864 25 9 7 3 78.5056 5.72440 4 9 7 3 63.6704 11.9751 6 9 7 4 23.9458 3.80616 4 -9 -7 -4 28.9638 8.16914 25 -9 -7 -5-12.5488 7.78246 25 9 7 5 0.71065 7.19809 6 -9 -7 -5 10.7026 8.73859 9 9 7 5 4.46120 4.48977 15 9 7 5 3.95949 3.10443 4 -10 -1 0 232.702 13.1063 16 10 1 1 28.5362 8.23980 7 -10 -1 -1 31.1082 7.78649 16 10 2 -1 41.9583 5.21227 15 10 2 0 11.1134 4.79795 15 -10 -2 0 0.90384 4.56928 16 -10 -2 -1 33.7882 7.91350 16 10 2 1 46.4428 10.1419 7 -10 -2 -2 298.309 18.2367 16 10 2 2 369.340 19.1062 7 10 3 0 24.9349 5.10292 15 10 3 1 36.7466 5.49608 15 -10 -3 -1 16.4661 6.87457 16 10 3 2 27.0127 4.88803 15 10 3 2 41.2185 10.8718 7 -10 -3 -2 23.5801 8.11003 26 -10 -3 -2 23.1241 8.61579 16 10 3 3 38.2566 11.0248 7 -10 -3 -3 34.4406 10.1043 16 -10 -3 -3 31.1162 8.49824 26 10 4 0 325.859 10.4170 15 10 4 1 10.8910 4.93943 15 -10 -4 -1 5.90094 6.67226 26 10 4 2 247.947 18.5469 7 -10 -4 -2 234.177 14.8248 26 0 0 0 0.00 0.00 0 TITL z00151320901_pl_jp_inc_om100_bkg1 in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 7.159349 8.219202 10.418237 70.7372 89.8582 77.7187 ZERR 2.00 0.000371 0.000446 0.000626 0.0052 0.0045 0.0046 LATT 1 SFAC Li O Si Ca UNIT 4.00 26.00 8.00 8.00 REM CrysAlisPro recorded range (K): Min=300.7; max=301.8; aver:301.2 TEMP 28 SIZE 0.02 0.03 0.04 TREF HKLF 4 END ; _shelx_hkl_checksum 78018 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.708 _oxdiff_exptl_absorpt_empirical_full_min 0.253