# Development of a Double-tilt Liquid Cell Holder for Zone-axis Incidence Imaging of FIB-prepared Single Crystal Samples

https://mdr.nims.go.jp/datasets/d40c72c8-d639-4397-92c5-4bafccd2b4c7

## File

- [MMPaper2025(M.Takeguchi).pdf](https://mdr.nims.go.jp/filesets/17317ac0-36da-4ba8-a810-d345b3d49ec8/download) ([Detail](https://mdr.nims.go.jp/filesets/17317ac0-36da-4ba8-a810-d345b3d49ec8.md))

## Id

d40c72c8-d639-4397-92c5-4bafccd2b4c7

## Local identifier



## Visibility

open_to_public

## State

published

## Created at

2025-09-11T10:21:58.684852Z

## Updated at

2025-09-12T02:41:26.237522Z

## Published at

2026-01-25T05:23:42.145000Z

## Doi

https://doi.org/10.48505/nims.5759

## First published url

https://doi.org/10.1093/mam/ozaf048.879

## Date published

2025-07-25

## Recorded date published

2025-7-25

## Resource type

conference_presentation

## Manuscript type

accepted_manuscript

## Collection



## Title

- title: Development of a Double-tilt Liquid Cell Holder for Zone-axis Incidence Imaging
    of FIB-prepared Single Crystal Samples
  title_type: original
  lang: en

## Description

- description: 'We developed a double-tilt liquid cell holder to image single crystal
    samples in a liquid on the zone-axis incident condition. FIB-prepared SrTiO3 <100>
    samples were picked-up and put onto a liquid cell chip window at the desired positions
    using a glass probe and an optical microscope. Atomic-resolution ADF-STEM images,
    acquired after aligning the sample orientation along the <100> zone axis, showed
    Sr and Ti-O atomic columns with high contrast. Thus, it was demonstrated that
    electron channeling along several tens nm atomic columns resulted in high-contrast
    atomic images overcoming background from thick windows and media.  '
  description_type: abstract
  lang: eng

## Creator

- name: Masaki Takeguchi
  role: author
  orcid: https://orcid.org/0000-0002-0282-6020
  organization: National Institute for Materials Science
  department: Research Center for Energy and Environmental Materials (GREEN)/Battery
    and Cell Materials Field/Environment-Controlled Microscopy Group
- name: Jonathan Lueke
  role: author
  organization: Norcada (Canada)
- name: Baibing Zhao
  role: author
  organization: KITANO SEIKI Ltd
- name: Ayako Hashimoto
  role: author
  orcid: https://orcid.org/0000-0002-1985-7667
  organization: National Institute for Materials Science
  department: Research Center for Energy and Environmental Materials (GREEN)/Battery
    and Cell Materials Field/Environment-Controlled Microscopy Group

## Contact agent



## Publisher

organization: Oxford University Press (OUP)

## Managing organization



## Keyword

- subject: Double-tilt Liquid Cell Holder
  schema: not_defined
- subject: FIB-prepared Single Crystal Sample
  schema: not_defined

## Rights

- description: 'This is a pre-copyedited, author-produced version of an article accepted
    for publication in Microscopy and Microanalysis following peer review. The version
    of record Masaki Takeguchi, Jonathan Lueke, Baibing Zhao, Ayako Hashimoto, Development
    of a Double-tilt Liquid Cell Holder for Zone-axis Incidence Imaging of FIB-prepared
    Single Crystal Samples, Microscopy and Microanalysis, Volume 31, Issue Supplement_1,
    July 2025, ozaf048.879 is available online at: https://doi.org/10.1093/mam/ozaf048.879.'
  identifier: http://rightsstatements.org/vocab/InC/1.0/

## Other identifier(s)



## Data origin

- data_origin_type: other

## Embargo

start_date: 2025-07-25
end_date: 2026-01-25

## Journal

- title: Microscopy and Microanalysis
  issn: '14319276'
  volume: '31'

## Conference

name: The Microscopy & Microanalysis 2025 Meeting (M&M 2025).
start_date: 2025-07-27
end_date: 2025-07-31
identifier: https://mmconference.microscopy.org/

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## Fileset

- id: 17317ac0-36da-4ba8-a810-d345b3d49ec8
  filename: MMPaper2025(M.Takeguchi).pdf
  content_type: application/pdf
  size: 239564
  md5: 22cb930b447285c7c255e2d517eecaee

## Thumbnail

fileset_id: 17317ac0-36da-4ba8-a810-d345b3d49ec8
filename: MMPaper2025(M.Takeguchi).pdf