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A narrow-gap semiconductor with a complex crystal structure was recently discovered in the Al–Ru–Si system. To determine the homogeneity range of the semiconductor phase and further discover new phases, phase equilibria in the Al–Ru–Si system near 1200 K were investigated through prolonged-annealing experiments. Eleven new ternary phases including two incommensurate composite-crystalline and an icosahedral quasicrystalline phases were identified using powder and single-crystal X-ray diffraction, and their compositions at two-phase and
three-phase equilibria were evaluated by means of electron-probe X-ray microanalysis. On the basis of the data obtained in this study and those adopted from the literature, a tentative isothermal section of the Al–Ru–Si equilibrium phase diagram near 1200 K was drawn.

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Keyword: aluminium–ruthenium–silicon system, phase equilibrium, crystal structure, X-ray diffraction, electron-probe X-ray microanalysis, incommensurate composite crystal, quasicrystal

Date published: 2024-01-01

Publisher: Japan Institute of Metals

Journal:

• MATERIALS TRANSACTIONS (ISSN: 13475320) vol. 65 issue. 1 p. 18-26 MT-M2023128

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Manuscript type: Publisher's version (Version of record)

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First published URL: https://doi.org/10.2320/matertrans.mt-m2023128

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Updated at: 2024-12-13 12:30:48 +0900

Published on MDR: 2024-12-13 12:30:48 +0900